Process Analytical Instruments
Process Analytical Instruments
Catalog Edition
PA 01 2015
© Siemens AG 2014
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© Siemens AG 2014
Supersedes:
Catalog PA 01 · 2014
Refer to the Industry Mall for current updates of Analytical Application Sets
4
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© Siemens AG 2014
Appendix
6
2 Siemens PA 01 · 2015
© Siemens AG 2014
The Siemens Industry Sector is the We consistently rely on integrated tech- Market launch times can be reduced
world's leading supplier of innovative nologies and, thanks to our bundled by up to 50% due to the combination
and environmentally friendly products portfolio, we can respond more quickly of powerful automation technology
and solutions for industrial companies. and flexibly to our customers' wishes. and industrial software from Siemens
End-to-end automation technology and With our globally unmatched range of Industry. At the same time, the costs for
industrial software, solid market exper- automation technology, industrial energy or waste water for a manufac-
tise, and technology-based services are control and drive technology as well turing company can be reduced signifi-
the levers we use to increase our cus- as industrial software, we equip compa- cantly. In this way, we increase our
tomers’ productivity, efficiency and nies with exactly what they need over customers’ competitive strength and
flexibility. With a global workforce of their entire value chain – from product make an important contribution to envi-
more than 100 000 employees, design and development to production, ronmental protection with our energy-
the Industry Sector comprises the sales and service. Our industrial custom- efficient products and solutions.
Industry Automation, Drive Technolo- ers benefit from our comprehensive
gies, and Customer Services divisions, portfolio, which is tailored to their
as well as the Metals Technologies market and their needs.
Business Unit.
Siemens PA 01 · 2015 3
© Siemens AG 2014
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Efficient engineering is the first step toward better production that is faster,
more flexible, and more intelligent. With all components interacting efficiently,
Totally Integrated Automation (TIA) delivers enormous time savings right from
the engineering phase. The result is lower costs, faster time-to-market, and
greater flexibility.
4 Siemens PA 01 · 2015
© Siemens AG 2014
• Integrated engineering
Consistent, comprehensive engineering throughout the
entire product development and production process
• Industrial data management
Access to all important data occurring in productive
operation – along the entire value chain and across
all levels
352),1(7 • Industrial communication
,QGXVWULDO(WKHUQHW
Integrated communication based on international
352),%86
cross-vendor standards that are mutually compatible
$6,QWHUIDFH
• Industrial security
.1;*$00$LQVWDEXV
Systematic minimization of the risk of an internal or
7RWDOO\ external attack on plants and networks
,QWHJUDWHG
3RZHU • Safety Integrated
Reliable protection of personnel, machinery, and the
environment thanks to seamless integration of safety
technologies into the standard automation
Siemens PA 01 · 2015 5
© Siemens AG 2014
Smart interfaces allow linking to industrial or building automation, making it possible to fully
exploit all the optimization potential of an integrated solution. This is how we provide our
customers around the world with answers to their challenges. With highly efficient, reliable,
and safe power distribution, we lay the foundation for sustainable infrastructure and cities,
Comprehensive answers for
power distribution in complex buildings, and industrial plants. We bring power to the point – wherever and whenever it is
energy systems – from Siemens needed.
6 Siemens PA 01 · 2015
© Siemens AG 2014
Electrification
Renewables
≤ 110 kV
Siemens PA 01 · 2015 7
© Siemens AG 2014
Industries
In the field of process instrumentation, process analytics and weighing technology, Siemens focuses on a
◼ Chemical
◼ Pharmaceutical
◼ Water/wastewater
◼ Marine
8 Siemens PA 01 · 2015
© Siemens AG 2014
Process Analytics
Siemens is a leading provider of process gas analyzers and analysis systems. We provide our global users the best
solutions for their applications based on innovative analysis technologies, customized system engineering, sound
knowledge of process applications and strong professional support. And with Totally Integrated Automation,
Siemens Process Analytics is your qualified partner for efficient solutions that seamlessly integrates process gas
Siemens PA 01 · 2015 9
© Siemens AG 2014
From emission monitoring in waste incinerators and power plants, gas analysis in the chemical
industry and rotary kiln monitoring in cement plants, the extremely accurate and reliable Siemens
gas analyzers are the perfect solution for the job.
SITRANS SL
Continuous gas analyzer with
benchmark-setting in-situ analysis
technology for process control
even under extreme measurement
conditions.
10 Siemens PA 01 · 2015
© Siemens AG 2014
The technology used in process gas analyzers is deter- The ULTRAMAT 23 is also available with a build-in H2S-
mined by the requirements of the specific application. The sensor for biogas applications.
analyzers must be cost-effective, functional, space- and
energy-saving, and must provide just the right amount of SERIES 6
power to meet all needs. The Series 6 gas analyzers are a family of gas analyzers
that meet a complete range of measurement require-
Siemens Process Analytics offers a comprehensive analyti-
ments:
cal portfolio to meet all user requirements for complete
measurement solutions. ◼ CALOMAT 6 [2] [3]
We combine proven expertise in developing high-perfor- is available in both 19” rack mount and field mount
mance analytical devices with in-depth application knowl- designs and uses the thermal conductivity measurement
edge from many process industry applications. principle to accurately measure the composition and
concentration of process gases. It is primarily designed for
The analyzers operate using a menu structure and comply
the measurement of hydrogen concentrations in inert gas
with the NAMUR recommendations. The analyzers can
such as blast furnace gases and carbon dioxide mixtures.
be easily integrated into the SIMATIC automation Totally
Integrated Automation (TIA) concept and are programmed ◼ CALOMAT 62 [2] [3]
using SIMATIC PDM software and PROFIBUS DP / PA uses the thermal conductivity detection (TCD) principle
interfaces. and is specially designed for use in applications with
For service and maintenance tasks with our extractive corrosive gases such as chlorine. The CALOMAT 62
process gas analyzers is the SIPROM GA software tool suit- measures the concentration of gas components such as
able. Integration into the Ethernet permits remote servic- H2, Cl2, HCl or NH3 in binary or quasi-binary gas mixtures.
ing and diagnostics over long distances.
◼ FIDAMAT 6 [3]
PROCESS GAS ANALYSIS – EXTRACTIVE measures the total hydrocarbon content in air or even in
◼ ULTRAMAT 23 [1] high-boiling gas mixtures. It is the ideal solution for nearly
all measurement requirements, from emission monitoring
is an innovative multicomponent analyzer for the as well as trace measurements of hydrocarbons in pure
measurement of up to 3 infrared sensitive gases using the gas analysis and total measurement of high hydrocarbon
NDIR principle as well as measuring oxygen (O2) using an concentrations, even in the presence of corrosive gases.
electrochemical or paramagnetic oxygen measuring cell.
The ULTRAMAT 23 is suitable for a wide range of stand-
ard applications, such as emission monitoring, furnace
optimization, room air monitoring and other applications.
Calibration using ambient air eliminates the need for ex-
pensive calibration gases.
Siemens PA 01 · 2015 11
© Siemens AG 2014
12 Siemens PA 01 · 2015
© Siemens AG 2014
Siemens PA 01 · 2015 13
© Siemens AG 2014
Siemens application experience and innovative technology in the field of process gas
chromatography enables us provide the perfect measurement solutions for our customers. With our
analyzers, we solve a wide range of measurement challenges in almost any industry – combining
exceptional performance with the lowest cost-of-ownership.
SITRANS CV
Ultra compact gas chromatograph
for reliable, exact and fast analysis
of natural gas and biogas.
14 Siemens PA 01 · 2015
© Siemens AG 2014
[1] [2]
Siemens PA 01 · 2015 15
© Siemens AG 2014
Our customers’ requirements drive the solution. We offer comprehensive designs covering the sampling
point and sample preparation up to complete analyzer cabinets whether used for portable applications or for
installation in a larger analyzer shelter. Signal processing and communications to the control room and process
control system is also part of the total system solution.
Our solutions for your application needs are based on dec- ◼ Remote maintenance, on-site servicing, spare parts
ades of global experience in process automation and engi- supplies and customized training.
neering as well as specialized knowledge in key industries
◼ Analytical Application Sets
and industrial sectors.
are standardized system solutions for a number of speci-
This guarantees you get Siemens quality from a single fic applications. Siemens offers ready-to-use developed
source with performance across the entire system. solution sets for various industries like energy, natural
Our portfolio of products and services include: gas, etc.
Standardized packages include the Set CEM 1 and Gas
◼ Customized services and solutions from front-end
met CEMS for the emission monitoring market. Specifi-
engineering and design (FEED) up to fully air-conditioned
cally designed for the natural gas market is the Set CV
analyzer shelters.
(calorific value). The Set CV includes a variety of modules,
◼ Support during the approval phase. which can be individually combined. For the monitoring
◼ Preliminary and detailed planning with state-of-the-art of hydrogen-cooled turbo generators the Set GGA is the
state-of-the-art solution. The Set BGA offers a modular a
tools and complete documentation.
standardized solution for the biogas market.
◼ System assembly and testing available in Siemens
We would be pleased to demonstrate our expertise as our
facilities in the USA, Germany and Singapore.
references speak for themselves!
◼ Experience with all relevant national and international
standards.
◼ Field commissioning and start-up by specialists all over
the world.
16 Siemens PA 01 · 2015
1
© Siemens AG 2014
1/2 Introduction
1/28 ULTRAMAT 23
1/28 General information
1/41 19" rack unit and portable version
1/59 Documentation,
Suggestions for spare parts
1/60 ULTRAMAT 6
1/60 General information
1/67 19" rack unit
1/81 Field device
1/92 Documentation
1/93 Suggestions for spare parts
1/94 ULTRAMAT/OXYMAT 6
1/94 General information
1/103 19" rack unit
1/115 Documentation
1/116 Suggestions for spare parts
1/117 OXYMAT 6
1/117 General information
1/125 19" rack unit
1/132 Field device
1/139 Documentation
1/140 Suggestions for spare parts
1/141 OXYMAT 61
1/141 General information
1/146 19" rack unit
1/151 Documentation
1/152 Suggestions for spare parts
1/153 OXYMAT 64
1/153 General information
1/160 19" rack unit
1/166 Documentation,
Suggestions for spare parts
1/167 CALOMAT 6
1/167 General information
1/172 19" rack unit
1/179 Field device
1/186 Documentation,
Suggestions for spare parts
1/187 CALOMAT 62
1/187 General information
1/192 19" rack unit
1/198 Field device
1/205 Documentation,
Suggestions for spare parts
1/206 FIDAMAT 6
1/206 General information
1/212 19" rack unit
1/219 Documentation
1/220 Suggestions for spare parts
Siemens PA 01 · 2015
© Siemens AG 2014
1 ■ Overview
Siemens process gas analyzers have been used in the process Integrated Automation" concept which is globally unique. This
industry for more than 40 years, and are renowned for their concept permits design of uniform process communication from
quality, reliability and accuracy. The flexibility provided by the the operations management level down to the field level. The
continuous process gas analyzers with respect to housing simple integration of analyzers into the host control systems is
design, explosion protection, corrosion resistance and commu- the basis for a uniform automation and analysis solution.
nications capability means that optimum solutions can be found
for all applications. Many years of experience in the development and production of
analyzers as well as in the planning and installation of analyzer
Nowadays, the communications capability of analyzers is systems distinguishes Siemens as a solution provider - reliable,
becoming increasingly important. Siemens process gas innovative and with global presence.
analyzers are an integral component of Siemens’ "Totally
Process line
Process
Sample Sample feedback/
Sampling Analyzer
gas preparation exhaust
■ Overview ■ Application
1
Application areas
Depending on the analyzer modules installed, the device is
predominantly used in the following sectors:
• Chemical industry
• Petrochemicals
• Steel
• Cement
• Power generation
• Environmental protection
■ Design
19" rack unit
• 19" rack unit with 3 height units (HU) for installation
- in hinged frames
- in cabinets with or without telescopic rails
• Gas connections for sample gas inlet and outlet: for pipe
The entire SIPROCESS GA700 device is configured in a modular diameter 6 mm or 1/4"
fashion and consists of a base unit and at least one – maximum • Purging gas connections 10 mm and 3/8" (optional)
two – analyzer modules. It can optionally be fitted with up to two
interfaces modules (option modules). Wall-mounted device
• Gas connections for sample gas inlet and outlet: Pipe union
■ Benefits for pipe diameter 6 mm or 1/4" (directly on the analyzer
modules)
The base unit provides: • Purging gas connections (optional), purging gas connection
• Transmission and evaluation of measurement results for 6 mm or 1/4" hose (optional)
• Display and transmission of device parameters Display and operator panel
• Operation (parameterization, configuration) • LCD panel for simultaneous display of:
- Measured value
In addition to the analyzer modules, the base unit contains the
- Status line
interfaces for the peripherals.
