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IISER Pune - Course Content: Coordinator and Dr. Moumita Majumdar

The course Advanced Inorganic Chemistry Laboratory is offered in the 6th, 8th, and 32nd semesters at IISER Pune in January 2024. It is a 3-credit lab course coordinated by Dr. Moumita Majumdar and Dr. Nirmalya Ballav. The course aims to provide an overview of common experimental characterization techniques and basic inorganic chemistry knowledge. Students will develop the ability to correlate chemical and physical properties of elements and compounds, and establish the link between theory and practice through laboratory experiments. The course involves experiments in spectrochemical analysis, stoichiometry determination, redox titration, polymer synthesis, phosphorescence observation, NMR analysis, salt preparation, analysis by IR spectroscopy

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53 views2 pages

IISER Pune - Course Content: Coordinator and Dr. Moumita Majumdar

The course Advanced Inorganic Chemistry Laboratory is offered in the 6th, 8th, and 32nd semesters at IISER Pune in January 2024. It is a 3-credit lab course coordinated by Dr. Moumita Majumdar and Dr. Nirmalya Ballav. The course aims to provide an overview of common experimental characterization techniques and basic inorganic chemistry knowledge. Students will develop the ability to correlate chemical and physical properties of elements and compounds, and establish the link between theory and practice through laboratory experiments. The course involves experiments in spectrochemical analysis, stoichiometry determination, redox titration, polymer synthesis, phosphorescence observation, NMR analysis, salt preparation, analysis by IR spectroscopy

Uploaded by

kk singh
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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IISER Pune - Course Content

Semester JAN 2024


Open to Semester 6,8,32
Course Code CH3253
Course title Advanced Inorganic Chemistry Laboratory
Nature of Course LB - Lab
Credit 3
Coordinator and Dr. Moumita Majumdar
participating faculty (if any) Dr. Nirmalya Ballav
Pre-requisites CH1223 - General Chemistry Practicals I
Objectives The course aims to provide an overview of the most
common experimental characterization and basic
knowledge in inorganic chemistry. It is designed to help
students develop the ability to correlate the chemical and
physical properties of elements and their compounds and to
establish the link
between theory and laboratory practice by conducting
laboratory experiments. Students will acquire expertise in
chemistry laboratory in handling of reagents and solvents
as well as in analytical techniques.
Course content 1. Spectrochemical analysis of a coordination complex (1)
2. Determination of the stoichiometry of a coordination
compound by Job’s method of continuous variations (1)
3. Determination of Iron by reaction with Permanganate -A
Redox Titration (1)
4. Preparation of ‘bouncing putty’ a silicone polymer with
unusual properties (1)
5. Synthesis and observation of phosphorescent emission
of
Tris(2,2’bipyridine) ruthenium- (II) dichloride hexahydrate
(1)
6. Synthesis of SnI4 and analysis by Sn119 NMR (1)
7. Preparation of Copper (I) Chloride (1)
8. The preparation of Potassium
tris(oxalato)ferrate(III)trihydrate and analysis by IR
spectroscopy (1)
9. Determination of Chloride by Mohr’s Method:
Precipitation titration (1)
10. Solvent Extraction: Determination of copper as the
‘neocuproin’
complex (1)
Evaluation / Assessment End-Sem Examination-NA%
Mid-Sem Examination-NA%

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IISER Pune - Course Content

Others-Lab records- 50%


Lab conduct/group work/ safety instructions etc - 10%
Quiz/Viva/Experiments- 40%
Suggested readings Lab manual and necessary study materials will be provided
When Next January 2024
Date Uploaded 2023-10-26 20:32:50

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