Particle Technology
Particle Technology
Importance
1.1 Particle Shape
● 0
Solids used in chemical industries are most ● The shape of an individual particle is
commonly in the form of particles.
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expressed in terms of the sphericity which is
● Solids in general are more difficult to handle
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independent of particle size.
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one.
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● Particulate materials, powders or bulk powders For non-spherical particle it is defined by:
or bulk solids are used widely in all areas of
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the process industries, for example in the food
processing, pharmaceutical, biotechnology, oil,
chemical mineral processing, metallurgical,
detergent, power generation, paint, plastics
and cosmetics industries,· (11)
● So the knowledge of their properties, handling,
storage, transportation, separation and ● The equivalent diameter is sometimes defined
processing is important from a chemical as the diameter of a sphere of equal volume.
engineering point of view. (b)
●
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For fine particles, 𝐷𝑝 is usually taken to be the
--
microscopic analysis.
Individual solid particles are characterized by
0
their size, shape and density.
● -
The surface area is found from adsorption
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bed of particles.
Size and shape are easily specified for regular
not
sub-ideas
● Better control of quality of product (cement,
urea, cosmetics etc.) enumeration
are One
not equidimensional, therefore cannot be
specified by a single dimension i.e. “diameter””
- -
C
2
area per unit mass,
𝑚 plates, where the size in at least one
𝑔
dimension can differ significantly from that of
other dimensions.
● Such particles are often characterized by the
second longest major dimension. For example
0
needle like particles, 𝐷𝑝 would refer to the
-
-
of particles.
particulate samples is particle size. men
- Packing density and porosity e.g. particle size which is relevant to the situation
ene
individual particles in it -
-
𝑁
can be counted or ∑ 𝑁𝑖𝐷𝑝𝑖
2
increments,
m
starting with that containing the ● Mass mean diameter:
smallest particles, and tabulating or plotting the 𝑁
cumulative sums against the maximum particle 𝐷𝑤 = ∑ 𝑥𝑖𝐷𝑝𝑖
diameter in the increment. 𝑖=1
● Volume mean diameter:
1.3 Mixed Particles sizes and size analysis 1
3
● In a sample of uniform particles of diameter 𝐷𝑝, ⎡ ⎤
⎢ 1 ⎥
the total volume of the particles is
𝑚
ρ𝑝
, where m 𝐷𝑣 = ⎢ 𝑁 𝑥 ⎥
⎢ ∑ 𝑖
3 ⎥
= mass of the sample, ρ𝑝 = density. Since the ⎣ 𝑖=1 𝐷 𝑝𝑖 ⎦
volume of the particle is 𝑣𝑝 the total number of ● For samples consisting of uniform particles
these average diameters are, of course, all the
particle in the sample is:
same. For mixtures containing particles of
𝑚
𝑁 = ρ𝑝 𝑣𝑝
various sizes, however, the several average
diameters may differ widely from one another.
● The total surface area of the particles is:
6𝑚 1.6 Number of particle in mixture
𝐴𝑤 = 𝑁𝑆𝑝 = ϕ𝑠 ρ𝑝 𝐷𝑝 The volume of any particle is proportional to its
“diameter” cubed.
1.4 Specific surface of mixture 3
𝑣𝑝 = 𝑎𝐷𝑝
● If the particle density ρ𝑝 and spericity Φ𝑠 are
a = volume shape factor
known, the surface area of particles in each
Assuming that a is independent of size, then:
fraction can be calculated and added to give
𝑁
the O
specific surface, 𝐴𝑤 (The total surface area 1 𝑥𝑖 1
𝑁𝑤 = ∑ =
O 𝑎ρ𝑝 3 3
of the unit mass of particle): 𝑖=1 𝐷𝑝𝑖 𝑎ρ𝑝𝐷𝑝𝑖
6𝑥1 6𝑥2 6𝑥𝑁 𝑁 𝑥𝑖
6
𝐴𝑤 = + +... + = ϕ𝑠 ρ𝑝
∑
ϕ𝑠 ρ𝑝𝐷𝑝1 ϕ𝑠 ρ𝑝𝐷𝑝2 ϕ𝑠 ρ𝑝𝐷𝑝𝑁 𝐷𝑝𝑖
𝑖=1
size.