- Measuring ranges
• Menu-driven operation for parameterization, test functions,
adjustment
• Operator support in plain text
• Operating software (11 languages)
Special keys
Display Numeric keypad
■ Function
Essential characteristics
• Measuring range identification
• Storage of measured values possible during adjustments
• Four freely parameterizable measuring ranges, also with
suppressed zero point
• Autoranging possible; remote switching is also possible
• Wide range of selectable time constants (static/dynamic noise
suppression); i.e. the response time of the analyzer can be
matched to the respective measuring task
• Measuring point switchover for up to 12 measuring points
(programmable)
• Parameterizable measuring point identification
• Automatic, parameterizable measuring range calibration
• Operation based on the NAMUR recommendation
• Three control levels with their own authorization codes for the
prevention of accidental and unauthorized operator interven-
tions
• Simple handling using a numerical membrane keyboard and
operator prompting
• Customer-specific analyzer options such as:
- Customer acceptance
- TAG labels
■ Technical specifications
1
19" rack unit Wall housing
General information General information
■ Dimensional drawings
1
132.55
37.7 57.15
10.3 170.8
13.5 421.5
482.3
441.3
421.5
419
Slot 1 Slot 2
47
80.5
104.5
128.5
205
297
389
370
20
291.5 0
272.5
237.5
0 0
168.5
260.5
408
425
0
76.5
450
196 338.3
0
28
164.6
493
549
567.6
■ Schematics
1
Connection of the signal cables
Connector number
4 3 2 1 vtYUX
Processing module
h Ethernet and SUB-D 37F,
digital inputs/outputs
1 Sample gas inlet
2 Sample gas outlet Option module 2.1
3 N.C. SUB-D 15M, binary inputs
4 Reference gas inlet and analog outputs
Expansion options for processing and option modules with the example of the rear wall of the rack unit
8
Analog output 13-N 15
Relay 10
7
Analog output 13-P 14
6
13
Analog output 11-N 5
Relay 11 12
Analog output 11-P 4
11
3
Analog output 12-N 10
Relay 9 2
Analog output 12-P 9
1
M 19 GND
37 NC
18 NC
36 Binary input 8-P
17 Binary input 7-P
35 Binary input 6-P
16 Binary input 5-P Floating via optocoupler
34 Binary input 4-P "0" = 0 V (-3 ... +5 V)
15 Binary input 3-P "1" = 24 V (15 ... 33 V)
33 Binary input 2-P
14 Binary input 1-P
32 Binary input 1 to 8-N
13
31 Relay 8
12
30
11 Relay 7
29
10
28 Relay 6
9
27
8 Relay 5 Contact load
26 max. 24 V/1.7 A, AC/DC; shown
7 relay contacts: relay coil has zero
25 current
Relay 4
6
24
5 Relay 3
23
4
22 Relay 2
3
21
2 Relay 1
20
M 1 GND
Terminal row A
M 1 GND
2
3 Relay 1
4
5
6 Relay 2
7
8
9 Relay 3 Contact load
10 max. 24 V/1.7 A, AC/DC; shown
11 relay contacts: relay coil has zero
12 Relay 4 current
13
14
15 Relay 5
16
17
18 Relay 6
19
Terminal row B
1 NC Contact load
2 max. 24 V/1.7 A, AC/DC; shown
3 Relay 7 relay contacts: relay coil has zero
4 current
5 Binary input 1 to 8-N (GND)
6 Binary input 1-P
7 Binary input 2-P
8 Binary input 3-P Floating via optocoupler
9 Binary input 4-P "0" = 0 V (-3 ... +5 V)
10 Binary input 5-P "1" = 24 V (15 ... 33 V)
11 Binary input 6-P
12 Binary input 7-P
13 Binary input 8-P
14 Binary input 1 to 8-N (GND)
15 NC
16 NC Contact load
17 max. 24 V/1.7 A, AC/DC; shown
18 Relay 8 relay contacts: relay coil has zero
19 current
Terminal row C
1 NC
2
3 Relay 21
4
5
6 Relay 22
7
8
9 Relay 23 Contact load
10 max. 24 V/1.7 A, AC/DC; shown
11 relay contacts: relay coil has zero
12 Relay 24 current
13
14
15 Relay 25
16
17
18 Relay 26
19
Terminal row D
1 NC
2 Analog output 11-P
3 Analog output 11-N
4 Analog output 12-P
5 Analog output 12-N
6 Analog output 13-P
7 Analog output 13-N Analog outputs floating
8 Analog output 21-P (also from each other), RL: ≤ 750 Ω
9 Analog output 21-N
10 Analog output 22-P
11 Analog output 22-N
12 Analog output 23-P
13 Analog output 23-N
14 NC
15 NC
16 NC
17 NC
18 NC
M 19 GND
Terminal row A
M 1 GND
2
3 Relay 9
4
5
6 Relay 10
7 Contact load
8
max. 24 V/1.7 A, AC/DC; shown
9 Relay 11
relay contacts: relay coil has zero
10 current
11
12 Relay 12
13
14
15 Relay 13
16
Terminal row B
1 NC
Contact load
2
max. 24 V/1.7 A, AC/DC; shown
3 Relay 14 relay contacts: relay coil has zero
4 current
5 Binary input 9 to 16-N
6 Binary input 9-P
7 Binary input 10-P
8 Binary input 11-P
Floating via optocoupler
9 Binary input 12-P
"0" = 0 V (-3 ... +5 V)
10 Binary input 13-P
"1" = 24 V (15 ... 33 V)
11 Binary input 14-P
12 Binary input 15-P
13 Binary input 16-P
Contact load
14 max. 24 V/1.7 A, AC/DC; shown
15 Relay 15 relay contacts: relay coil has zero
16 current
Terminal row C
1 NC
2
3 Relay 16
4
5
6 Relay 17
7 Contact load
8
max. 24 V/1.7 A, AC/DC; shown
9 Relay 18
relay contacts: relay coil has zero
10 current
11
12 Relay 19
13
14
15 Relay 20
16
Terminal row D
1 NC
2 Binary input 17 to 18-N Floating via optocoupler
Binary input 17-P "0" = 0 V (-3 ... 5 V)
3
Binary input 18-P "1" = 24 V (15 ... 33 V)
4
5 Analog input 1-P
M 6 Analog input 1-N
7 Analog input 2-P
M 8 Analog input 2-N Analog inputs non-floating,
9 Analog input 3-P 0 ... 20 mA/(internal resistance ≤ 100 Ω)
M 10 Analog input 3-N
11 Analog input 4-P
M 12 Analog input 4-N
13 Binary input 19 to 20-N Floating via optocoupler
14 Binary input 19-P "0" = 0 V (-3 ... 5 V)
15 Binary input 20-P "1" = 24 V (15 ... 33 V)
M 16 GND
■ Design
1
2
3
4
Options
Pressure Diaphragm FKM (Viton)
switch
Enclosure PA 6.3 T
7 6 10
4
8
11
5
1
Gas path plan, high-pressure version with optional pressure switch for monitoring reference gas pressure
7 6
4
8 10
9
5
1
Gas path plan, low-pressure with external reference gas pump, with hoses
■ Mode of operation
1
Oxygen is highly paramagnetic. This outstanding property of
paramagnetism is used as a physical measuring effect for
oxygen analysis. 1
Table 2: Zero point error due to diamagnetism or paramagnetism of some carrier gases with nitrogen as the reference gas at 60 °C and
1 000 hPa absolute (according to IEC 1207/3)
Conversion to other temperatures:
The deviations from the zero point listed in Table 2 must be multiplied by a correction factor (k):
• with diamagnetic gases: k = 333 K / ( [°C] + 273 K)
• with paramagnetic gases: k = [333 K / ( [°C] + 273 K)]2
(All diamagnetic gases have a negative deviation from zero point).
• Devices with tubes 500 … 1 450 hPa (abs.) • At span 0.5 % of the current measuring
span/10 K or 50 vpm O2/10 K,
• Devices with pipes 500 … 2 450 hPa (abs.) whichever is larger
Reference gas pressure Sample gas pressure
• High-pressure connection 0.2 to 0.4 MPa above the sample • Without pressure compensation Deviation approx. 2 % of current
gas pressure, but a maximum of measuring span/1 % pressure
0.5 MPa (absolute) variation
- Without vibration compensation 2 000 … 3 500 hPa above sample • With pressure compensation 0.2 % of the current measuring
gas pressure; max. 5 000 hPa (abs.) switched on span/1 % pressure variation or
50 vpm O2/1 % pressure variation,
- With vibration compensation 2 500 … 4 000 hPa above sample
whichever is larger
gas pressure; max. 5 000 hPa (abs.)
Sample gas flow 1 % of the current measuring span
• Low-pressure connection with exter- 100 hPa above the sample gas
with a flow rate change of 0.1 l/min
nal reference gas pump (only for pressure
within the permissible flow range
sample gas pressure 500 ...
(0.3 ... 1 l/min)
1 500 hPa (absolute))
Carrier gases Zero point deviation (cross-sensitiv-
Pressure loss between sample gas < 100 hPa at 1 l/min
ity) in accordance with Table A.1 of
inlet and sample gas outlet
EN 61207-3
Sample gas flow 18 … 60 l/h (0.3 … 1 l/min)
Supply voltage (fluctuations of the 0.1 % of full-scale value of
Sample gas temperature 0 … 60 °C supply voltage of the base unit*) in the characteristic
range of 90 to 253 V AC/47 to 63 Hz)
Sample gas humidity (rel. humidity) < 90 % (condensation inside the
gas path is to be avoided)
Sample chamber temperature
Standard version Approx. 72 °C
Click on the Article No. for the online configuration in the PIA Life Cycle Portal.
Integrated into base unit1)
Rack unit 0
Wall-mounted device 1
Reference gas pressure
Low-pressure version 100 hPa (for the connection of an external pump; without pressure switch) A A A
High pressure (3 000 ... 5 000 hPa) (absolute pressure values) C
High pressure (3 000 ... 5 000 hPa) (absolute pressure values), with pressure switch D
Smallest measuring range Largest measuring range
0 ... 0.5 % 0 ... 100 % B B
0 ... 1 % 0 ... 100 % C C
0 ... 2 % 0 ... 100 % D
0 ... 5 % 0 ... 100 % E
Gas path
Material of gas path Material of sample chamber Temperature of analysis part
Hose made of FKM (Viton) Stainless steel (1.4571) 72 °C (thermostatted) 0
Pipe made of stainless steel (1.4571) Stainless steel (1.4571) 72 °C (thermostatted) 2 2
Vibration compensation
Without 0
With 1
1)
With order code "W01", please specify option "0".
Ordering examples
OXYMAT 7 module in rack unit enclosure "Example1"
7MB3000-0DX00-2AA0-Z + Y01 "Example1"
7MB3020-0AD00-0AA0-Z + Y01 "Example1"
OXYMAT 7 module in wall housing "Example2"
7MB3000-3DX00-2AA0-Z + Y01 "Example2"
7MB3020-0AD00-0AA0-Z + Y01 "Example2"
■ Schematics
1
Gas connections
4 3 2 1
■ Application
1
Areas of application Special versions
• Optimization of small firing systems • Separate gas paths
• Monitoring of exhaust gas concentration from firing systems The ULTRAMAT 23 with 2 IR components without pump is
with all types of fuel (oil, gas and coal) as well as operational also available with two separate gas paths. This allows the
measurements with thermal incineration plants measurement of two measuring points as used e.g. for the
NOx measurement before and after the NOx converter.
• Room air monitoring The ULTRAMAT 23 gas analyzer can be used in emission
• Monitoring of air in fruit stores, greenhouses, fermenting measuring systems and for process and safety monitoring.
cellars and warehouses • TÜV version/QAL/MCERTS
• Monitoring of process control functions TÜV-approved versions of the ULTRAMAT 23 are available for
• Atmosphere monitoring during heat treatment of steel measurement of CO, NO, SO2 and O2 according to
13th BlmSchV/27th BlmSchV/30th BImSchV (N2O)
• For use in non-potentially-explosive atmospheres and TA Luft.
Application areas in biogas plants Smallest TÜV-approved and permitted measuring ranges:
- 1- and 2-component analyzer
• Monitoring of fermenters for generating biogas (input and CO: 0 to 150 mg/m3
pure sides) NO: 0 to 100 mg/m3
• Monitoring of gas-driven motors (power generation) SO2: 0 to 400 mg/m3
• Monitoring of feeding of biogas into the commercial gas net- - 3-component analyzer
work CO: 0 to 250 mg/m3
NO: 0 to 400 mg/m3
Application area of paramagnetic oxygen sensor SO2: 0 to 400 mg/m3
• Flue gas analysis All larger measuring ranges are also approved.
• Inerting plants
Furthermore, the TÜV-approved versions of the ULTRAMAT 23
• Room air monitoring comply with the requirements of EN 14956 and QAL 1 accord-
• Medical engineering ing to EN 14181. Conformity of the analyzers with both stan-
dards is TÜV-certified.
Further applications
• Environmental protection Determination of the analyzer drift according to EN 14181
(QAL 3) can be carried out manually or with a PC using the
• Chemical plants SIPROM GA maintenance and servicing software. In addition,
• Cement industry selected manufacturers of emission evaluation computers of-
fer the possibility for downloading the drift data via the ana-
lyzer’s serial interface and to automatically record and process
it in the evaluation computer.
