Industrial Process Design
Industrial Process Design
Design
Evaluate Economics
& Select Design
Customer
Approval
Detailed Design & Procurement
Begin Operation
Equipment Selection & Construction
Project Business
Sponsor Input
Project
Manager
• On-time
5 Verify Full Design Criteria
6 Process Design/Optimization
7 Cold Flow Modeling 206 days
8 Design Sparger
9 Approve Sparger Design 7/15
10 Construction of Wedge
11
12
13
PP design/construction/shakedown
Cold Flow Testing
Catalyst Scale-up 150 days
• On-budget
14 Catalyst Scale-up
15 Demonstration Plant 251 days
24 Procurement
this happens
25 Fabrication
26 Delivery & Installation
27 Begin Run 12/28
Evaluate Economics
& Select Design
Customer
Approval
Detailed Design & Procurement
Begin Operation
Equipment Selection & Construction
deliverables
8 Design Sparger
9 Approve Sparger Design 7/15
10 Constru ction of Wedge
11 PP design/construction/shakedown
12 Cold Flow Testing
13 Catalyst Scale-up 150 days
• Allows scheduling of
14 Catalyst Scale-up
15 Demons tration Plant 251 days
20 Basic Engineering
21 P&ID re view 5/18
24 Procurement
25 Fabrication
We need to know:
• What are we designing? How much of it do we want?
• Where will it be built? What are the boundary conditions?
Plant Location
Correspondance Contacts
Address
2 Measurement System
4 Primary Products
Product Name
Product Grade
MSDS Form Number
• This record is also essential in handing
off information between the operating
Production Rate
Tons per year
Tons per day
Other units
contractors
5 Primary Raw Materials
(Attach additional sheets if needed)
Feedstock name
Feedstock availability
Tons per year
Elsevier.com/Towler
Tons per day
Other units
Known feedstock impurities Name ppmw Name ppmw Name ppmw Name ppmw
http://booksite.elsevier.com/9780080966595/
Additional specifications
6 Site Information
DESIGN BASIS
Form XXXXX-YY-ZZ
1 General Information
Owners Name
Plant Location
Correspondance Contacts
Address
Telephone / Fax
E-mail
2 Measurement System
English Metric
Project Name
3 Equipment Numbering System
Product Name
Product Grade
MSDS Form Number
Production Rate
Tons per year
Tons per day
Additional Specifications
Feedstock availability
Tons per year
Tons per day
Other units
Known feedstock impurities Name ppmw Name ppmw Name ppmw Name ppmw
Additional specifications
6 Site Information
DESIGN BASIS
Form XXXXX-YY-ZZ
1 General Information
Owners Name
Plant Location
Correspondance Contacts
Address
Telephone / Fax
E-mail
2 Measurement System
English Metric
4 Primary Products
Product Name
Product Grade
MSDS Form Number
Production Rate
Tons per year
Tons per day
Other units
Feedstock availability
Tons per year
Tons per day
Other units
Process Unit Name
Feedstock price ($/lb)
(Default: open market price)
Known feedstock impurities Name ppmw Name ppmw Name ppmw Name ppmw
Plant Location
Correspondance Contacts
Additional specifications
E-mail
Other site design requirements
Contact information
• Company name
• Process unit name
• Who to contact & where to reach them
DESIGN BASIS
Form XXXXX-YY-ZZ
1 General Information
Owners Name
Plant Location
Correspondance Contacts
Address
Telephone / Fax
E-mail
2 Measurement System
English Metric
4 Primary Products
Product Name
Product Grade
2 Measurement System
MSDS Form Number
Production Rate
Tons per year
Tons per day
Other units
Additional Specifications
English Metric
5 Primary Raw Materials
(Attach additional sheets if needed)
Feedstock name
Feedstock grade
MSDS form number
Known feedstock impurities Name ppmw Name ppmw Name ppmw Name ppmw
6 Site Information
Conventions followed
• Units of measurement
– Customer specific and may also depend on location
– Design engineers have to be able to work with both metric and English units
Form XXXXX-YY-ZZ
1 General Information
Plant Location
Correspondance Contacts
Address
Telephone / Fax