n
Screening Operation
A wide range of industries, including mining and 1. Scalping
mineral processing, food, agricultural, chemical, Scalping is typically the first step in the screening
recycling, plastics, and pharmaceuticals, use the
aforementioned approach.
process, it is the process of removing bulkier0
components from the mixture. Scalping screeners
output various sizes of material using vibrating
Screening serves several purposes, including meshes. The material is dumped on top of the stacked
enhancing the coarse particles for further size tiers of meshes, or “”screens.”
reduction, eliminating the fine particles from the
crusher feed to prevent over-grinding, classifying the
crushed particle products into commercial sizes, and
carrying out a step in the concentration process.
Mechanism of Screening
The primary objective of screening is to allow
undersized particles to pass through the apertures
while rejecting oversized for a useful purpose. As a
result, the particles must be delivered to the screen
openings and presented there at a speed and angle
such that the passage of undersize particles is not
impeded by the openings’ edges or walls. Particles
Scalping Screens
approach the opening from a particular direction, with
a particular orientation, and at a particular speed that C
A scalping screens’ function is to pre-process material
for various purposes. As an illustration, gravel for
they are unable to pass, and as a result, many
landscaping purposes can call for stones that are no
undersize particles avoid the access of screen
longer than 2 inches and no smaller than 0.5 inches.
openings for a significant amount of time.
Any material that is either coarser or finer than these
sizes could be removed using scalping screen.
Stratification
0
The characteristics of particle orientation in the bed.
Important for the transport of large particles and the
Advantages
- Works well with bulky material mixed with fines
avoidance of blinding screen openings, excessive
- Limits with fast precision screening and small
movement reduces the effectiveness of the screen.
finished specs
- Application versatility
Separation Probability Quality checker Bigx;smalle
=
Coarse Screens
Coarse screens are usually called bar screens or
me
racks and are used where the wastewater contains
large quantities ofCcoarse solids that might disrupt
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Dewatering Screens
Dewatering Screens can be used to dewater -4 mesh
(5 mm) particles of sand, coal, iron ore, salt, etc., as
well as for limited efficiency fine sizing, washing and
rinsing, desliming and organics screening at or above
10 mesh (2 mm) to create differential products, for
stone washing and rinsing <2” (-50 mm) aggregates,
achieves dry products with moisture content 8-20%
Advantages
- Low noise, easy maintenance
- Stable structure with strong exciting force
- High screening efficiency and low noise
pollution
- Light weight, easy to disassemble and replace
- Stable structure and strong exciting force
Disadvantages
Advantages - High-wear process
- Extremely dry discharge - screens used to filter and separate are
- Low percent moisture continuously subjected to extremely harsh
- Shio material the same day or next day conditions.
- Low horsepower requirements
- Low maintenance and wear cost Applications:
- Very high capacity unit 1. Coal Industry
2. Ore Industry
Disadvantages 3. Mining Industry
- Limited in their ability to accommodate large 4. Metallurgy Industry
volumes of water
- Dewatered sand moisture content is typically (7) Various Types of Screening Equipments
half that of most other equipment options, Stationary Screens
typically 12 to 15 percent by weight, which Stationary Screens are made of punched metal plate
produces a drip-free sand product. or woven wire mesh, usually set at an angle with the
- All dewatering screens lose fines along with horizontal up to about 60 degrees. They are suitable
the water through the screen mesh. for intermittent small-scale operations, such as
ummmmm
screening sand, gravel, or coal by throwing the
Application for Dewatering material against the screen.