• Version with reduced response time
The connection between the two condensation traps is
equipped with a stopper to lead the complete flow through the
measuring cell (otherwise only 1/3 of the flow), i.e. the re-
sponse time is 2/3 faster. The functions of all other compo-
nents remain unchanged
• Chopper compartment flushing: consumption 100 ml/min
(upstream pressure: approx. 3 000 hPa)
8
Gas outlet
12 2
13 P 10
F 11
Zero gas
3
14
15
16 with O2
2 Enclosure
without O2
15 5 flushing
17
9
P Chopper
compartment
7
flushing
ULTRAMAT 23, portable, in sheet-steel housing with internal sample gas pump, condensation trap with safety filter on front plate, optional oxygen
measurement
16 with O2
2 without O2
15
17
P
ULTRAMAT 23, 19" rack unit enclosure with internal sample gas pump, optional oxygen measurement
13
12
F P 9
Gas inlet
1
Gas outlet
14 2
not used
3
not used
4
Enclosure
5 flushing
Inlet atmospheric
9 pressure sensor
15 6
Chopper
purge
7
16 with O2
2 without O2
15
17
P
ULTRAMAT 23, 19" rack unit enclosure without internal sample gas pump, optional oxygen measurement
13
1
12
F P 9
Gas inlet 1
14 1
15
16
with O2
2
15 without O2
13
12
P Gas outlet 1
F 9 2
Gas inlet 2
3
14
15
15 Gas outlet 2
4
Enclosure
5 flushing
17
Inlet atmospheric
P pressure sensor
9 6
Chopper
7 purge
ULTRAMAT 23, 19" rack unit enclosure without internal sample gas pump, with separate gas path for the 2nd measured component or for the 2nd and
3rd measured components, optional oxygen measurement
Gas inlet 1
1
14
Gas outlet 1
2
Gas inlet 2
3
14
Gas outlet 2
4
Enclosure flushing
5
Inlet atmospheric
pressure sensor
9 6
Chopper
purge
7
17
P
ULTRAMAT 23, 19" rack unit enclosure, sample gas path version in pipes, optional separate gas path, always without sample gas pump, without safety
filter and without safety condensation trap
2 GvY
15
17
P
ULTRAMAT 23, 19" rack unit enclosure with internal sample gas pump and H2S sensor
13
12 9
F P Sample/calibration gas
11 10 1 inlet
Gas outlet
9 2
Zero gas inlet
14 3
Not used
4
Enclosure flushing
5 Inlet of
atmospheric
9 6 pressure sensor
Inlet of chopper
15 compartment
7
flushing (option)
19
15
17
P
ULTRAMAT 23, 19" rack unit enclosure with internal sample gas pump and paramagnetic oxygen measurement
■ Function
1
The ULTRAMAT 23 uses two independent measuring principles
which work selectively. 12
1
Infrared measurement 10
2
The measuring principle of the ULTRAMAT 23 is based on the
molecule-specific absorption of bands of infrared radiation,
which in turn is based on the "single-beam procedure". A radia- 3
tion source (7) operating at 600 C emits infrared radiation, 9
which is then modulated by a chopper (5) at 8 1/3 Hz.
The IR radiation passes through the sample chamber (4), into 11
which sample gas is flowing, and its intensity is weakened as a
function of the concentration of the measured component. 9
Sample gas
The reciever chamber - set up as a two- or three-layer detector -
outlet
is filled with the component to be measured.
The first detector layer (11) primarily absorbs energy from the 4
central sections of the sample gas IR bands. Energy from the pe-
ripheral sections of the bands is absorbed by the second (2) and Sample gas
third (12) detector layers. inlet
The microflow sensor generates a pneumatic connection be- 9
tween the upper layer and the lower layers. Negative feedback
from the upper layer and lower layers leads to an overall narrow-
ing of the spectral sensitivity band. The volume of the third layer
8 5
and, therefore, the absorption of the bands, can be varied using
a "slide switch" (10), thereby increasing the selectivity of each in- 6
dividual measurement.
The rotating chopper (5) generates a pulsating flow in the re- 7
ciever chamber that the microflow sensor (3) converts into an
electrical signal.
The microflow sensor consists of two nickel-plated grids heated 1 Capillary 7 IR source
to approximately 120 ºC, which, along with two supplementary 2 Second detector layer 8 Reflector
resistors, form a Wheatstone bridge. The pulsating flow together 3 Microflow sensor 9 Window
with the dense arrangement of the Ni grids causes a change in 4 Sample cell 10 Slide
5 Chopper wheel 11 First detector layer
resistance. This leads to an offset in the bridge, which is depen-
6 Chopper motor 12 Third detector layer
dent on the concentration of the sample gas.
Note ULTRAMAT 23, principle of operation of the infrared channel (example
with three-layer detector)
The sample gases must be fed into the analyzers free of dust.
Condensation in the sample chambers must be prevented.
Therefore, the use of gas modified for the measuring task is nec-
essary in most application cases.
As far as possible, the ambient air of the analyzer should not
have a large concentration of the gas components to be mea-
sured.
H2S H 2S
H 2S H 2S
Gas diaphragm
Working electrode
Reference electrode
H2SO4 electrolyte
Counterelectrode
Connection pins
Iso-butylene C4H8 -0.94 -1.06 Cross-sensitivities (with accompanying gas concentration 100 %)
■ Technical specifications
1
General information Gas inlet conditions
Measured components Maximum of 4, comprising three Sample gas pressure
infrared-sensitive gases and oxy- • Without pump Unpressurized (< 1 200 hPa,
gen absolute)
Measuring ranges Two per measured component • With pump Depressurized suction mode, set
Display LCD with LED backlighting and in factory with 2 m hose at sample
contrast control; function keys; gas outlet; full-scale value cali-
80 characters (4 lines/20 charac- bration necessary under different
ters) venting conditions
(800 ... 1 050 hPa, absolute)
Operating position Front wall, vertical
Sample gas flow 72 … 120 l/h (1.2 … 2 l/min)
Conformity CE symbol EN 61000-6-2,
EN 61000-6-4 Sample gas temperature Min. 0 to max. 50 °C, but above
the dew point
Design, enclosure
Sample gas humidity < 90 % RH (relative humidity),
Weight Approximately 10 kg non-condensing
Degree of protection, 19" rack unit IP20 according to EN 60529
and desktop model Technical data, infrared channel
Electrical characteristics So that the technical data can be complied with, a cycle time of
24 hours must be activated for the AUTOCAL. The cycle time of the
EMC In accordance with standard AUTOCAL function must be 6 hours when measuring small NO and
(Electromagnetic Compatibility) requirements of NAMUR NE21 SO2 measuring ranges ( 400 mg/m³) on TÜV/QAL-certified systems.
(safety extra-low voltage (SELV) (08/98) or EN 50081-1,
with safety isolation) EN 50082-2 Measuring ranges See ordering data
Power supply 100 V AC, +10 %/-15 %, 50 Hz, Chopper compartment flushing Upstream pressure approximately
120 V AC, +10 %/-15 %, 50 Hz, 3 000 hPa; purging gas con-
sumption approximately
200 V AC, +10 %/-15 %, 50 Hz, 100 ml/min
230 V AC, +10 %/-15 %, 50 Hz,
Time response
100 V AC, +10 %/-15 %, 60 Hz,
Warm-up period Approximately 30 min (at room
120 V AC, +10 %/-15 %, 60 Hz, temperature) (the technical speci-
230 V AC, +10 %/-15 %, 60 Hz fication will be met after 2 hours)
Power consumption Approx. 60 VA Delayed display (T90 time) Dependent on length of analyzer
chamber, sample gas line and
Electrical inputs and outputs parameterizable attenuation
Analog output Per component, 0/2/4 up to Attenuation(electrical time constant) Parameterizable from 0 … 99.9 s
20 mA, NAMUR, isolated,
max. load 750 Measuring response
(relating to sample gas pressure 1 013 hPa absolute, 1.0 l/min sample
Relay outputs 8, with changeover contacts, gas flow and 25 °C ambient temperature)
freely parameterizable, e.g. for
measuring range identification; Output signal fluctuation < 1 % of the current measuring
24 V AC/DC/1 A load, potential- range (see rating plate)
free, non-sparking Detection limit 1 % of the current measuring
Digital inputs 3, dimensioned for 24 V, potential- range
free Linearity error • In largest possible measuring
• Pump range:
< 1 % of the full-scale value
• AUTOCAL • In smallest possible measuring
• Synchronization range:
< 2 % of the full-scale value
Serial interface RS 485
Repeatability 1 % of the current measuring
AUTOCAL function Automatic unit calibration with range
ambient air (depending on mea-
sured component); adjustable Drift
cycle time from 0 (1) … 24 hours Zero point
Options Add-on electronics, each with 8 • With AUTOCAL Negligible
additional digital inputs and relay
outputs for e.g. triggering of auto- • Without AUTOCAL < 2 % of the current measuring
matic calibration and for range/week
PROFIBUS PA or PROFIBUS DP
Full-scale value drift
Climatic conditions
• With AUTOCAL Negligible
Permissible ambient temperature
• Without AUTOCAL < 2 % of the current measuring
• During operation 5 … 45 °C range/week
• During storage and transportation -20 ... +60 °C
Permissible ambient humidity < 90 % RH (relative humidity) dur-
ing storage and transportation
Permissible pressure fluctuations 600 … 1 200 hPa
Technical data, H2S channel for measuring ranges of 0 ... 5 000 vpm Technical data, paramagnetic oxygen cell
1
Measured components Maximum of 4, comprising 1 or 2 Measured components Maximum of 4, comprising up to 3
infrared-sensitive gases, 1 oxy- infrared-sensitive gases and an
gen component and 1 hydrogen oxygen component
sulfide component
Measuring ranges 2 per component
Measuring ranges of H2S sensor
MB 5000 • Min. 0 ... 2 % vol O2
• Smallest measuring range 0 ... 5 000 vpm • Max. 0 ... 100 % vol O2
• Suppressed measuring range
• Largest measuring range 0 ... 5 000 vpm possible; e.g. 95 ... 100 %
Service life of the sensor Approx. 12 months
Permissible atmospheric pressure 700 ... 1 200 hPa
Permissible atmospheric pressure 750 ... 1 200 hPa
Permissible operating temperature 5 ... 45 °C (41 ... 113 °F)
Permissible operating temperature 5 ... 40 °C (41 ... 104 °F)
Influencing variables Cross-inferences (interfering gases) See Table "Cross-sensitivities"
Zero point drift • Measuring range 2 %: max.
Carrier gases The hydrogen sulfide sensor must 0.1 % with weekly zero adjust-
not be used if the accompanying ment
gas contains the following com-
ponents: • Measuring range 5 %: max.
0.1 % with weekly zero adjust-
• Compounds containing chlorine ment
• Compounds containing fluorine • Measuring range 25 % or
• Heavy metals greater:
• Aerosols max. 0.5 % with monthly zero
adjustment
• Alkaline components
(e.g. NH3 > 5 vpm) Measured-value drift Negligible with AUTOCAL
Cross-inferences 100 ppm SO2 result in a cross- Temperature error < 2 %/10 K referred to measuring
(interfering gases) interference of < 30 ppm H2S range 5 %
Drift < 1 % of the current measuring < 5 %/10 K referred to measuring
range per month range 2 %
Temperature < 3 %/10 K relating to full-scale Humidity error for N2 with 90 % rela- < 0.6 % at 50 °C
value tive humidity after 30 min
Atmospheric pressure < 0.2 % of the measured value Atmospheric pressure < 0.2 % of measured value
per 1 % pressure variation per 1 % pressure variation
Measuring response Delayed display (T90 time) < 60 s
Delayed display (T90 time) < 80 s with sample gas flow of Output signal noise < 1 % of smallest measuring
approx. 1 ... 1.2 l/min range
Output signal noise < 15 ppm H2S Repeatability < 1 % of smallest measuring
range
Display resolution < 0.2 % of the full-scale value
Output signal resolution < 30 ppm H2S
Repeatability < 4 % referred to full-scale value
}
0 ... 100 mg/m³ 0 ... 750 mg/m³ T
0 ... 150 mg/m³ 0 ... 750 mg/m³ U
TÜV version
0 ... 250 mg/m³ 0 ... 1 250 mg/m³ V
0 ... 400 mg/m³ 0 ... 2 000 mg/m³ W
0 ... 50 vpm 0 ... 2 500 vpm X
Oxygen measurement5)
Without O2 sensor 0
With O2 sensor 1 1
With paramagnetic oxygen measuring cell 8 8 8 8
Hydrogen sulfide measurement
Without 0
With H2S sensor 0 ... 5/50 ppm 1 1 1 1
With H2S sensor 0 ... 5 000 ppm 3 3 3 3
Power supply
100 V AC, 50 Hz 0
120 V AC, 50 Hz 1
200 V AC, 50 Hz 2
230 V AC, 50 Hz 3
100 V AC, 60 Hz 4
120 V AC, 60 Hz 5
230 V AC, 60 Hz 6
Operating software, documentation3)
German 0
English 1
French 2
Spanish 3
Italian 4
Footnotes: See next page.