E-mail
2 Measurement System
AC Air cooler
Metric
Product Name
Product Grade
MSDS Form Number
Other units
Production Rate
Tons per year
Tons per day
Other units
Additional Specifications
Feedstock availability
Tons per year
Tons per day
Other units
Known feedstock impurities Name ppmw Name ppmw Name ppmw Name ppmw
Product Purity (wt%)
Additional specifications
Additional Specifications
Site elevation (ft)
Maximum wind loading (mph)
Other site design requirements
DESIGN BASIS
Form XXXXX-YY-ZZ
1 General Information
Owners Name
Feedstock availability
Plant Location
Correspondance Contacts
Address
Telephone / Fax
E-mail
2 Measurement System
English Metric
Tons per year
Tons per day
3 Equipment Numbering System
Other units
indicated CT Cooling tower M Mixer V Vessel (including columns)
D Dryer ME Miscellaneous equipment
First digit - process section E Exchanger P Pump
Second & third digits - equipment count F Filter, classifier PRV Pressure relief valve
4 Primary Products
Product Name
Product Grade
MSDS Form Number
Production Rate
Tons per year
Tons per day
Other units
Additional Specifications
Feedstock availability
Tons per year
Tons per day
Other units
Known feedstock impurities Name ppmw Name ppmw Name ppmw Name ppmw
Additional specifications
6 Site Information
• Feedstock grades
• Safety information
• Availability and pricing
• Feed impurities and their concentrations
DESIGN BASIS
Form XXXXX-YY-ZZ
Owners Name
Plant Location
English Metric
Product Name
Product Grade
MSDS Form Number
Production Rate
Tons per year
Additional Specifications
Feedstock availability
Tons per year
Tons per day
Other units
Known feedstock impurities Name ppmw Name ppmw Name ppmw Name ppmw
Additional specifications
6 Site Information
Site information
• Ambient conditions needed for design of insulation, air coolers, etc.
• Special conditions such as wind loads, hurricane and earthquake
conditions that are needed for mechanical and civil engineering
design
Form XXXXX-YY-ZZ
DESIGN BASIS
Sheet 2 of the Design Basis has
utility information
7 Utility Information
Fuel Gas
Gas source or operation mode Nat Gas
Supply header temperature (F)
Supply header pressure (psia)
Net calorific value (BTU/lb)
Marginal availability (lb/h)
Marginal fuel cost ($/MMBTU)
• Fuel gases
Sulfur content (wppm)
Nitrogen content (wppm)
Chlorine content (wppm)
Gas composition (vol%)
H2O
O2
N2
CO
CO2
• Fuel oils
H2S
H2
CH4
C2H4
C2H6
C3H6
C3H8
C4H8
iC4H10
nC4H10
• Steam levels
C5H10
C5+
Fuel Oil
Fuel source or operation mode #2 Heating Oil
Supply header temperature (F)
Supply headder pressure (psia)
Net calorific value (BTU/lb)
Marginal availability (lb/h)
• Coolants
Marginal fuel cost ($/MMBTU)
Fuel viscosity at F
Fuel viscosity at F
Flash point (F)
Pour point (F)
Sulfur content (wppm)
Nitrogen content (wppm)
Ash content (wt %)
Steam
• Process water
Steam header classification VHP HP MP LP
Operating pressure (psia)
Operating temperature (F)
Mechanical design pressure (psia)
Mechanical design temperature (F)
Marginal availability (lb/h)
Marginal cost ($/Mlb)
Coolants
• Electricity
Coolant classification Cooling Tower Water Once-Through Water Chilled Water
Operating pressure (psia)
Supply temperature (F)
Maximum return temperature (F)
Marginal availability (lb/h)
Marginal cost ($)
Marginal cost units
• Process Air
Supply pressure (psia)
Supply temperature (F)
Marginal availability (lb/h)
Marginal cost ($/1000 gal)
Total dissolved solids (wt%)
Hardness as CaCO3 (ppmw)
Chloride as Cl (ppmw)
Metallurgy
• Standard sizes for piping & equipment, compositions, etc. are given in
standards
• Tubing dimensions, valve sizes, exchanger layouts, screw threads, wire gauges, screens, …
• Always consult the current (latest) edition of the code. Always make
sure that the codes and standards used comply with local legal
requirements.