1. Mining Industry
2. Pulp paper Manufacturing
4. Desliming
Desliming means to
remove slime from
desliming of fine coal.
Generally, the aim of the
desliming step is to
minimize the feed fines
to avoid their negative
effects in the
downstream process.
- This provides the initial size separation for the Stationary Screens are typically used in series with a
large and fine coal circuits. primary screen facing the flow. A roving screen is
- Water is applied to the material as it passes placed downstream to capture debris when the
over the screen decking to assist the primary screen is fouled and requires cleaning.
un
separation process.
The disadvantages are inefficiency, blinding, difficult
to change the opening between the bars, separations
not effective, and in the case of coal screening,
breakage of oversize particles
Vibrating Screens
Vibrating Screens are used where large tonnages are
to be treated. The vibrating motion is imparted to the
screen surface by means of cams, eccentric shafts,
unbalanced flywheels, or electromagnetic means.
Grizzly
Grizzlies are widely used for screening large sizes,
particularly of 1 in and over. They consists simply of a
Mee
circular.
sand.
n
Oscillating Screens
Oscillating screens or gyratory screens are used in the
mee
They are suitable for separating lighter wet and dry Trommels are quite efficient for coarse sizes. The
recyclables and raw materials (wood chips, wood inclination of the trommel varies from about ¾ in. (wet
shavings, wood pellets, waste wood). screening) to 3 in./ ft of length, depending on the
nature of the material to be processed.
The Ocapacity of the trommel increases with increased services to follow up the screening process such as
speed of rotation up to a point where blinding occurs packaging or warehousing.
due to crowding of material through the screen. If the
speed of rotation is increased still further to the critical Advantage and Disadvantage of Wet Screening:
speed, the material no longer cascades over the Advantage
screen surface but is carried around by centrifugal - Consistent Travel Speed
force. - More clearance/access.
1.0 Xi...
-
totals re
NSA
Work Done
Arithmetic
mean-Eppic=087 =
0.045
ecos
Mass MeanDiameter 2 xi Dpi 1.678
=
=
an
poison=6.55
e Work Done -
specific power
input-work
bone-I=
Yin MFproductis
in
Mesh No. Ave. Particle surface MF Feed
Ratio
(Tyler) Diameter (Dpi) (Ni)
Xi x
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6 8 +
2.845 6.3 0.14 0.3100
-
8+
10 2,007 0.5336 Input
-
-
10 + 14 4.2
2
conv.
-
20 28 +
0.711 3.4 0.120.5738 0.23 1,0999
-
28 35 +
0.503 3.0.0.07 0.4175 0.28 1.6700 =
289932.8859 295K =
-
35 48 +
0.356 2.8 0.04 0.3146 0.15 1. 1798 Maintenance, over, replace cost
-
48 65 +
0.252 2.6
a
-
0.10 1,0317 :0.5(* 295k)
-
65 100
+
0.178 2.4 -
- 0.07 0.9438 =
147k
-
100 + 150 0.126 2.25
-
- 0.04 0.7143 purchase cost:#240K
epreciationcotta
kt
Total1,0 =
TOtal 1.0 =
I 7,737
=
(SA1)
I IN
surface Area Feed 35,749Cm 77.37cm
=
30k *473K
#
=
processed/yr:9 (24ay)(300)
-mig35tras.On
ore
the
64,800 ton/yr
=
SAp-SAF
=175.177-80.94
NSAC/S
(cm2/s)
I
qp.c
=
ringtorotationtonote
NSA2=
94.237m 235592.5cm2/sec
=
What is the theory behind Size Reduction? the coarse, medium and fine grinding of a wide
The energy requirement for particle size reduction is a range of materials.
function of input and output of particle size, hardness,
strength and other properties of solids. Varieties of Impact
1. Gravity Impact
Various theories for energy requirement are: Gravity impact, the free-falling material is
Rittinger;s Theory momentarily stopped by the stationary object.