1)
For measuring ranges below 1 %, a CO2 absorber cartridge can be used for setting the zero point (see accessories)
2)
Without separate zero gas input or solenoid valve
3)
User language can be changed
4)
Standard setting: smallest measuring range, largest measuring range
5)
O2 sensor in gas path of infrared measured component 1
6)
With chopper compartment purging (N2 approx. 3 000 hPa required for measuring ranges below 0.1 % CO2),
to be ordered separately (see order code C02 or C03)
7)
Not suitable for use with emission measurements since the cross-sensitivity is too high
8)
CO2 measurement in accompanying gas Ar or Ar/He (3:1); forming gas
9)
Only for version with Viton hose
10)
Not checked for suitability, maximum possible AUTOCAL cycle 6 h, constant ambient conditions (max. deviation ±1 °C (1.8 °F)
}
0 ... 100 mg/m³ 0 ... 750 mg/m³ T
0 ... 150 mg/m³ 0 ... 750 mg/m³ U
TÜV version
0 ... 250 mg/m³ 0 ... 1 250 mg/m³ V
0 ... 400 mg/m³ 0 ... 2 000 mg/m³ W
0 ... 50 vpm 0 ... 2 500 vpm X
Oxygen measurement5)
Without O2 sensor 0
With O2 sensor 1 1
With paramagnetic oxygen measuring cell 8 88 8
Hydrogen sulfide measurement
Without 0
With H2S sensor 0 ... 5/50 ppm 1 1 1 1
With H2S sensor 0 ... 5 000 ppm 3 3 3 3
Power supply
100 V AC, 50 Hz 0
120 V AC, 50 Hz 1
200 V AC, 50 Hz 2
230 V AC, 50 Hz 3
100 V AC, 60 Hz 4
120 V AC, 60 Hz 5
230 V AC, 60 Hz 6
}
0 ... 100 mg/m³ 0 ... 750 mg/m³ T
0 ... 150 mg/m³ 0 ... 750 mg/m³ U
TÜV version
0 ... 250 mg/m³ 0 ... 1 250 mg/m³ V
0 ... 400 mg/m³ 0 ... 2 000 mg/m³ W
0 ... 50 vpm 0 ... 2 500 vpm X
0 ... 500 vpm 0 ... 5 000 vpm Y
Operating software, documentation3)
German 0
English 1
French 2
Spanish 3
Italian 4
Footnotes: See next page.
1)
For measuring ranges below 1 %, a CO2 absorber cartridge can be used for setting the zero point (see accessories)
2)
Without separate zero gas input or solenoid valve
3)
User language can be changed
4)
Standard setting: smallest measuring range, largest measuring range
5)
O2 sensor in gas path of infrared measured component 1
6)
With chopper compartment purging (N2 approx. 3 000 hPa required for measuring ranges below 0.1 % CO2),
to be ordered separately (see order code C02 or C03)
7)
Not suitable for use with emission measurements since the cross-sensitivity is too high
8)
CO2 measurement in accompanying gas Ar or Ar/He (3:1); forming gas
9)
Only for version with Viton hose
10)
Only in conjunction with CO2 measuring range 0 to 5 % to 0 to 25 % (CP)
11)
Not checked for suitability, maximum possible AUTOCAL cycle 6 h, constant ambient conditions (max. deviation ±1 °C (1.8 °F)
}
0 ... 50 mg/m³ 0 ... 500 mg/m³ S
0 ... 150 mg/m³ 0 ... 750 mg/m³ TÜV version U
0 ... 250 mg/m³ 0 ... 1 250 mg/m³ V
0 ... 400 mg/m³ 0 ... 2 000 mg/m³ W
0 ... 50 vpm 0 ... 2 500 vpm X
0 ... 500 vpm 0 ... 5 000 vpm Y
Operating software, documentation3)
German 0
English 1
French 2
Spanish 3
Italian 4
Footnotes: See page 1/51.
1)
For measuring ranges below 1 %, a CO2 absorber cartridge can be used for setting the zero point (see accessories)
2)
Without separate zero gas input or solenoid valve
3)
User language can be changed
4)
Standard setting: smallest measuring range, largest measuring range
5)
O2 sensor in gas path of infrared measured component 1
6)
With chopper compartment purging (N2 approx. 3 000 hPa required for measuring ranges below 0.1 % CO2),
to be ordered separately (see order code C02 or C03)
7)
Not suitable for use with emission measurements since the cross-sensitivity is too high
8)
CO2 measurement in accompanying gas Ar or Ar/He (3:1); forming gas
9)
Only for version with Viton hose
10)
Only in combination with CO/CO2, measuring range 0 to 75/750 mg/m³, 0 to 5/25 % [-BL-]
11)
Only in combination with CO2/NO, measuring range 0 to 5/25 %, 0 to 500/5 000 vpm [-DC-]
12)
Only in combination with N2O, measuring range 0 to 50/500 mg/m³ [-SS-]
13)
Not checked for suitability, maximum possible AUTOCAL cycle 6 h, constant ambient conditions (max. deviation ±1 °C (1.8 °F)
■ Dimensional drawings
1
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■ Schematics
1
Pin assignment (electrical and gas connections)
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M 19 GND
37 NC
18 NC
36 Binary input 8-P
Isolated
17 Binary input 7-P
35 Binary input 6-P via optocoupler
16 Binary input 5-P "0" = 0 V (0 ... 4.5 V)
34 Binary input 4-P "1" = 24 V (13 ... 33 V)
15 Binary input 3-P Safety extra-low voltage
33 Binary input 2-P (SELV) with safe
14 Binary input 1-P electrical isolation.
32 Binary input 1 to 8-N
13
31 Relay 16
12
30
11 Relay 15
29
10
28 Relay 14
9
Contact load
27
8 Relay 13 max. 24 V/1 A, AC/DC
26 for shown
7 relay contact position,
25 Relay 12 the relay has zero current
6
24 Safety extra-low voltage
5 Relay 11 (SELV) with safe
23 electrical isolation.
4
22 Relay 10
3
21
2 Relay 9
20
M 1 GND
5 DGND 5
9 CNTR-N 9
4 CNTR-P/direction control 4
8 RxD/TxD-N (A) 8 PA-N(-)
3 RxD/TxD-P (B) 3 PA-P(+)
7 7
2 2
6 VP /+ 5 V 6
1 1
Note:
All cables to the connectors or terminal blocks must
be shielded and rest against the enclosure potential.
7 6 5 4 3 2 1
ULTRAMAT 23, 19“ unit, e.g. one infrared component with oxygen measurement
Desktop unit
7 5 3 2
ULTRAMAT 23, portable unit, in sheet-steel housing, gas and electrical connections
Chopperraumbespülung
6 atmospherical pressure transducer 6 atmospherical pressure transducer 6 atmospherical pressure transducer
capteur de pression atmosphérique capteur de pression atmosphérique capteur de pression atmosphérique
7 Chopper purge
Balayage de l’obturateur Chopperraumbespülung Chopperraumbespülung Chopperraumbespülung
7 Chopper purge
Balayage de l’obturateur
7 Chopper purge
Balayage de l’obturateur
7 Chopper purge
Balayage de l’obturateur
LED backlit graphic Status line for display Two code levels
display and of analyzer status according to NAMUR
membrane keyboard (programmable) (maintenance and
with noticeable click specialist level)
Display of current
Display of
measuring ranges
concentrations as
numbers and bargraph
for channel 2
Status line for channel 2
to display the unit
Display of status (programmable)
start-of-scale and
full-scale values
ESC key
to abort inputs
Keyboard to
enter values
INFO key
for help in plain text
CLEAR key
to delete inputs
ENTER key MEAS key
to accept to return to
input values measurement mode
Options
Gas path 19" rack unit Field device Field device Ex
Flow indicator Measurement pipe Duran glass - -
Variable area Duran glass
Suspension boundary PTFE (Teflon)
Angle pieces FKM (e.g. Viton)
Pressure switch Membrane FKM (e.g. Viton) - -
Enclosure PA 6.3T
9 10 2 1 4 3
8
P 13
P 11 12
F
Gas path ULTRAMAT 6, single-channel unit, 19" unit, with flow-type reference cell (option)
&KDQQHO &KDQQHO
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3
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Gas path ULTRAMAT 6, field unit, with flow-type reference cell (option)
■ Function
1
Principle of operation
The ULTRAMAT 6 gas analyzer operates according to the infra-
red two-beam alternating light principle with double-layer detec- 1
tor and optical coupler.
2
The measuring principle is based on the molecule-specific
absorption of bands of infrared radiation. The absorbed wave-
lengths are characteristic to the individual gases, but may par-
tially overlap. This results in cross-sensitivities which are re-
duced to a minimum in the ULTRAMAT 6 gas analyzers by the
following measures: 3
• Gas-filled filter cell (beam divider) 4
• Double-layer detector with optical coupler
• Optical filters if necessary
The figure shows the measuring principle. An IR source (1)
which is heated to approx. 700 ºC and which can be shifted to
balance the system is divided by the beam divider (3) into two 5
equal beams (sample and reference beams). The beam divider
also acts as a filter cell. 6
The reference beam passes through a reference cell (8) filled
with N2 (a non-infrared-active gas) and reaches the right-hand
side of the detector (11) practically unattenuated. The sample
beam passes through the sample chamber (7) through which
the sample gas flows and reaches the left-hand side of the de- 7 8
tector (10) attenuated to a lesser or greater extent depending on
the concentration of the sample gas. The detector is filled with a
defined concentration of the gas component to be measured.
The detector is designed as a double-layer detector. The center
of the absorption band is preferentially absorbed in the upper
detector layer, the edges of the band are absorbed to approxi- 9
mately the same extent in the upper and lower layers. The upper
and lower detector layers are connected together via the micro-
flow sensor (12). This coupling means that the spectral sensitiv-
ity has a very narrow band. 10 11
The optical coupler (13) lengthens the lower receiver cell layer 12
optically. The infrared absorption in the second detector layer is
varied by changing the slider position (14). It is thus possible to
individually minimize the influence of interfering components.
A chopper (5) rotates between the beam divider and the sample
chamber and interrupts the two beams alternately and periodi-
cally. If absorption takes place in the sample chamber, a pulsat- 13
ing flow is generated between the two detector levels which is
converted by the microflow sensor (12) into an electric signal.
14
The microflow sensor consists of two nickel-plated grids heated
to approximately 120 ºC, which, along with two supplementary
resistors, form a Wheatstone bridge. The pulsating flow together
1 IR source, adjustable 8 Reference cell
with the dense arrangement of the Ni grids causes a change in
resistance. This leads to an offset in the bridge, which is depen- 2 Optical filter 9 Sample gas outlet
dent on the concentration of the sample gas. 3 Beam divider 10 Detector, meas. side
4 Eddy current drive 11 Detector, reference side
Notes 5 Chopper 12 Microflow sensor
The sample gases must be fed into the analyzers free of dust. 6 Sample gas inlet 13 Optical coupler
Condensation should be prevented from occurring in the sample 7 Sample cell 14 Slider, adjustable
chambers. Therefore, the use of gas modified for the measuring
task is necessary in most application cases.
ULTRAMAT 6, principle of operation
As far as possible, the ambient air of the analyzer should not
have a large concentration of the gas components to be mea- Channels with electronically suppressed zero point only differ
sured. from the standard version in the measuring range parameteriza-
tion.
Flow-type reference sides with reduced flow must not be oper-
ated with flammable or toxic gases. Physically suppressed zeros can be provided as a special ap-
plication.
Flow-type reference sides with reduced flow and an O2 content
> 70 % may only be used together with Y02 (Clean for O2).
■ Technical specifications
1
General information Pressure correction range
Measuring ranges 4, internally and externally switch- Pressure sensor
able; autoranging is also possible • Internal 700 … 1 200 hPa absolute
Smallest possible measuring range Dependent on the application: • External 700 … 1 500 hPa absolute
e.g. CO: 0 … 10 vpm,
CO2: 0 … 5 vpm Measuring response (relating to sample gas pressure 1 013 hPa
absolute, 0.5 l/min sample gas flow and 25 °C ambient temperature)
Largest possible measuring span Dependent on the application
Output signal fluctuation < 1 % of the smallest possible
Measuring range with suppressed Any zero point within measuring range according to
zero point 0 … 100 vol.% can be imple- rating plate
mented; smallest possible span
20 % Zero point drift < 1 % of the current measuring
range/week
Operating position Front wall, vertical
Measured-value drift < 1 % of the current measuring
Conformity CE mark in accordance with range/week
EN 50081-1, EN 50082-2
Repeatability 1 % of the current measuring
Influence of interfering gases must be considered separately range
Design, enclosure Detection limit 1 % of the smallest possible
Weight Approx. 15 kg measuring range
(with one IR channel) Linearity error < 0.5 % of the full-scale value
Approx. 21 kg
(with two IR channels) Influencing variables (relating to sample gas pressure 1 013 hPa
absolute, 0.5 l/min sample gas flow and 25 °C ambient temperature)
Degree of protection IP20 according to EN 60529
Ambient temperature < 1 % of current measuring
Electrical characteristics range/10 K (with constant
EMC In accordance with standard receiver cell temperature)
(Electromagnetic Compatibility) requirements of NAMUR NE21 Sample gas pressure • When pressure compensation
(08/98) has been switched on: < 0.15 %
Electrical safety According to EN 61010-1, of the span/1 % change in atmo-
overvoltage category III spheric pressure
Power supply 100 … 120 V AC (nominal range • When pressure compensation
of use 90 … 132 V), 48 … 63 Hz has been switched off: < 1.5 %
or of the span/1 % change in atmo-
200 … 240 V AC (nominal range spheric pressure
of use 180 … 264 V), 48 … 63 Hz Sample gas flow Negligible
Power consumption 1-channel unit: Approx. 40 VA Power supply < 0.1 % of the current measuring
2-channel unit: Approx. 70 VA range with rated voltage 10 %
Fuse values Environmental conditions Application-specific measuring
• 100 ... 120 V 1 T/250 (7MB2121) influences possible if ambient air
1.6 T/250 (7MB2123) contains measured components or
cross interference-sensitive gases
• 200 ... 240 V 0.63 T/250 (7MB2121)
1 T/250 (7MB2123) Electrical inputs and outputs
Pipe made of titanium Tantalum Non-flow-type 4 4 A20, A21, A40, A41, Y02
Tantalum Flow-type 5 5 Y02
Stainless steel pipe Aluminum Non-flow-type 6 6 A20, A21, A40, A41
(mat. no. 1.4571) Tantalum Non-flow-type 8 8 A20, A21, A40, A41
Add-on electronics
Without 0
AUTOCAL function
• With 8 additional digital inputs/outputs each for channel 1 1
• With 8 additional digital inputs/outputs each for channel 1 and channel 2 2 2
• With serial interface for the automotive industry (AK), channel 1 3 3 E20
• With serial interface for the automotive industry (AK), 4 4 E20
channel 1 and channel 2
• With 8 additional digital inputs/outputs for channel 1 5
and PROFIBUS PA interface
• With 8 additional digital inputs/outputs each for channel 1 and channel 2 6 6
and PROFIBUS PA interface
• With 8 additional digital inputs/outputs for channel 1 7
and PROFIBUS DP interface
• With 8 additional digital inputs/outputs each for channel 1 and channel 2 8 8
and PROFIBUS DP interface
1)
