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CHM Lab.5 Student Report

This document appears to be a lab report for a qualitative analysis chemistry experiment. It provides instructions for using various reagents like sodium hydroxide, dilute ammonia, sodium iodide, barium chloride, and silver nitrate solutions to observe reactions and identify metal cations and anions present in an unknown sample. The student is asked to record their observations of color changes or precipitate formations and provide the corresponding ionic equations to show the reactions taking place for various metal and non-metal ions. They will then test an unknown sample X with these same reagents and record their observations and inferences to identify what ions may be present in the unknown.

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Nikoli Major
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80 views

CHM Lab.5 Student Report

This document appears to be a lab report for a qualitative analysis chemistry experiment. It provides instructions for using various reagents like sodium hydroxide, dilute ammonia, sodium iodide, barium chloride, and silver nitrate solutions to observe reactions and identify metal cations and anions present in an unknown sample. The student is asked to record their observations of color changes or precipitate formations and provide the corresponding ionic equations to show the reactions taking place for various metal and non-metal ions. They will then test an unknown sample X with these same reagents and record their observations and inferences to identify what ions may be present in the unknown.

Uploaded by

Nikoli Major
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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______________________________________________ ____________________________

SURNAME, First Name(s) USI


CHM 1207 Lab #5 – Qualitative Analysis
https://www.youtube.com/watch?v=NFTBOIvTLtI

Sodium Hydroxide Solution, NaOH


Metal Cation Observation (must include ionic equation that represents the observed
reaction)
Ca2+
Zn2+
Pb2+
Cu2+
Cr3+
Fe2+
Fe3+

Dilute Ammonia Solution, NH3


Metal Cation Observation (must include ionic equation that represents the observed
reaction for the ions in bold)

Ca2+
Zn2+
Pb2+
Cu2+
Cr3+
Fe2+
Fe3+

For the cations that could not be differentiated by either of the above tests; add 1mL of
each to a separate clean test tubes followed by an equal amount of sodium iodide.
Observations: (Include an ionic equation for your observation)

Fig. 7.1 Reaction of cations with sodium iodide solution


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1
Barium Chloride Solution, BaCl2
Anion Reaction With BaCl2 Solubility in HCl
(ionic equations for insoluble compounds)
CO32-

SO32-

SO42-

Silver Nitrate Solution, AgNO3


Anion Reaction With AgNO3 Solubility in NH3 Solubility in HCl
(ionic equations for observed
reactions)
Cl-

Br-

I-

SO32-

CO32-

Unknown X:

Fig 7.2 Reaction on Unknown X with, from left to right, barium choride solution, acidified
silver nitrate solution, aqueous ammonia and potassium hydroxide solution.

TEST OBSERVATION INFERENCE


Sodium hydroxide

2
solution was added
dropwise then in excess
to 1mL of X
Aqueous ammonia
solution was added
dropwise then in excess
to 1mL of X
Acidified silver nitrate
solution was added to
1mL of X followed by
ammonia
Barium Chloride solution
was added to 1mL of X
followed by dilute HCl

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