&
The work required for size reduction is proportional to
the new surface area created
It is most often used when it is necessary to
separate two materials which have relatively
Kick’s Theory different friability. The more friable material is
0
Energy required to reduce a material in size was broken first, while the less friable material
directly proportional to the size-reduction ratio. remains unbroken.
Bond’s Theory
Works ⑦
⑲ required using a large-size feed is proportional
to the square root of the surface/volume of the
2. Dynamic Impact
Dynamic Impact, the material is unsupported
product. and the force of impact accelerates movement
of the reduced particles towards the breaker
Objectives of Size Reduction plate and/or other hammers.
- To produce smaller particles for smaller scale Dynamic impact is advantageous for size
- To optimize the feeding efficiency on certain reduction of many materials and it is specially
equipment needed when ·
the particle size. This method of size reduction are suitable for
reducing extremely hard and abrasive rock
Mechanism of Size Reduction
Size reduction is the process of conversion of bigger As a mechanical reduction method,
particles into smaller particles. Various size-reduction compression is chosen
equipment employ different actions to solid particles (i) If the material is hard and tough,
for size reduction, which is customer tailored. There (ii) If the material is abrasive
are four basic ways to reduce the size of a (iii) If the material is not sticky,
material-impact, compression, attrition and shear. (iv) Where the finished product is to be
Most of the size-reduction equipment employ a relatively coarser in size, and
combination of all these size reduction methods (v) When the material will break cubically
1. Impact ⑲
3.
4. Attrition
Particles are subjected to a single violent force Attrition is a method of size reduction by
and in crushing terminology, it refers to the rubbing or scrubbing the materials between
sharp, instantaneous collision of one moving two hard surfaces. Attrition consumes more--
object against another. Impact forces are power, it is preferred for crushing the less
=>
general-purpose forces that can be found in abrasive materials such as pure limestone
and coal.
Attrition crushin is most useful when employed for an intermediate duty are referred to as
(i) the material is friable or not too abrasive, -
grinders,
and A grinder is often charged with the product from a
(ii) a closed-circuit system is not desirable to crusher which it reduces to powder. The commercial
control the oversize grinders described in this section are hammer mills
and revolving mills.
N
4.
5. Shear The product from a crusher is often fed to grinder in
Shear consists of a trimming or cleaving which it is reduced to powder.
action rather than the rubbing action
Cutters
In some size reduction problems, the feedstock is too
tenacious or too resilient to be broken by
compression, impact, or attrition, In other problems
Primary and Secondary Size Reduction feed must be reduced to particles of fixed dimensions.
Crushers
Crushers do the heavy work of breaking large pieces These requirements are met by the devices that cut,
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of solids into smaller lumps. Primary crushers are chop, or tear the material into desired characteristics.
run on materials out of mine, the size of which may
reach more than one meter and breaking it into Rotary knife cutters and granulators are considered as
150-300 mm (6-10 in) lumps. cutting machines.
A secondary crusher reduces those lumps to particles
in the size range of 5-10 mm. These are used in the manufacture of rubber,
Crushers are slow-speed machines employed for the plastics, and recycling of paper and pulp.
coarse reduction of large quantities of solids. The
different types of crushers are operated by In agricultural industry, cutting machines are mainly
compression and can break large pumps of hard used to cut fruits and vegetables.
materials. They find application in rockery and mining
industries. Cutters are size-reduction machines which give
A. Crushers (Coarse and Fine) particles of definite size and shape, usually 2 to 10
1. Jaw Crusher mm in length. A cutting action is the characteristics of
2. Gyratory Crusher knife cutters, dicers and slitters.
3. Crushing Rolls
Size Reduction Equipment
Jaw Crusher
Jaw crushers consist of two crushing faces (jaws) one
of them is fixed vertically to the frame, while the other
one is movable, which is either pivoted at the top or
bottom.