Only for cell length 20 to 180 mm
■ Dimensional drawings
1
s
8/75$0$7
0
M 5 GND
GND 9 R_Level-N-
4 NC It is possible to connect
8 RD/TD-N bus terminating resistors
3 RD/TD-P to pins 7 and 9.
+5 V 7 R_Level-P-
2 NC
6 NC
M 1 GND
M 8 GND
15 Analog output 2-P For 2-component version only
7 Analog output 2-N of the ULTRAMAT part
14 Analog output 1-P Analog outputs isolated
6 Analog output 1-N (also from each other), RL: ≤ 750 Ω
13 NC
5 NC
12 Pressure correction Analog inputs
Analog input 2-P non-isolated,
M 4 Analog input 2-N Pressure correction
0 ... 20 mA/500 Ω
11 Analog input 1-P Correction of cross-interference or 0 ... 10 V
M 3 Analog input 1-N Correction of cross-interference (low-resistance)
10 Binary input 6-P Isolated via optocoupler
2 Binary input 5-P "0" = 0 V (0 ... 4.5 V)
9 Binary input 5 to 6-N "1" = 24 V (13 ... 33 V)
M 1 GND
M 13 GND
25 Binary input 4-P Isolated via optocoupler
12 Binary input 3-P "0" = 0 V (0 ... 4.5 V)
24 Binary input 2-P "1" = 24 V (13 ... 33 V)
11 Binary input 1-P
23 Binary input 1 to 4-N
10
22 Relay 6
9
21
8 Relay 5
20
7
19 Relay 4 Contact load
6 max. 24 V/1 A, AC/DC; relay
18 contacts shown: relay coil has
5 Relay 3 zero current
17
4
16 Relay 2
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2 Relay 1 PXVWEHVKLHOGHGDQGUHVWDJDLQVWWKH
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ULTRAMAT 6, 19“ unit, pin assignment of AUTOCAL board and PROFIBUS connectors
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ULTRAMAT 6, 19“ unit, gas and electrical connections (example: 2-channel version)
■ Technical specifications
1
General information Gas inlet conditions
Measuring ranges 4, internally and externally switch- Permissible sample gas pressure
able; autoranging is also possible • With hoses (without pressure 600 … 1 500 hPa (absolute)
Smallest possible measuring range Dependent on the application, switch)
e.g. CO: 0 … 10 vpm, • With pipes (without pressure 600 … 1 500 hPa (absolute)
CO2 : 0 … 5 vpm switch)
Largest possible measuring range Dependent on the application - Ex (leakage compensation) 600 … 1 160 hPa (absolute)
Measuring range with suppressed Any zero point within - Ex (continuous purging) 600 … 1 500 hPa (absolute)
zero point 0 … 100 vol.% can be
implemented; smallest possible Purging gas pressure
span 20 %
• Permanent < 165 hPa above ambient pres-
Heated version 65 °C sure
Operating position Front wall, vertical • For short periods 250 hPa above ambient pressure
Conformity CE mark in accordance with Sample gas flow 18 … 90 l/h (0.3 … 1.5 l/min)
EN 50081-1, EN 50082-2
Sample gas temperature Min. 0 ... max. 50 °C, but above
Influence of interfering gases must be considered separately the dew point, for heated version
min. 0 … max. 80 °C
Design, enclosure
Sample gas humidity < 90 % RH (RH: relative humidity)
Weight Approx. 32 kg or dependent on measuring task
Degree of protection IP65 in accordance with Dynamic response
EN 60529, restricted breathing
enclosure to EN 50021 Warm-up period At room temperature < 30 min
(the technical specification will be
Electrical characteristics met after 2 hours)
Power supply 100 … 120 V AC (nominal range Delayed display (T90-time) Dependent on length of analyzer
of use 90 … 132 V), 48 … 63 Hz chamber, sample gas line and
or parameterizable damping
200 … 240 V AC (nominal range
of use 180 … 264 V), 48 … 63 Hz Damping (electrical time constant) 0 … 100 s, parameterizable
Power consumption Approx. 35 VA; approx. 330 VA Dead time (purging time of the gas Approximately 0.5 ... 5 s,
with heated version path in the unit at 1 l/min) depending on version
EMC In accordance with standard Time for device-internal signal pro- <1s
(Electromagnetic Compatibility) requirements of NAMUR NE21 cessing
(08/98) Pressure correction range
Electrical safety In accordance with EN 61010-1 Pressure sensor
• Heated units Overvoltage category II • Internal 700 … 1 200 hPa absolute
• Unheated units Overvoltage category III • External 700 … 1 500 hPa absolute
Fuse values (unheated unit) Measuring response (relating to sample gas pressure 1 013 hPa
• 100 ... 120 V F3: 1 T/250; F4: 1 T/250 absolute, 0.5 l/min sample gas flow and 25 °C ambient temperature)
• 200 ... 240 V F3: 0.63 T/250; F4: 0.63 T/250 Output signal fluctuation < 1 % of the smallest possible
measuring range according to
Fuse values (heated unit) rating plate
• 100 ... 120 V F1: 1 T/250; F2: 4 T/250 Zero point drift < 1 % of the current measuring
F3: 4 T/250; F4: 4 T/250 range/week
• 200 ... 240 V F1: 0.63 T/250; F2: 2.5 T/250 Measured-value drift < 1 % of the current measuring
F3: 2.5 T/250; F4: 2.5 T/250 range/week
Repeatability 1 % of the current measuring
range
Detection limit 1 % of the smallest possible mea-
suring range
Linearity error < 0.5 % of the full-scale value
Add-on electronics
Without 0
AUTOCAL function
• With 8 additional digital inputs/outputs 1
• With 8 digital inputs/outputs and PROFIBUS PA interface 6 6 E12
• With 8 digital inputs/outputs and PROFIBUS DP interface 7 7 E12
• With 8 digital inputs/outputs and PROFIBUS PA Ex i 8 8
Power supply
Standard unit and acc. to ATEX II 3G version (Zone 2)
• 100 ... 120 V AC, 48 ... 63 Hz 0 0
• 200 ... 240 V AC, 48 ... 63 Hz 1 1
ATEX II 2G versions (Zone 1), incl. certificate
• 100 ... 120 V AC, 48 ... 63 Hz, according to ATEX II 2G2) 2 2 2
(operating mode: leakage compensation)
• 200 ... 240 V AC, 48 ... 63 Hz, according to ATEX II 2G2) 3 3 3
(operating mode: leakage compensation)
• 100 ... 120 V AC, 48 ... 63 Hz, according to ATEX II 2G2) 6 6 6
(operating mode: continuous purging)
• 200 ... 240 V AC, 48 ... 63 Hz, according to ATEX II 2G2) 7 7 7
(operating mode: continuous purging)
Heating of internal gas paths and analyzer unit
Without A
With (max. 65 °C) B
Language (supplied documentation, software)
German 0
English 1
French 2
Spanish 3
Italian 4
1)
Only for cell length 20 to 180 mm
2)
Only in connection with an approved purging unit
■ Dimensional drawings
1
148
184
250
259
394
418
112
20
42
77
0
271
253
237
222
201
127
65
58
438 311
328 26.5 20
14
s ULTRAMAT 6
440
480
14
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ULTRAMAT 6, field device, pin and terminal assignment of the AUTOCAL board and PROFIBUS connectors
a b c d 7
5
1 3
9
2 4
8
6
Documentation
7MB-2111/2 Ex
Description 2 years 5 years Article No.
(quantity) (quantity)
7MB-2121
7MB-2123
7MB-2124
7MB-2111
7MB-2112
Analyzer unit
O-ring for cover (window) x x x x x x 2 4 C79121-Z100-A24
Cover (cell length 20 ... 180 mm) x x x x x x 2 2 C79451-A3462-B151
Cover (cell length 0.2 ... 6 mm) x x x x x x 2 2 C79451-A3462-B152
O-rings, set x x x x x x 1 C79451-A3462-D501
Sample gas path
O-ring (hose clip) x x x 2 4 C71121-Z100-A159
Pressure switch x x x 1 2 C79302-Z1210-A2
Flow indicator x x x 1 2 C79402-Z560-T1
Hose clip x x x x x x 1 C79451-A3478-C9
Heating cartridge (heated unit) x x x 1 W75083-A1004-F120
Electronics
Temperature fuse (heated unit) x x 1 W75054-T1001-A150
Fuse (device fuse) x 1 2 A5E00061505
Temperature controller - x x x 1 A5E00118527
electronics, 230 V AC
Temperature controller - x x x 1 A5E00118530
electronics, 115 V AC
Fan, 24 V DC (heated unit) x x x 1 A5E00302916
Front plate with keyboard x x x 1 1 C79165-A3042-B504
Temperature sensor x x x 1 C79165-A3044-B176
Adapter plate, LCD/keyboard x x x x x 1 1 C79451-A3474-B605
Motherboard, with firmware: see x x x x x x 1
spare parts list
LC display x x x x x 1 1 W75025-B5001-B1
Connector filter x x x x x 1 W75041-E5602-K2
Fusible element, T 0.63 A/250 V x x x x x 2 3 W79054-L1010-T630
Fusible element, T 1 A/250 V x x x x x x 2 3 W79054-L1011-T100
Fusible element, T 1.6 A/250 V x x 2 3 W79054-L1011-T160
Fusible element, T 2.5 A/250 V x x x 2 3 W79054-L1011-T250
If the ULTRAMAT 6 is supplied with a specially cleaned gas path for high oxygen content ("Cleaned for O2 service"), please ensure
that you specify this when ordering spare parts. This is the only way to guarantee that the gas path will continue to comply with the
special requirements for this version.
INFO key
for help in plain text
CLEAR key
to delete inputs
ENTER key MEAS key
to accept to return to
input values measurement mode
Options
Gas path ULTRAMAT channel 19" rack unit
Flow indicator Measurement pipe Duran glass
Variable area Duran glass
Suspension boundary PTFE (Teflon)
Angle pieces FKM (e.g. Viton)
Pressure switch Membrane FKM (e.g. Viton)
Enclosure PA 6.3T
Options
Gas path ULTRAMAT channel 19" rack unit
and OXYMAT channel
Flow indicator Measurement pipe Duran glass
Variable area Duran glass
Suspension boundary PTFE (Teflon)
Angle pieces FKM (e.g. Viton)
Pressure switch Membrane FKM (e.g. Viton)
Enclosure PA 6.3T
9 10 5 6 1 2 4
17
18 P
11
P
13
12
16
P P
14 14
P 13
F F
15 15
ULTRAMAT/OXYMAT 6, gas path (example) IR channel without flow-type reference side
9 10 5 6 8 7 1 2 4
17
18 P
11
P
13
12
16
P P
14 14
P 13
F F
15 15
ULTRAMAT/OXYMAT 6, gas path (example) IR channel with flow-type reference side
■ Function
1
Principle of operation, ULTRAMAT channel
The ULTRAMAT channel operates according to the infrared two-
beam alternating light principle with double-layer detector and 1
optical coupler.
2
The measuring principle is based on the molecule-specific ab-
sorption of bands of infrared radiation. The absorbed wave-
lengths are characteristic to the individual gases, but may par-
tially overlap. This results in cross-sensitivities which are
reduced to a minimum by the following measures:
3
• Gas-filled filter cell (beam divider)
4
• Double-layer detector with optical coupler
• Optical filters if necessary
The figure shows the measuring principle. An IR source (1)
which is heated to approx. 700 ºC and which can be shifted to
balance the system is divided by the beam divider (3) into two
equal beams (sample and reference beams). The beam divider 5
also acts as a filter cell.
