MCL2
MCL2
– 2
Stress – Relaxation Experiment on Thermoplastic
material
OBJECTIVE:
To determine the mechanical behaviour of a thermoplastic sample by plotting
stress and strain curve with the help of UTM (Universal Testing Machine).
THEORY:
The test is conducted on a dog-bone specimen made of Poly Lactic Acid (PLA).
A 3D printed sample is prepared by using fluid deposition moulding. A stress
relaxation test measures how the stress in a material change over time while the
strain is held constant. This experiment is particularly useful for understanding
the time-dependent behaviour of thermoplastics under deformation. The sample
will be subjected to tensile loading, and the corresponding stress and strain data
will be acquired during the test.
∈ = ∈𝑠 + ∈ 𝑑
𝑑 ∈ 𝑑 ∈𝑠 𝑑 ∈𝑑
= +
𝑑𝑡 𝑑𝑡 𝑑𝑡
( 𝜎𝑠 = 𝜎𝑑 = 𝜎)
𝑑 ∈ 1 𝑑 𝜎𝑠 𝜎𝑑
= +
𝑑𝑡 𝐸 𝑑𝑡 𝜂
𝑑 ∈ 1 𝑑𝜎 𝜎
= +
𝑑𝑡 𝐸 𝑑𝑡 𝜂
𝜎 𝐸
ln = − (𝑡 − 𝑡0 )
𝜎0 𝜂
Since, 𝑡0 = 0
𝜎 𝐸
ln = − 𝑡
𝜎0 𝜂
𝜎 𝐸
− 𝑡
= 𝑒 𝜂
𝜎0
𝐸
− 𝑡
𝜎 = 𝜎0 𝑒 𝜂
APPARATUS:
1. Digital Universal Testing Machine (UTM)
2. Data Acquisition system
3. Poly Lactic Acid (PLA) Sample
4. Vernier Calliper Scale
OBSERVATION:
Least count of Vernier Calliper Scale = 0.02mm
Length of the Sample = 61.38 mm
Width of the Sample = 13.06 mm
Thickness of the Sample = 3.4 mm
Cross-Sectional area of the sample = 44.404 mm2
➢ Strain vs Time
Strain v/s Time
0.007
0.006
0.005
Strain
0.004
0.003
0.002
0.001
0
-2 0 2 4 6 8 10 12
Time (min)
➢ Stress vs Time
3
Stress (MPa)
2.5
1.5
0.5
0
0 2 4 6 8 10 12
Time (min)
CONCLUSIONS:
1. Thermoplastics exhibit both elastic (instantaneous) and viscous (time-
dependent) responses.
2. The gradual decrease in stress shows the material’s viscoelastic
relaxation.
3. The rate of stress decrease gives insight into the relaxation time (τ) of the
thermoplastic.
PRECAUTIONS:
1. Wear appropriate safety gear, including safety glasses and gloves.
2. Fixtures must be properly lubricated to reduce the effect of friction.
3. Follow the manufacturer’s safety guidelines for handling and disposal of
chemicals.