An Internet-of-Things Enabled Smart Sensing System For Nitrate Monitoring
An Internet-of-Things Enabled Smart Sensing System For Nitrate Monitoring
Abstract—Monitoring the nitrate concentration in the field is a routine manner. This is done by expert staff at regular inter-
an excellent ability for a water-monitoring study. We report an vals to track the change of nitrate concentration [10]. However,
interdigital FR4-based capacitive sensor, which is characterized data taken too seldom may not be adequate to measure the
for nitrate concentration. The concentration range of nitrate is
0–40 ppm (mg/L). Different unknown samples were measured actual nitrate profile.
and validated with standard UV-Spectrometry. A smart sensing There are conventional standard methods available for
node has been developed which can collect water from a lake, nitrate measurement, such as UV/V is spectrometry, chro-
stream, or river, measure the instantaneous nitrate concentration, matography, HPLC, and capillary electrophoresis. They are
and transfer the data through the gateway to a user-defined unsuitable for creating a large-scale wireless sensor net-
cloud server. The system is completely autonomous and solar
powered, robust, and trialed in the field successfully. A simple work (WSN) due to their massive instrumentation, bulky fea-
moving-average algorithm is used to smooth the collected data in tures, and complex and sensitive measurement procedure; and
the cloud side. The LoRa protocol and WiFi protocol are com- above all they are costly. They also produce lots of chemical
pared in terms of power consumption. The proposed system is waste which might be harmful to the environment [11].
trialed in the field continuously and the result validated with A WSN consists of a number of dedicated sensor nodes
standard UV-Spectrometry. The developed smart system can be
easily deployable and friendly to use, and offers new possibilities with physical sensing and computing abilities, which can sense
for both spatial and temporal analysis for nitrate concentration. and monitor the surrounding physical parameters. A WSN has
a lot of essential characteristics and a few constraints, such
Index Terms—Interdigital sensor, Internet of Things (IoT), as limited energy and computational power. During the last
LoRa protocol, nitrate concentration, sensing node, water mon- decades, WSNs have been widely used in different applica-
itoring, WiFi protocol, wireless sensor network (WSN). tions related to water monitoring [12]–[14], forests [15], [16],
industrial [17], [18], and agricultural [19]–[22]. Some
researches were reported [23]–[25] to monitor the nitrate con-
I. I NTRODUCTION
centration through the WSN network [26]. Their limitation
ITROGEN is an important nutrient for plants and is
N contained in the building blocks of life, such as in
nucleotides, amino acids, and proteins [1]. The excessive use
was that most of them are laboratory-based and perform the
real-time analysis in the laboratory only. Capella et al. [24]
reported in-line analysis of nitrate concentration in river water
of fertilizers, urination due to animal farming, and indus- and emphasized the feasibility of development of WSNs-based
trial waste are the significant reasons for nitrate leaching in continuous monitoring.
water [2]–[7]. Excessive nitrate can hamper aquatic life and The Internet of Things (IoT) enables any physical objects
can lead to algal blooms and eutrophication [8]. According to communicate through the Internet and transfer data to
to the U.S. Environmental Protection Agency, the maximum a specific server for further processing. It requires pervasive
allowable nitrate concentration in drinking water should be computing, smart sensors, embedded devices, communication
44.2 ppm. Over this range of concentration it would be technologies, Internet protocols, and applications. IoT-enabled
considered as contaminated water [9]. WSNs help to connect more objects for monitoring purposes
The concentration of nitrate fluctuates in water, both spa- to build up smart cities, smart industries, smart agriculture,
tially and temporally. It also depends on the season, weather etc.
conditions, and the rainfall of any location. Currently, the In this paper, a low-cost interdigital FR4-based capacitive
regional council or local government collects water samples in sensor is proposed for nitrate measurement. The developed
sensor has been characterized and calibrated against standards
Manuscript received November 15, 2017; revised December 22, 2017
and February 3, 2018; accepted February 20, 2018. Date of publication to measure nitrate components. The measured results are val-
February 27, 2018; date of current version January 16, 2019. (Corresponding idated against the standard UV-spectrometry method. A smart
author: Md. Eshrat E. Alahi.) sensing node has been developed which is suitable for an IoT-
Md. E. E. Alahi, N. Pereira-Ishak, and S. C. Mukhopadhyay are with
the School of Engineering, Macquarie University, Sydney, NSW 2109, enabled WSN. The sensing node collects water from stream
Australia (e-mail: [email protected]; [email protected]; or lake and measures the nitrate concentration. The collected
[email protected]). water can be discharged automatically to stream or lake again.
L. Burkitt is with the School of Agriculture, Massey University, Wellington,
New Zealand (e-mail: [email protected]). A solar panel is used for energy harvesting and provides the
Digital Object Identifier 10.1109/JIOT.2018.2809669 system with the necessary energy for monitoring continuously.