6
The reference beam passes through a reference cell (8) filled
with N2 (a non-infrared-active gas) and reaches the right-hand
side of the detector (11) practically unattenuated. The sample
beam passes through the sample chamber (7) through which
the sample gas flows and reaches the left-hand side of the de-
tector (10) attenuated to a lesser or greater extent depending on 7 8
the concentration of the sample gas. The detector is filled with a
defined concentration of the gas component to be measured.
The detector is designed as a double-layer detector. The center
of the absorption band is preferentially absorbed in the upper
detector layer, the edges of the band are absorbed to approxi-
mately the same extent in the upper and lower layers. The upper 9
and lower detector layers are connected together via the micro-
flow sensor (12). This coupling means that the spectral sensitiv-
ity has a very narrow band.
The optical coupler (13) lengthens the lower receiver cell layer 10 11
optically. The infrared absorption in the second detector layer is 12
varied by changing the slider position (14). It is thus possible to
individually minimize the influence of interfering components.
A chopper (5) rotates between the beam divider and the sample
chamber and interrupts the two beams alternately and periodi-
cally. If absorption takes place in the sample chamber, a pulsat-
ing flow is generated between the two detector levels which is 13
converted by the microflow sensor (12) into an electric signal.
The microflow sensor consists of two nickel-plated grids heated
14
to approximately 120 ºC, which, along with two supplementary
resistors, form a Wheatstone bridge. The pulsating flow together
with the dense arrangement of the Ni grids causes a change in
1 IR source, adjustable 8 Reference cell
resistance. This leads to an offset in the bridge, which is depen-
dent on the concentration of the sample gas. 2 Optical filter 9 Sample gas outlet
3 Beam divider 10 Detector, meas. side
Note 4 Eddy current drive 11 Detector, reference side
The sample gases must be fed into the analyzers free of dust. 5 Chopper 12 Microflow sensor
Condensation should be prevented from occurring in the sample 6 Sample gas inlet 13 Optical coupler
chambers. Therefore, the use of gas modified for the measuring 7 Sample cell 14 Slider, adjustable
task is necessary in most application cases.
ULTRAMAT channel, principle of operation
As far as possible, the ambient air of the analyzer should not
have a large concentration of the gas components to be mea- Channels with electronically suppressed zero point only differ
sured. from the standard version in the measuring range parameteriza-
tion.
Flow-type reference sides with reduced flow must not be oper-
ated with flammable or toxic gases. Physically suppressed zeros can be provided as a special ap-
plication.
Flow-type reference sides with reduced flow and an O2 content
> 70 % may only be used together with Y02.
■ Technical specifications
1
ULTRAMAT/OXYMAT 6, 19" rack unit Technical data, ULTRAMAT channel
General information Measuring ranges 4, internally and externally switch-
able; autoranging is also possible
Operating position Front wall, vertical
Smallest possible measuring range Dependent on the application,
Conformity CE mark in accordance with e.g.
EN 50081-1, EN 50082-2 CO: 0 ... 10 vpm
Design, enclosure CO2: 0 ... 5 vpm
Weight Approx. 21 kg Largest possible measuring range Dependent on the application
Degree of protection IP20 according to EN 60529 Measuring ranges with suppressed Any zero point within 0 ... 100
zero point vol.% can be implemented; small-
Electrical characteristics est possible span 20 %
EMC In accordance with standard Characteristic Linearized
(Electromagnetic Compatibility) requirements of NAMUR NE21
(08/98) Influence of interfering gases must be considered separately
Electrical safety According to EN 61010-1, Gas inlet conditions
overvoltage category III Permissible sample gas pressure
Power supply 100 ... 120 V AC (nominal range • Without pressure switch 700 ... 1 500 hPa (absolute)
of use 90 ... 132 V), 48 ... 63 Hz or
200 ... 240 V AC (nominal range • With integrated pressure switch 700 ... 1 300 hPa (absolute)
of use 180 ... 264 V), 48 ... 63 Hz
Sample gas flow 18 ... 90 l/h (0.3 ... 1.5 l/min)
Power consumption Approx. 70 VA
Sample gas temperature Min. 0 to max. 50 °C, but above
Fuse values 120 ... 120 V: F1/F2 = T 1.6 A the dew point
200 ... 240 V: F1/F2 = T 1 A
Sample gas humidity < 90 % (relative humidity), or
Electrical inputs and outputs (per channel) dependent on measuring task,
non-condensing
Analog output 0/2/4 ... 20 mA, isolated;
max. load 750 Dynamic response
Relay outputs 6, with changeover contacts, Warm-up period At room temperature < 30 min
freely parameterizable, e.g. for (the technical specification will be
measuring range identification; met after 2 hours)
load: 24 V AC/DC/1 A, isolated,
non-sparking Delayed display (T90-time) Dependent on length of analyzer
chamber, sample gas line and
Analog inputs 2, dimensioned for parameterizable damping
0/2/4 … 20 mA for external pres-
sure sensor and correction of Damping (electrical time constant) 0 ... 100 s, parameterizable
influence of accompanying gas Dead time (purging time of the gas Approx. 0.5 ... 5 s, depending on
(correction of cross-interference) path in the unit at 1 l/min) version
Binary inputs 6, designed for 24 V, isolated, Time for device-internal signal <1s
freely parameterizable, e.g. for processing
measuring range switchover
Pressure correction range
Serial interface RS 485
Pressure sensor
Options AUTOCAL function each with
8 additional binary inputs and • Internal 700 ... 1 200 hPa absolute
relay outputs, also with • External 700 ... 1 500 hPa absolute
PROFIBUS PA or PROFIBUS DP
Measuring response (relating to sample gas pressure 1 013 hPa
Climatic conditions absolute, 0.5 l/min sample gas flow and 25 °C ambient temperature)
Permissible ambient temperature -30 ... +70 °C during storage and Output signal fluctuation < 1 % of the smallest possible
transportation, 5 … 45 °C during measuring range according to
operation rating plate
Permissible humidity < 90 % relative humidity, during Zero point drift < 1 % of the current measuring
storage and transportation (dew range/week
point must not be undershot)
Measured-value drift < 1 % of the current measuring
range/week
Repeatability 1 % of the current measuring
range
Detection limit 1 % of the smallest possible
measuring range
Linearity error < 0.5 % of the full-scale value
Add-on electronics
Without 0
AUTOCAL function
• With 8 additional digital inputs and outputs for OXYMAT channel 1
• With 8 additional digital inputs and outputs for ULTRAMAT channel 2
• With 8 additional digital inputs and 8 additional digital outputs for 3
ULTRAMAT channel and OXYMAT channel
• With serial interface for the automotive industry (AK) 5 5 Y02
• With 8 additional digital inputs/outputs 6
and PROFIBUS PA interface for
ULTRAMAT channel and OXYMAT channel
• With 8 additional digital inputs/outputs 7
and PROFIBUS DP interface for
ULTRAMAT channel and OXYMAT channel
Power supply
100 ... 120 V AC, 48 ... 63 Hz 0
200 ... 240 V AC, 48 ... 63 Hz 1
Footnotes, see next page
Add-on electronics
Without 0
AUTOCAL function
• With 8 additional digital inputs and outputs for 1
ULTRAMAT channel and OXYMAT channel
• With serial interface for the automotive industry (AK) 5 5 Y02
• With 8 additional digital inputs/outputs and PROFIBUS PA interface for 6
ULTRAMAT channel and OXYMAT channel
• With 8 additional digital inputs/outputs and PROFIBUS DP interface for 7
ULTRAMAT channel and OXYMAT channel
Power supply
100 ... 120 V AC, 48 ... 63 Hz 0
200 ... 240 V AC, 48 ... 63 Hz 1
Footnote, see next page
s
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■ Schematics
1
Pin assignment (electrical and gas connections)
M 5 GND
GND 9 R_Level-N-
4 NC It is possible to connect
8 RD/TD-N bus terminating resistors
3 RD/TD-P to pins 7 and 9.
+5 V 7 R_Level-P-
2 NC
6 NC
M 1 GND
M 8 GND
15 Analog output 2-P For 2-component version only
7 Analog output 2-N of the ULTRAMAT part
14 Analog output 1-P Analog outputs isolated
6 Analog output 1-N (also from each other), RL: ≤ 750 Ω
13 NC
5 NC
12 Pressure correction Analog inputs
Analog input 2-P non-isolated,
M 4 Analog input 2-N Pressure correction
0 ... 20 mA/500 Ω
11 Analog input 1-P Correction of cross-interference or 0 ... 10 V
M 3 Analog input 1-N Correction of cross-interference (low-resistance)
10 Binary input 6-P Isolated via optocoupler
2 Binary input 5-P "0" = 0 V (0 ... 4.5 V)
9 Binary input 5 to 6-N "1" = 24 V (13 ... 33 V)
M 1 GND
M 13 GND
25 Binary input 4-P Isolated via optocoupler
12 Binary input 3-P "0" = 0 V (0 ... 4.5 V)
24 Binary input 2-P "1" = 24 V (13 ... 33 V)
11 Binary input 1-P
23 Binary input 1 to 4-N
10
22 Relay 6
9
21
8 Relay 5
20
7
19 Relay 4 Contact load
6 max. 24 V/1 A, AC/DC; relay
18 contacts shown: relay coil has
5 Relay 3 zero current
17
4
16 Relay 2
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M 1 GND
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ULTRAMAT/OXYMAT 6, 19“ unit, pin assignment of AUTOCAL board and PROFIBUS connectors
Sample gas outlet Sample gas inlet Reference gas outlet 15-pin connector: 9-pin
binary inputs and connector:
Reference Reference Sample Sample analog inputs/outputs RS 485
gas inlet gas inlet gas outlet gas inlet
4 2 1 8 7 6 5 Purging gas
inlet
9-pin interface
connector
(option): e.g.
PROFIBUS
37-pin connector:
binary inputs
and
relay outputs
(optional board)
Power supply
and miniature
fuses
25-pin connector:
binary inputs and
relay outputs
Gas connections: stubs 6 mm or ¼"
Documentation
If the device was supplied with a specially cleaned gas path for high oxygen context ("Clean for O2 service"), please ensure that you
specify this when ordering spare parts. This is the only way to guarantee that the gas path will continue to comply with the special
requirements for this version.
■ Design
19" rack unit
• With 4 HU for installation
- in hinged frame
- in cabinets with or without telescopic rails
• Front plate can be swung down for servicing purposes
(laptop connection)
The function of the OXYMAT 6 gas analyzers is based on the • Internal gas paths: hose made of FKM (Viton) or pipe made of
paramagnetic alternating pressure method and are used to titanium or stainless steel (mat. no. 1.4571)
measure oxygen in gases.