• By convention, feeds
enter at left, products exit
right
• Often summarized as a
table at the bottom of the
PFD
1 2 3 4 5 6 7 8 9 10 11 12
25C 25C 25C 25C 25C 25C 25C 25C 25C 25C 25C 25C
120 kPa 121 kPa 122 kPa 123 kPa 124 kPa 125 kPa 126 kPa 127 kPa 128 kPa 129 kPa 130 kPa 131 kPa
kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol%
Hydrogen
Helium
Lithium
Beryllium
Boron
XYZ Co.
Nitrogen
Carbon
Nitrogen
Oxygen
Fluorine
Neon
T otal
1 2 3 4 5 6 7 8 9 10 11 12
25C 25C 25C 25C 25C 25C 25C 25C 25C 25C 25C 25C
120 kPa 121 kPa 122 kPa 123 kPa 124 kPa 125 kPa 126 kPa 127 kPa 128 kPa 129 kPa 130 kPa 131 kPa
kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol% kg/h kmol/h wt% mol%
Hydrogen
Helium
Lithium
Beryllium
Boron
Nitrogen
Carbon
Nitrogen
XYZ Co.
Oxygen
Fluorine
Neon
Total
properties
Normal temperature ºF
Max temperature ºF
Min temperature ºF
Pressure psia
Pressure drop allowed psi
Number of passes
Film transfer coefficient Btu/h.ft2.F
7. Equipment specification
Fouling coefficient Btu/h.ft2.F
Heat duty Btu/h
FT factor
Effective mean temperature difference ºF
Minimum surface required ft2
sheets
CONSTRUCTION & MATERIALS PER SHELL
Tubes
Material
Count Pitch in Square Triangular Welded
Length ft O.D. in Wall thickness in
Shell
diagram
Material
Length ft I.D. in Wall thickness in
Design pressure at max temp psia Test pressure psia Min internal pressure psia
Baffle material Baffle type Baffle pitch in
Tubesheet material Tubesheet thickness in
Bonnet material Bonnet type
1.
2.
3.
4.
5.
summary information
Surface per unit ft2 Surface per shell ft2
DATA PER UNIT
for design
Dynamic viscosity lbm/ft.s
Specific heat capacity Btu/lb.F
Thermal conductivity Btu.ft/h.ft2.F
Latent heat Btu/lb
Normal temperature ºF
Max temperature ºF
Min temperature ºF
Pressure psia
Pressure drop allowed psi
• Calculated design
Pressure drop calculated psi
Flow velocity ft/s
Number of passes
equipment
Minimum surface required ft2
Tubes
Material
Count Pitch in Square Triangular Welded
Length ft O.D. in Wall thickness in
• Dimensions and
Design pressure at max temp psia Test pressure psia Max external pressure psia
Number of tubes blanked
Shell
Material
construction details
Length ft I.D. in Wall thickness in
Design pressure at max temp psia Test pressure psia Min internal pressure psia
Baffle material Baffle type Baffle pitch in
Tubesheet material Tubesheet thickness in
Bonnet material Bonnet type
Branches
Shell side inlet in N.B. Shell side outlet in N.B.
• Notes
Tube side inlet in N.B. Tube side outlet in N.B.
NOTES
1.
2.
3.
4.
5.
booksite.Elsevier.com/Towler
• http://booksite.elsevier.com/9780080966595/
• Capital costs
– Working capital
– Installed capital cost
– Royalty costs
– Annual capital charge
© 2012 G.P. Towler / UOP. For educational use in conjunction with
Towler & Sinnott Chemical Engineering Design only. Do not copy Chemical Engineering Design
Design Documentation
• Information on materials safety is
1. The design basis
2. A written description of the process
required for hazard analysis,
3. Process flow diagram detailed design
4. At least one mass & energy balance
5. Product specifications and
properties • Material Safety Data Sheets
6. A list of major plant equipment (MSDSs) must be provided to
7. Equipment specification sheets
8. A piping and instrumentation employees and customers by law
diagram in the U.S.A. (OSHA Hazard
9. A cost estimate
Communication Standard 29 CFR
10.HS&E information
Part 1910.1200)