2327-4662 c 2018 IEEE. Personal use is permitted, but republication/redistribution requires IEEE permission.
See http://www.ieee.org/publications_standards/publications/rights/index.html for more information.
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ALAHI et al.: IoT ENABLED SMART SENSING SYSTEM FOR NITRATE MONITORING 4411
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4412 IEEE INTERNET OF THINGS JOURNAL, VOL. 5, NO. 6, DECEMBER 2018
B. System Description
Fig. 7. Different parts of the proposed system.
A smart sensing system is proposed to carry out the in-
line nitrate analysis as per Fig. 5. Fig. 6 shows the circuit
diagram of the developed system. Arduino Uno and Arduino gateway is also responsible to send the data to the cloud server.
Uno WiFi [35] was used as the main microcontroller. An Thingspeak is used as an IoT-based cloud server, which is free
AD5933 [36] is used to get the impedance data from the sen- to use and can easily store data.
sor. The impedance analyzer gets the impedance and the phase WiFi and LoRa, both communication protocols, were used
shift of the sensor. The impedance analyzer has the ability to to examine the durability of the sensor nodes. The Arduino
sweep the frequency, which is not required in the current appli- Uno WiFi has a WiFi module, which is responsible for trans-
cation. The operating frequency is fixed and each measurement mitting and receiving data through the gateway. An LG01S is
is done five times. Only the average nitrate concentration is also used as a WiFi gateway. All the microcontrollers, sensor,
sent to the IoT cloud server. inlet and outlet pumps, rechargeable battery, solar charge con-
A Dragino LoRa shield is used as a long-range transceiver troller, and water reservoir are contained in a steel box which
to communicate with the gateway. It allows sending data and is robust and easy to install. Fig. 7 indicates the materials
reaching an extremely long range with low data rates. It is which are used in the sensing node. Fig. 8 shows the inside
based on the RFM95W/RFM98W [37] and used for 915-MHz of the steel box.
transmission/reception. An L298N [38] is used as a motor
driver to control the inlet and outlet pumps. The inlet pump
brings the water into the reservoir and the outlet pump empties C. Energy-Harvesting Technique
the reservoir after the measurement. A solar panel (model: ZM-9051), solar charge controller
LG01S [39] is used as the LoRa/WiFi gateway to commu- (MP-3750), and a sealed rechargeable battery (12 V, 12 AH)
nicate between the sensing node and the cloud server. The were used to provide energy continuously without any human
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ALAHI et al.: IoT ENABLED SMART SENSING SYSTEM FOR NITRATE MONITORING 4413
Fig. 10. Study location and distance between gateway and the sensor node.
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4414 IEEE INTERNET OF THINGS JOURNAL, VOL. 5, NO. 6, DECEMBER 2018
TABLE I
U NKNOWN S AMPLE M EASUREMENT C OMPARED TO
L ABORATORY S TANDARD M ETHOD
Fig. 12. Frequency versus real impedance for different nitrate concentrations.
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ALAHI et al.: IoT ENABLED SMART SENSING SYSTEM FOR NITRATE MONITORING 4415
TABLE II
AVERAGE N ITRATE C ONCENTRATION OF THE S TUDY L OCATION
C OMPARED W ITH L ABORATORY S TANDARD M ETHOD
In addition, the collected data have been smoothed with a sim- LoRa enabled microcontroller. Therefore, a LoRa enabled
ple moving-average algorithm. The smoothed data can provide sensing system was used to do the necessary field trial.
the trend of nitrate concentration, which might be useful over
a longer time. The creek does not carry a high level of nitrate
concentration as it is located inside the University and the V. C ONCLUSION
administration of the University control all kind of pollution An IoT-enabled smart nitrate sensor and sensing system is
(air, water, and environment) very carefully. proposed to monitor the nitrate concentration in real-time. An
FR4-based interdigital sensor is characterized and is extremely
useful for robust use during nitrate monitoring. The system
E. LoRa Protocol Over WiFi Protocol is autonomous and was trialed in the field for seven days
Components for remote IoT applications must draw as little without any interruption. The LoRa protocol was used to run
power as possible to maximize battery life. The difference of the system over longer periods than for the WiFi protocol.