• Gas connections for sample gas inlet and outlet and for refer-
ence gas: fittings, pipe diameter of 6 mm or ¼"
■ Benefits • Flow indicator for sample gas on front plate (option)
• Paramagnetic alternating pressure principle • Pressure switch in sample gas path for flow monitoring
- Small measuring ranges (0 to 0.5 % or 99.5 to 100 % O2) (option)
- Absolute linearity
• Detector element has no contact with the sample gas Field device
- Can be used under harsh conditions • Two-door enclosure with gas-tight separation of analyzer and
- Long service life electronics sections
• Physically suppressed zero through suitable selection of • Each half of the enclosure can be purged separately
reference gas (air or O2), e.g. 98 to 100 % O2 for purity moni- • Analyzer unit and piping can be heated up to 130 °C (option)
toring/air separation
• Gas path and stubs made of stainless steel (mat. no. 1.4571)
• Open interface architecture (RS 485, RS 232, PROFIBUS) or titanium, Hastelloy C22
• SIPROM GA network for maintenance and service information • Purging gas connections: pipe diameter 10 mm or 3/8"
(option)
• Gas connections for sample gas inlet and outlet and for refer-
• Electronics and physics: gas-tight isolation, purging is possi- ence gas: clamping ring connection for a pipe diameter of
ble, IP65, long service life even in harsh environments (field 6 mm or ¼"
device only)
• Heated versions (option), use also in presence of gases con- Display and control panel
densing at low temperature (field device only) • Large LCD panel for simultaneous display of:
• EEx(p) for zones 1 and 2 according to ATEX 2G and ATEX 3G - Measured value (digital and analog displays)
(field device only) - Status bar
- Measuring ranges
■ Application • Contrast of LCD panel adjustable using menu
• Permanent LED backlighting
Fields of application • Washable membrane keyboard with five softkeys
• For boiler control in incineration plants • Menu-driven operation for parameterization, test functions,
• For safety-relevant applications (SIL) adjustment
• In the automotive industry (testbed systems) • User help in plain text
• In chemical plants • Graphic display of concentration trend; programmable time
• For ultra-pure gas quality monitoring intervals
• Environmental protection • Bilingual operating software German/English,
English/Spanish, French/English, Spanish/English,
• Quality monitoring Italian/English
• Versions for analyzing flammable and non-flammable gases
or vapors for use in hazardous areas
LED backlit graphic Status line for display Two code levels
display and of analyzer status according to NAMUR
membrane keyboard (programmable) (maintenance and
with noticeable click specialist level)
Display of
concentrations as
numbers and bargraph Display of current
measuring ranges
Display of
start-of-scale and
full-scale values
ESC key
to abort inputs
Keyboard to
enter values
INFO key
for help in plain text
CLEAR key
to delete inputs
ENTER key MEAS key
to accept to return to
input values measurement mode
Options
Flow indicator Measurement pipe Duran glass - -
Variable area Duran glass, black
Suspension boundary PTFE (Teflon)
Angle pieces FKM (Viton)
Pressure switch Membrane FKM (Viton) - -
Enclosure PA 6.3 T
)
3
3
F
6 P
13 7 8
P
11
4
5
12
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10
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■ Technical specifications
1
General information Dynamic response
Measuring ranges 4, internally and externally switch- Warm-up period At room temperature < 30 min
able; autoranging is also possible (the technical specification will be
met after 2 hours)
Smallest possible span (relating to 0.5 vol.%, 2 vol.% or 5 vol.% O2
sample gas pressure 1 000 hPa Delayed display (T90-time) Min. 1.5 … 3.5 s, depending on
absolute, 0.5 l/min sample gas flow version
and 25 °C ambient temperature) Damping (electrical time constant) 0 … 100 s, parameterizable
Largest possible measuring span 100 vol.% O2 (for a pressure Dead time (purging time of the gas Approximately 0.5 ... 2.5 s,
above 2 000 hPa: 25 vol.% O2) path in the unit at 1 l/min) depending on version
Measuring ranges with suppressed Any zero point can be imple- Time for device-internal signal <1s
zero point mented within 0 … 100 vol.%, processing
provided that a suitable reference
gas is used (see Table 1 in Pressure correction range
"Function")
Pressure sensor
Operating position Front wall, vertical
• Internal 500 … 2 000 hPa absolute
Conformity CE mark in accordance with
• External 500 … 3 000 hPa absolute
EN 50081-1, EN 50082-2
Measuring response (relating to sample gas pressure 1 013 hPa
Design, enclosure
absolute, 0.5 l/min sample gas flow and 25 °C ambient temperature)
Degree of protection IP20 according to EN 60529
Output signal fluctuation < 0.75 % of the smallest possi-
Weight Approx. 13 kg ble measuring range according to
rating plate, with electronic
Electrical characteristics damping constant of 1 s (corre-
Power supply 100 … 120 V AC (nominal range sponds to 0.25 % at 2 )
of use 90 … 132 V), 48 … 63 Hz Zero point drift < 0.5 %/month of the smallest
or 200 … 240 V AC (nominal possible span according to rating
range of use 180 … 264 V), plate
48 … 63 Hz
Measured-value drift < 0.5 %/month of the current
Power consumption Approx. 35 VA measuring range
EMC In accordance with standard Repeatability < 1 % of the current measuring
(Electromagnetic Compatibility) requirements of NAMUR NE21 range
(08/98), EN 61326
Detection limit 1 % of the current measuring
Electrical safety According to EN 61010-1, range
overvoltage category III
Linearity error < 0.1 % of the current measuring
Fuse values 100 ... 120 V: 1.0 T/250 range
200 ... 240 V: 0.63 T/250
Influencing variables (relating to sample gas pressure 1 013 hPa
Gas inlet conditions absolute, 0.5 l/min sample gas flow and 25 °C ambient temperature)
Permissible sample gas pressure Ambient temperature < 0.5 %/10 K relating to the small-
est possible measuring range
• With pipes 500 … 3 000 hPa absolute according to rating plate, with
• With hoses measuring span 0.5 %: 1 %/10 K
- Without pressure switch 500 … 1 500 hPa absolute Sample gas pressure (with air • When pressure compensation is
(100 hPa) as reference gas, correc- switched off: < 2 % of the current
- With pressure switch 500 … 1 300 hPa absolute tion of the atmospheric pressure measuring range/1 % pressure
Sample gas flow 18 … 60 l/h (0.3 … 1 l/min) fluctuations is only possible if the change
sample gas can vent to ambient air) • When pressure compensation is
Sample gas temperature Min. 0 ... max. 50 °C, but above switched on: < 0.2 % of the cur-
the dew point rent measuring range/1 % pres-
Sample gas humidity < 90 % RH (RH: relative humidity) sure change
Reference gas pressure 2 000 ... 4 000 hPa above sample Carrier gases Deviation from zero point corre-
(high-pressure version) gas pressure, but max. 5 000 hPa sponding to paramagnetic or dia-
magnetic deviation of carrier gas
Reference gas pressure Min. 100 hPa above sample gas
(low-pressure version) pressure Sample gas flow at zero point < 1 % of the current measuring
range according to rating plate
with a change in flow of 0.1 l/min
within the permissible flow range
Power supply < 0.1 % of the current measuring
range with rated voltage 10 %
■ Dimensional drawings
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■ Schematics
1
Pin assignment (electrical and gas connections)
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OXYMAT 6, 19“ unit, pin assignment of AUTOCAL board and PROFIBUS connectors
4 2 1 Purging gas
inlet
9-pin
interface
connector
(option): e.g.
PROFIBUS
Power supply
and fuses
37-pin connector
Binary inputs and
relay outputs (option)
25-pin connector
Binary inputs and
Gas connections: stubs 6 mm or ¼" relay outputs
º
s &$/20$7
■ Schematics
1
Pin assignment (electrical and gas connections)
&RQQHFWRU68%')56
0 *1'
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1&
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OXYMAT 6, field unit, connector and terminal assignment of the AUTOCAL board and PROFIBUS connectors
2 4
8
6
Documentation
If the OXYMAT 6 was supplied with a specially cleaned gas path for high oxygen context ("Clean for O2 service"), please ensure that
you specify this when ordering spare parts. This is the only way to guarantee that the gas path will continue to comply with the special
requirements for this version.
■ Overview ■ Design
1
• 19" rack unit with 4 HU for installation
- in hinged frame
- in cabinets with or without telescope rails
• Front plate can be swung down for servicing purposes
(laptop connection)
• Gas connections for sample gas inlet and outlet;
pipe diameter 6 mm or ¼"
• Gas and electrical connections at the rear
Display and control panel
• Large LCD field for simultaneous display of:
- Measured value
- Status bar
- Measuring ranges
• Contrast of LCD panel adjustable using menu
• Permanent LED backlighting
• Washable membrane keyboard with five softkeys
• Menu-driven operation for parameterization, test functions,
The measuring principle of the OXYMAT 61 gas analyzers is adjustment
based on the paramagnetic alternating pressure method and is
used to measure oxygen in gases in standard applications. • User help in plain text
• Graphic display of concentration trend; programmable time
■ Benefits intervals
• Bilingual operating software German/English, English/
• Integrated pump for reference gas (option, e.g. ambient air)
Spanish, French/English, Spanish/English, Italian/English
• High linearity
Input and outputs
• Compact design
• One analog output per medium (from 0, 2, 4 to 20 mA; NAMUR
• Physically suppressed zero possible
parameterizable)
Easy operation
menu controlusing
the softkeys
Display of
concentrations as
numbers and bargraph Display of current
measuring ranges
Display of
start-of-scale and
full-scale values
ESC key
to abort inputs
Keyboard to
enter values
INFO key
for help in plain text
CLEAR key
to delete inputs ENTER key MEAS key
to accept to return to
input values measurement mode
Options
Flow indicator Measurement pipe Duran glass
Variable area Duran glass, black
Suspension boundary PTFE (Teflon)
Angle pieces FKM (Viton)
Pressure switch Membrane FKM (Viton)
Enclosure PA 6.3 T
F
14 7 P
8
3
15
6 2
10
4
5
12 13
P
11
Gas path OXYMAT 61 with integrated reference gas pump (connection for 1 100 hPa, absolute)
F
14 7 P
8
3
15
6 2
4
5
13
Gas path OXYMAT 61 with reference gas connection 3 000 to 5 000 hPa, absolute
Table 1: Zero error due to diamagnetism or paramagnetism of some accompanying gases with nitrogen as the reference gas at 60 °C and 1 000 hPa
absolute (according to IEC 1207/3)
Conversion to other temperatures:
The deviations from the zero point listed in Table 1 must be multiplied by a correction factor (k):
• with diamagnetic gases: k = 333 K / ( [°C] + 273 K)
• with paramagnetic gases: k = [333 K / ( [°C] + 273 K)]2
(all diamagnetic gases have a negative deviationfrom zero point)
Reference gases
Measuring range Recommended reference gas Reference gas connection pressure Remarks
0 to … vol.% O2 N2 2 000 … 4 000 hPa above sample gas The reference gas flow is set
pressure (max. 5 000 hPa absolute) automatically to 5 … 10 ml/min
... to 100 vol.% O2 (suppressed O2
zero point with full-scale value
100 vol.% O2)
Around 21 vol.% O2 (suppressed Air Atmospheric pressure with internal
zero point with 21 vol.% O2 within reference gas pump
the measuring span)
Weight Approx. 13 kg Influencing variable (relating to sample gas pressure 1 013 hPa
absolute, 0.5 l/min sample gas flow and 25 °C ambient temperature)
Electrical characteristics
Ambient temperature < 2 %/10 K with span 5 %
Power supply 100 … 120 V AC (nominal range
of use 90 … 132 V), 48 … 63 Hz Sample gas pressure (with air • When pressure compensation
or 200 … 240 V AC (nominal (100 hPa) as internal reference gas has been switched off: < 2 % of
range of use 180 … 264 V), supply, correction of the atmo- the current measuring
48 … 63 Hz spheric pressure fluctuations is only range/1 % pressure change
possible if the sample gas can vent • When pressure compensation
Power consumption Approx. 45 VA to ambient air.) has been switched on: < 0.2 %
EMC In accordance with standard of the current measuring
(Electromagnetic Compatibility) requirements of NAMUR NE21 range/1 % pressure change
(08/98) Accompanying gases Deviation from zero point corre-
Electrical safety According to EN 61010-1, sponding to paramagnetic or dia-
overvoltage category III magnetic deviation of
accompanying gas (see table)
Fuse values 100 ... 120 V: 1.0 T/250
Sample gas flow at zero point < 1 % of the current measuring
200 ... 240 V: 0.63 T/250 range according to rating plate
Gas inlet conditions with a change in flow of 0.1 l/min
within the permissible flow range
Permissible sample gas pressure
Power supply < 0.1 % of the current measuring
• External reference gas supply 800 … 1 200 hPa absolute range with rated voltage 10 %
• With integrated pump Atmospheric pressure 50 hPa Electrical inputs and outputs
Sample gas flow 18 … 60 l/h (0.3 … 1 l/min) Analog output 0/2/4 … 20 mA, isolated;
Sample gas temperature Min. 0 to max. 50 °C, but above max. load 750
the dew point Relay outputs 6, with changeover contacts,
Sample gas humidity < 90 % relative humidity freely parameterizable, e.g. for
measuring range identification;
Reference gas pressure (high-pres- 2 000 ... 4 000 hPa above sam- load: 24 V AC/DC/1 A, potential-
sure version) ple gas pressure, but max. free
5 000 hPa absolute (version
without reference gas pump) Analog inputs 2, dimensioned for
0/2/4 … 20 mA for external pres-
Reference gas pressure (low-pres- Min. 100 hPa above sample gas sure sensor and accompanying
sure version) with external pump pressure gas influence correction (correc-
tion of cross-interference)
Dynamic response
Binary inputs 6, designed for 24 V, isolated,
Warm-up period At room temperature < 30 min
freely parameterizable, e.g. for
(the technical specification will be
measuring range switchover
met after 2 hours)
Serial interface RS 485
Delayed display (T90) 3.5 s
Options AUTOCAL function with 8 addi-
Damping (electrical time constant) 0 … 100 s, parameterizable
tional binary inputs and relay out-
Dead time (purging time of the gas Approximately 0.5 ... 2.5 s, puts, also with PROFIBUS PA or
path in the unit at 1 l/min) depending on version PROFIBUS DP
Time for device-internal signal pro- <1s Climatic conditions
cessing
Permissible ambient temperature -30 … +70 °C during storage and
Pressure correction range transportation
5 … 45 °C during operation
Pressure sensor internal 500 … 2 000 hPa, absolute
(see gas inlet conditions for per- Permissible humidity < 90 % relative humidity as
missible sample gas pressure) annual average, during storage
and transportation (must not fall
below dew point)
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■ Schematics
1
Pin assignment (electrical connections)
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M 19 GND
37 NC
18 NC
36 Binary input 14-P
17 Binary input 13-P
35 Binary input 12-P Isolated
16 Binary input 11-P via optocoupler
34 Binary input 10-P "0" = 0 V (0 ... 4.5 V)
15 Binary input 9-P "1" = 24 V (13 ... 33 V)
33 Binary input 8-P
14 Binary input 7-P
32 Binary input 7 to 14-N
13
31 Relay 14
12
30
11 Relay 13
29
10
28 Relay 12
9
27 Contact load
8 Relay 11 max. 24 V/1 A, AD/DC
26
7 for shown
25 Relay 10 relay contact position,
6 the relay has zero current
24
5 Relay 9
23
4
22 Relay 8
3
21
2 Relay 7
20
M 1 GND
5 DGND 5
9 CNTR-N 9
4 CNTR-P/direction control 4
8 RxD/TxD-N (A) 8 PA-N(-)
3 RxD/TxD-P (B) 3 PA-P(+)
7 7
2 2
6 VP /+ 5 V 6
1 1
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OXYMAT 61, 19“ unit, pin assignment of the AUTOCAL board and PROFIBUS connectors
4 2 1 Purging gas
inlet
9-pin interface
connector
(option):
e.g. PROFIBUS
Power supply
and fuses
37-pin connector:
Binary inputs and
relay outputs (option)
25-pin connector:
Binary inputs and
relay outputs
Gas connections: stubs 6 mm or ¼"
Documentation
If the OXYMAT 61 was supplied with a specially cleaned gas path for high oxygen context ("Clean for O2 service"), please ensure
that you specify this when ordering spare parts. This is the only way to guarantee that the gas path will continue to comply with the
special requirements for this version.
