ANALYTICAL REPORT No: 0876-LQ-14

Client SIBUR International GmbH

S-Peterburg № 7652-0488-14/7
Date of report 11.09.2014
Object Production Plant Sibur-Kstovo
Location Kstovo
Product : Heavy pyrolysis resin 1 Received On: 02.09.2014
Sample Drawn : Sample is selected and provided customer representative.
Sample Description : Dark-colored product which is liquid at room temperature
Testing Performed By: Intertek S-Petersburg Laboratory Date: 04÷11.09.2014
Specification Result Within
Tests Units Method2 Result Specification?
limits
Density at 15 deg C kg/l ASTM D 4052 unknown 1.0656 _
Density at 20 deg C kg/l ASTM D 4052 unknown 1.0621 _
2
Kinematic Viscosity at 50ºC mm /s ASTM D 445 unknown 15.73 _
Viscosity assumed (Engler) at 50ºC ºE conversion unknown 2.40 _
2
Kinematic Viscosity at 100ºC mm /s ASTM D 445 unknown 3.886 _
Viscosity assumed (Engler) at 100ºC ºE conversion unknown 1.30 _
Sulphur content %mass ASTM D 4294 unknown 0.1095 _
Flash Point, closed Cup ºC ISO 2719(A) unknown 23.0 _
Water content %mass ASTM D 95 unknown 0.10 _
Pour Point (upper) ºC ASTM D 97 unknown minus 24 _
Total Nitrogen %mass ASTM D 3228 unknown 0.022 _
3
Aniline Point (mixed) ºC ASTM D 611 (A) unknown 23.5 _
Conradson carbon Residue (CCR) %mass ASTM D 189 unknown 10.9 _
Vacuum Distillation (50 - 30 mm Hg): ASTM D 1160
Initial bolling point ºC mod. unknown 192 _
5% vol recovered ºC unknown 220 _
10% vol recovered ºC unknown 226 _
20% vol recovered ºC unknown 233 _
30% vol recovered ºC unknown 243 _
40% vol recovered ºC unknown 256 _
50% vol recovered ºC unknown 279 _
60% vol recovered ºC unknown 313 _
70% vol recovered ºC unknown 356 _
80% vol recovered ºC unknown 423 _
90% vol recovered ºC unknown 465 _
95% vol recovered ºC unknown 486 _
Final Boiling Point /cracking ºC unknown 486 _
Loss %vol unknown 0.0 _
Residue %vol unknown 5.0 _
ASTM D 1160
Recovered at 360 ºC % vol unknown 72 _
mod.
Bromine number(cut 360 ºC) gBr/100g ASTM D 1159 unknown 52.7 _
Saturated, aromatic and polar
IP 469
compounds
Saturated hydrocarbons %mass Less 5.0 _
Aromatics hydrocarbons %mass 38.4 _
more 29.0
Polar compounds I %mass _
(454.3)
Polar compounds II5 %mass 7.3 _

Intertek St.Petersburg.
21,Rozenshteina,St.Petersburg,Russia
tel(7-812) 363 12 00; (7-812) 930 17 52
 2 Specification Result Within
Tests Units Method Result Specification?
limits

Toluene equivalent % vol EXXON 79-004 unknown 100 (not passes) _

Toluene equivalent % vol EXXON 79-004 unknown 63 _

Toluene Insolubles %mass (paragraph 6.2) unknown 0.08 _

Xylene equivalent BP 230 unknown 100 (not passes) _

P-value SMS 1600 unknown 1.7 _

Hot Filtration potential % (m/m) IP 390(A)/IP 375 unknown 0.07 _
Metals:
Vanadium mg/kg IP 470 unknown 2 _
Sodium mg/kg IP 470 unknown 5 _
Nickel mg/kg IP 470 unknown 1 _
4
Aluminium mg/kg IP 470 unknown less 5 ( 0.4) _
4
Silicon mg/kg IP 470 unknown less 10 ( 6) _
Iron mg/kg IP 470 unknown 5 _
4
Zinc mg/kg IP 470 unknown less 1( 0.2) _
Calcium mg/kg IP 470 unknown 3 _
Colour ASTM (dilution) ASTM D 1500 unknown D 8 ASTM Color _
Asphaltenes %mass IP 143 unknown 6.3 _

Note 1 This product is not included in the Scope of accreditation laboratory.

Note 2. All these methods are intended to record for analysis of residual oil. Sample testing is proposed for
petrochemicals. Thus, the results can not be interpreted as the results obtained in the framework of the above methods.
Terms perform some tests had to pick from the properties of the product.
Note 3. The result is difficult to accurately fix. This value is taken as the average value between 22.5 - 24.5 degrees C..
Note 4.Actual values
Note 5.This class of compounds is similar but not identical to, asphaltenes insoluble in heptane as defined in IP 143.

LABORATORY MANAGER: P.Obukhova

This Analytical Report applies only to the samples tested.

This Analytical Report may not be partially or fully copied or reprinted without the permission of Intertek Testing Laboratory St. Petersburg

Intertek St.Petersburg.
21,Rozenshteina,St.Petersburg,Russia
tel(7-812) 363 12 00; (7-812) 930 17 52