Division:
Coarse Crushers (Large feed size to 50-5 cm product
size)
Application:
- Metallurgical Industries
- Mining Industries
- Construction
- Railways Crushing Rolls
Although roll crushers have been around for more
than 200 years, they have recently lost ground to jaw
and gyratory crushers in terms of popularity due to
their poor wear characteristics with hard rocs.
Depending on how many rolls are utilized, there are
two different types of roll crushers. The two primary
types of crushers are single-roll and double-roll
· crushers.
Gyratory Crushers
Gyratory crushers were created more recently in order Single Roll Crusher
O
to outperform jaw crushers in terms of capacity.
Gyratory crushers use a similar crushing mechanism
Mechanism Used:
Single-roll crushers employ three different methods of
to jaw crushers in that the bottom of the machine size reduction - impact, shear and compression
Division:
Coarse Crushers (Large feed size to 50-5mm)
Application:
● Crushing Petroleum Coke
● ROM feed Crushing Roll
● Mining Industry Capacity:
The theoretical capacity of a crushing roll Q in kg/h is
given by:
Attrition Mills
Operating Principles
Attrition mills use the hammer mill principle to a
certain extent: e.e., shattering by/impact. However,
Roller Mill C
they also impart a shearing and cutting action
Operating Principle:
Roller Mills use the process of stress and attrition in Construction and Working:
milling of solids in suspensions, pastes or ointments A statistically and dynamically balanced runner head
and some solid materials. assembly, precise machining and alignment of the
discs, and constant spring pressure combine to
Construction: maximize uniformity of the reduced material. The
Roller mill is a form of compression mill that uses a replaceable milling plates are offered in several
single, double, or triple cylindrical heavy wheel patterns to optimize size reduction for specific types of
mounted horizontally and rotated about their long axis materials.
·
Disc Mills
It is a type of crusher that can be used to grind, cut
shear, shred, fiberize, pulverize, granulate, crack , rub,
curl, fluff, twist, hull, blend, or refine, It works in a
similar manner to the ancient Buhrstone mill in that the
feedstock is fed between opposing discs or plates.
The discs may be grooved, serrated or spiked.
Pin/Rod/Ball Grinders
Operating Principle: Ball Grinders or ball mills consist of a hollow
C
Disc mill is the type of attrition in which two surfaces cylindrical or conical shell, made of steel, with
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rotates past each other at high speed with close approximately half-full2
of steel balls, rotating about its
tolerance axis, either horizontal or at a small angle to the
horizontal. The grinding media is the balls, which may
Construction: be made of steel or stainless steel.
At this part of the disc mill, the material to be grinded
is inserted into the machine. It has a specific size and Operating Principle:
feed should be processed at least through the primary The principle of size reduction in ball mills is impact of
crushers. balls, which fall from the top of the shell on the feed
particles near the bottom of the shell.
Grinding Disc
A disc mill consists of two saucer shaped discs with Construction:
their surface having specially shaped grooves the Ball Grinders or ball mills consists of hollow cylindrical
depth of which is reduced towards the circumference. or conical shell, made of steel or rubber-lined steel,
The discs are face to face mounted vertically or with approximately half-full of steel balls, rotating
horizontally and revolve at the different speeds and in about its axis, either horizontal or at a small angle to
the opposite directions. In most designs one of the the horizontal. The grinding media is the balls, which
discs is driven while the other is not. Also, one of the may be made of steel or stainless steel. THe h material
A
discs is rather strongly fixed while the other flutters or to be ground may be fed in through an opening at one
gyrates during revolving.Like other crushing end and the product leaves through a similar opening
machines, a disc mill has not of the discs spring at the other end, which is covered with a coarse
loaded through a screw mechanism that helps in screen to prevent the escape of balls.
adjusting the set and provides safety against
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Mechanical Efficiency
Mechanical efficiency (nm), is defined as the ratio of
energy absorbed and the energy fed to the machine.
In another way, this may be defined as the ratio of the
energy absorbed by the solid to form heat and the
energy input to the machine.