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Sys Master - Pdfs - h03 - H5e - 10133532180510 - COA - DRE GS09010494 - ST WB CERT 2972235 1 1 1

This document provides a certificate for a certified reference material (CRM) for cyclopentane. The CRM has a certified concentration of 96.4 wt% cyclopentane with an expanded uncertainty of 4.8 wt%. The document details the production, certification, intended use, safety, and traceability of the CRM.

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0% found this document useful (0 votes)
30 views2 pages

Sys Master - Pdfs - h03 - H5e - 10133532180510 - COA - DRE GS09010494 - ST WB CERT 2972235 1 1 1

This document provides a certificate for a certified reference material (CRM) for cyclopentane. The CRM has a certified concentration of 96.4 wt% cyclopentane with an expanded uncertainty of 4.8 wt%. The document details the production, certification, intended use, safety, and traceability of the CRM.

Uploaded by

Verilisima
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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REFERENCE MATERIAL CERTIFICATE ISO 17034

Certified Reference Material


This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This certified reference material
(CRM) was designed, produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered
quality management system ISO 9001.

Product Name
D5191 Vapor Pressure - 68.3kPa (9.91 psi)

Product Code Lot Number


DRE-GS09010494 2-H367597NA
CAS No. Format
287-92-3 Solution
Mol. Weight Expiry
70.14 21 Feb 2021
Mol. Formula Storage
C5H10 Ambient (15-25 ºC)

Concentration Expanded Uncertainty (U)


96.4 Wt % 4.8 Wt %

Uncertainty
The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95%
confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of
preparation, purity of neat materials, homogeneity, long-term stability testing, and transportation stability.

The producer certifies that this reference material meets the specification stated in this certificate until the
expiry date, provided it is stored unopened at the recommended temperature herein. Product warranties for
this reference material are set out in the terms and conditions of purchase.

CERTIFIED BY CERTIFIED ON
RM Release
HuiChen Stavros, Ph.D. 27 Feb 2019

Version 1 Page 1 of 2
REFERENCE MATERIAL CERTIFICATE ISO 17034
Instrument
GC/FID
Detection
FID
Column
CHRO MATO GRAM

Phenomenex ZB-1HT 30m x 0.25


mm, ID 0.25 um
Method Details
Rate Temp.(C) Hold time (min)
45.0 2.0
10.0 150.0 0.0
25.0 345.0 2.0
Inj.-Vol
1 µl
Flow
1 ml/min

Method of Preparation
The certified value is based on gravimetric and volumetric preparation of this CRM. This CRM has been
confirmed by the appropriate analytical techniques.
Batch Information
Solvent: Cyclopentane, Lot no. a0390016, 250 mL
Gravimetric Data
Weight Chemical
Compound Name Lot No.
(mg) Purity

Cyclopentane 250000.
2386.9.1P 96.4
00

Intended Use the balances is verified daily Instructions for use


This CRM is intended for use in a internally and annually by an The CRM should be used shortly after
laboratory as a calibration and quality external accredited calibration opening to avoid concentration
control standard or in method service. Chromatographic methods changes due to evaporation. It is
development for analytical are traceable to the International recommended to use 1 µL as the
techniques. System of Units (SI). minimum sample size. If storage after
opening is necessary, it should be
Safety Homogeneity transferred to an amber vial with
Proper precautions should be Random replicate samples of the minimum head space and a Teflon-
observed while handling. See Safety final packaged CRM have been lined silicon septum. If handled as
Data Sheet. analysed to prove homogeneity recommended, use period after
compliant with ISO 17034. opening is a maximum of 2000 days
Traceability for an estimated 5% drift in
The balances used for gravimetric Storage concentration as a result of analyte
measurements are calibrated with The CRM should be stored in the and/or solvent transpiration. Visit the
weights traceable to the national original sealed container at the support section of our website
standards (NIST). The calibration of indicated temperature. lgcstandards.com for a series of Dr.
Ehrenstorfer Tech Tip videos and
frequently asked questions.

The producer of this reference


7290-B Investment Drive material is registered to ISO 9001:2015
North Charleston, SC 29418 under IZ391-IS4 by NSF-ISR and accredited
United States to ISO 17025:2005 and ISO 17034:2016
T | +1 843 763 4884 by A2LA with the accreditation numbers ISO 17034 Accredited
F | +1 866 509 5146 3031.01 and 3031.02. Reference Material Producer
E | [email protected] Cert. No. 3031.02

Version 1 Page 2 of 2

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