The LoRa protocol over the WiFi RF protocol was to reduce The LoRa protocol is a low-power energy-saving protocol,
overall power consumption during sleep mode to less than half. which was implemented successfully. The system’s collected
It also allows transmissions to penetrate obstacles and allows data were also validated through the UV-spectrometry method.
the data to travel larger distances whilst consuming less power The collected data shows that few data have been lost dur-
than the standard WiFi protocol. It optimizes the data exchange ing transmission, and 98% of data are successfully collected
with the gateway, allowing for lower power consumption as through the gateway to the cloud server. The results show
compared to WiFi. The current drain from each component that the proposed smart sensing system can be very useful to
for each stage, comparing WiFi and LoRa, can be observed develop a WSN to monitor nitrate concentration in real time.
in Table III. It is observed that the LoRa protocol is consum- It also shows that, without human interaction, changes of both
ing less current, which helped to harvesting the energy for temporal and spatial evolutions of nitrate concentration can be
longer time. The consumption of energy for pumps and motor monitored successfully.
drivers are similar for both the system. However, WiFi enabled The future work would be to use more sensing nodes to
microcontroller consumes 2.22 times more energy than the create a WSN. The data would be collected for a longer time to
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4416 IEEE INTERNET OF THINGS JOURNAL, VOL. 5, NO. 6, DECEMBER 2018
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and availability evaluation of wireless sensor networks for industrial Bangladesh. He received the B.Sc. degree in electri-
applications,” Sensors, vol. 12, no. 1, pp. 806–838, 2012. cal engineering from the Military Institute of Science
[18] G. Zhao, “Wireless sensor networks for industrial process monitor- and Technology, Dhaka, in 2007, and the M.Sc.
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pp. 46–63, 2011. from the University of Bremen, Bremen, Germany,
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no. 2, pp. 120–132, 2008. Sydney, NSW, Australia.
[20] X. Li, Y. Deng, and L. Ding, “Study on precision agriculture monitoring His current research interests include smart sens-
framework based on WSN,” in Proc. 2nd Int. Conf. Anti Counterfeiting ing systems, Internet of Things, and embedded
Security Identification (ASID), Guiyang, China, 2008, pp. 182–185. systems.
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ALAHI et al.: IoT ENABLED SMART SENSING SYSTEM FOR NITRATE MONITORING 4417
Najid Pereira-Ishak was born in Sydney, NSW, Lucy Burkitt was born in Melbourne, Australia. She
Australia. He has recently completed his final year received the Bachelor of Agricultural Science degree
of study as an undergraduate student with Macquarie and the Ph.D. degree in soil science from LaTrobe
University, Syndney, graduating with a Bachelor of University, Melbourne, VIC, Australia, in 1998 and
Engineering (with Honours) in mechatronics. 2003, respectively.
He is currently with CSIRO, as a Research She was a Researcher with the University of
Assistant with the Department of Agriculture and Tasmania, Hobart, TAS, Australia, for ten years,
Food. He has interests in Internet of Things (IoT) specializing in soil nutrient management and nutri-
systems, smart systems applications, data acquisi- ent loss. She is currently a Senior Researcher with
tion, and data analysis. Massey University, Wellington, New Zealand, spe-
cializing in reducing the impacts of agriculture on
water quality and high frequency water quality monitoring.
Dr. Burkitt was an Editor of the joint Australian and New Zealand Society of
Soil Science Conference Proceedings in 2012, and a member of the Organizing
Committee for this conference in 2012 and 2016.
Subhas Chandra Mukhopadhyay (A’97–M’99–
SM’02–F’11) received the B.E.E. (gold medalist),
M.E.E., Ph.D., and the Doctor of Engineering
degrees.
He is currently a Professor of mechanical/
electronics engineering with Macquarie University,
Sydney, NSW, Australia, and the Discipline
Leader of the Mechatronics Engineering Degree
Programme. Before joining Macquarie University,
he was a Professor of sensing technology with
Massey University, Wellington, New Zealand. He
has over 26 years of teaching, industrial, and research experience. He has
supervised over 40 postgraduate students and over 100 honors students. He
has examined over 50 postgraduate theses. He has authored or co-authored
over 400 papers in different international journals and conference proceedings,
written 6 books and 36 book chapters, and edited 15 conference proceedings.
He has also edited 25 books with Springer-Verlag and 17 journal special
issues. He has delivered 292 presentations including keynote, invited, tutorial
and special lectures. His current research interests include smart sensors and
sensing technology, instrumentation techniques, wireless sensors and network,
Internet of Things, numerical field calculation, and electromagnetics.
Dr. Mukhopadhyay is a Topical Editor of the IEEE S ENSORS J OURNAL,
and an Associate Editor of the IEEE T RANSACTIONS ON I NSTRUMENTATION
AND M EASUREMENTS . He is a Distinguished Lecturer of the IEEE Sensors
Council from 2017 to 2019. He chairs the IEEE IMS Technical Committee
18 on Environmental Measurements. He has organized over 20 international
conferences as either the General Chair/Co-Chair or the Technical Programme
Chair. He is a Fellow of IET, U.K. and IETE, India.
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