■ Overview ■ Design
1
• 19" rack unit with 4 HU for installation
- in hinged frames
- in cabinets with or without telescopic rails
• Front plate for service purposes can be pivoted down
(laptop connection)
• Connections for sample gas
- Input: Clamping ring connection for a pipe diameter of 6 mm
or ¼"
- Output: Pipe connection with diameter 6 mm or ¼"
• High-pressure and low-pressure versions
• Catalytically active and inactive cell
Display and control panel
• Large LCD field for simultaneous display of
- Measured value
- Status bar
- Measuring ranges
• Contrast of the LCD field adjustable via the menu
The OXYMAT 64 gas analyzer is used for the trace measurement • Permanent LED backlighting
of oxygen.
• Washable membrane keyboard with five softkeys
■ Benefits • Five-digit measured-value display
(decimal point counts as one digit)
• High linearity • Menu-driven operation for parameterization, configuration,
• Compact design test functions, adjustment
• Open interface architecture (RS 485, RS 232, PROFIBUS) • Operator support in plain text
• SIPROM GA network for maintenance and service information • Graphical display of the concentration progression; time inter-
(option) vals parameterizable
• Bilingual operating software German/English,
■ Application English/Spanish, French/English, Spanish/English,
• Production of technical gases Italian/English
- Measurements in N2 and CO2 • Switchover from ppm measuring range to % measuring range
• Welding Inputs and outputs
- Measurements in protective gases during welding of highly
alloyed steels, titanium, etc. • One analog output per medium (from 0, 2, 4 to 20 mA; NAMUR
parameterizable)
• Systems for air separation
- Measurements in N2 and in inert gases (e.g. Ne, Ar) • Six binary inputs freely configurable (e.g. for measurement
- Measurements in CO2 range switchover, processing of external signals from sample
preparation)
• Food production
- Measurement in CO2 (e.g. breweries) • Six relay outputs freely configurable (failure, maintenance re-
quest, maintenance switch, threshold alarm, external solenoid
• Electronics industry valves)
- Low-pressure version with pump
• Two analog inputs configurable (e.g. correction of cross-inter-
• Flow soldering systems ference, external pressure sensor)
• Extension with eight additional binary inputs and eight addi-
tional relay outputs, e.g. for autocalibration with up to four cal-
ibration gases
Communication
RS 485 present in basic unit (connection from the rear).
Options
• RS 485/RS 232 converter
• RS 485/Ethernet converter
• RS 485/USB converter
• Connection to networks via PROFIBUS DP/PA interface
• SIPROM GA software as the service and maintenance tool
Easy operation
menu controlusing
the softkeys
Display of
concentrations as
numbers and bargraph Display of current
measuring ranges
Display of
start-of-scale and
full-scale values
ESC key
to abort inputs
Keyboard to
enter values
INFO key
for help in plain text
CLEAR key
to delete inputs
9 1 2
10 10 4
O2 sensor
(KAZ /KIZ)
5 P 7
6
F
8
7 1 2
8
O2 sensor 3
(KAZ /KIZ)
4 P 5
F
6
9 1 2
Δp
8 4
6
F
The differences in concentration at each side means that a dif- The sample gas must be fed into the analyzer free of dust. Con-
ferential partial pressure prevails. Since ZrO2 conducts ions at densation should be avoided. Therefore, gas modified for the
650 °C, ionic migration takes place in the direction of the lower measuring tasks is necessary in most application cases.
partial pressure. Calibration
An oxygen gradient arises across the width of the ZrO2 mem- Calibration of the calibration point is carried out as with the other
brane, which, according to equation (1), results in an electrical analyzers of Series 6 after a maximum of 14 days by connecting
potential difference between the platinum electrodes. the calibration gas O2 in residual N2 at concentrations of approx.
Defects in the crystal lattice, caused by contamination of the 60 to 90 % of the master measuring range.
ZrO2 material with Y2O3 and/or CaO (introduced originally to Contrary to the other analyzers of Series 6, the zero point calibra-
prevent cracks forming in ceramic material) make it easier for O2 tion cannot be carried out using pure nitrogen, but with a "small"
ions to diffuse in the ZrO2 grid. concentration of oxygen in nitrogen appropriate to the selected
measuring range (e.g.: measuring range 0 to 10 vpm; calibration
Catalytically active ZrO2 sensor (CAZ) gas approx. 2 ppm O2 in residual N2).
The electrode material is made of platinum (Pt). This type of sen-
sor has a higher cross-sensitivity when flammable accompany- Essential characteristics
ing gas components are present. • Four measurement ranges freely parameterizable, all mea-
surement ranges linear
Catalytically inactive ZrO2 sensor (CIZ)
• Galvanically isolated measurement value output 0/2/4 through
The catalytically inactive sensor has the same general design as 20 mA (also inverted) and as per NAMUR
the CAZ. The contacts and electrode surface inside the pipe are • Autoranging selectable; possibility of remote switching
made of a specially developed material which largely prevents
catalytic oxidation except of H2, CO and CH4. • Storage of measured values possible during adjustments
• Wide range of selectable time constants (static/dynamic noise
suppression); i.e. the response time of the device can be
adapted to the respective measuring task
• Easy handling thanks to menu-driven operation
• Low long-term drift
• Two control levels with their own authorization codes for the
prevention of accidental and unauthorized operator interven-
tions
• Automatic, parameterizable measuring range calibration
• Operation based on the NAMUR recommendation
• Monitoring of the sample gas (via pressure switch)
• Customer-specific analyzer options such as:
- Customer acceptance
- TAG labels
- Drift recording
• Simple handling using a numerical membrane keyboard and
operator prompting
• Smallest span 0 to 10 vpm O2
• Largest span 0 to 100 % (testing with ambient air)
• Internal pressure sensor for correction of the influence of sam-
1 Pipe made of ZrO2 and Y2O3 or ple gas pressure fluctuations
ceramic CaO-mixed oxide
2 Ceramic protective coating
3 Sample electrode (Pt)
4 Reference electrode (Pt)
5 Thermoelement
6 Contact to reference electrode
7 Contact to sample electrode
Power consumption Approx. 37 VA • Catalytically active sensor (CAZ) Only gases with non-combustible
residual gas components can be
Fuse values 100 ... 120 V: 1.0T/250 introduced
200 ... 240 V: 0.63T/250 • Catalytically inactive sensor (CIZ) Residual gas concentration of
Gas inlet conditions 10 vpm H2; CO and CH4 have a
lower cross-interference; higher
Sample gas flow HCs are negligible
• through the sensor 7.5 l/h Sample gas flow < 2 % of the smallest possible
span with a change in flow of
• Overall consumption 15 ... 30 l/h
10 ml/min
Permissible sample gas pressure
Power supply < 0.1 % of the current measuring
• without internal pressure regulator 2 000 hPa (abs.) range with rated voltage 10 %
• with internal pressure regulator 2 000 ... 6 000 hPa (abs.) Electrical inputs and outputs
Sample gas temperature Min. 0 ... max. 50 °C, but above Analog output 0/2/4 ... 20 mA, 4 … 20 mA
the dew point (NAMUR), isolated; max. load
750
Sample gas humidity < 1 % relative humidity
Relay outputs 6, with changeover contacts, freely
Dynamic response parameterizable, e.g. for measur-
Warm-up period At room temperature < 30 min (the ing range identification;
technical specification will be met load: 24 V AC/DC/1 A, isolated
after 2 hours) Analog inputs 2, dimensioned for 0/2/4 … 20 mA
Damping (electrical time constant) 0 ... 100 s, parameterizable for external pressure sensor and
correction of influence of residual
Dead time (high-pressure version) 10 ... 30 s gas (correction of cross-interfer-
(purging time of the gas path in the ence)
unit at 125 ml/min)
Binary inputs 6, designed for 24 V, isolated,
Dead time (low-pressure version <5s freely parameterizable, e.g. for
without pump) measurement range switchover
Dead time (low-pressure version < 10 s Serial interface RS 485
with pump)
Options AUTOCAL function each with 8
Time for device-internal signal <1s additional binary inputs and relay
processing outputs, also with PROFIBUS PA or
Pressure correction range PROFIBUS DP
Pressure sensor internal 800 ... 1 100 hPa (abs.) Climatic conditions
Permissible ambient temperature -40 ... +70 °C during storage and
transportation, 5 … 45 °C during
operation
Permissible humidity < 90 % relative humidity as annual
average, during storage and trans-
portation (must not fall below dew
point)
Explosion protection
Without A
Language
German 0
English 1
French 2
Spanish 3
Italian 4
Additional versions Order code
Add "-Z" to Article No. and specify Order code
Telescopic rails (2 units) A31
TAG labels (specific lettering based on customer information) B03
Clean for O2 service (specially cleaned gas path) Y02
Measuring range indication in plain text, if different from the standard setting Y11
Special setting Y12
(only in conjunction with an application no., e.g. extended measuring range)
Extended special setting Y13
(only in conjunction with an application no., e.g. determination of cross-interfer-
ences)
Accessories Article No.
RS 485/Ethernet converter A5E00852383
RS 485/RS 232 converter C79451-Z1589-U1
RS 485/USB converter A5E00852382
AUTOCAL function each with 8 digital inputs/outputs C79451-A3480-D511
AUTOCAL function 8 digital inputs/outputs each and PROFIBUS PA A5E00057307
AUTOCAL function 8 digital inputs/outputs each and PROFIBUS DP A5E00057312
Set of Torx screwdrivers A5E34821625
384.5
351.5
27.5
15.6
173 128 4
s
101.6
37.7
149.5
177
82
172
M4
2;<0$7
86.5
465
483
440
411.5
104
132
320
345
36
0
■ Schematics
1
Pin assignment (electrical connections)
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0 *1'
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M 19 GND
37 NC
18 NC
36 Binary input 14-P
17 Binary input 13-P
35 Binary input 12-P Isolated
16 Binary input 11-P via optocoupler
34 Binary input 10-P "0" = 0 V (0 ... 4.5 V)
15 Binary input 9-P "1" = 24 V (13 ... 33 V)
33 Binary input 8-P
14 Binary input 7-P
32 Binary input 7 to 14-N
13
31 Relay 14
12
30
11 Relay 13
29
10
28 Relay 12
9
27 Contact load
8 Relay 11 max. 24 V/1 A, AD/DC
26
7 for shown
25 Relay 10 relay contact position,
6 the relay has zero current
24
5 Relay 9
23
4
22 Relay 8
3
21
2 Relay 7
20
M 1 GND
5 DGND 5
9 CNTR-N 9
4 CNTR-P/direction control 4
8 RxD/TxD-N (A) 8 PA-N(-)
3 RxD/TxD-P (B) 3 PA-P(+)
7 7
2 2
6 VP /+ 5 V 6
1 1
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VKLHOGHGDQGUHVWDJDLQVWWKHHQFORVXUHSRWHQWLDO
OXYMAT 64, 19" rack unit, pin assignment of the AUTOCAL plate and PROFIBUS plug
2 1 Purge gas
inlet
9-pin
interface
connector
(Optional):
e.g.
PROFIBUS
Mains connection
and miniature
fuses
37-pin connector:
Binary inputs and
relay outputs (optional)
25-pin connector:
Binary inputs and
Gas connections relay outputs
Sample gas inlet: Clamping ring connection 6 mm or ¼"
Sample gas outlet: Fittings 6 mm or ¼"
OXYMAT 64, 19" rack unit, gas connections and electrical connections
■ Design
19" rack unit
• With 4 HU for installation
- in hinged frame
- in cabinets with or without telescopic rails
• Front plate for service purposes can be pivoted down
(laptop connection)
• Internal gas paths: stainless steel pipe (mat. no. 1.4571)
• Gas connections for sample gas inlet and outlet and for purg-
ing gas: fittings, pipe diameter of 6 mm or ¼"
Field device
The CALOMAT 6 gas analyzer is primarily used for quantitative • Two-door enclosure (IP65) with gas-tight separation of ana-
determination of H2or He in binary or quasi-binary non-corrosive lyzer and electronics sections
gas mixtures. • Individually purgeable enclosure halves
Concentrations of other gases can also be measured if their • Stainless steel gas path and stubs (mat. no. 1.4571)
thermal conductivities differ significantly from the residual gases • Purging gas connections: pipe diameter 10 mm or 3/8"
like Ar, CO2, CH4, NH3.
• Gas connections for sample gas inlet and outlet: clamping
ring connection for a pipe diameter of 6 mm or ¼"
■ Benefits
Display and control panel
• Small T90 time due to micromechanical-produced Si sensor
• Large LCD panel for simultaneous display of:
• Universally applicable hardware basis, high measuring range - Measured value (digital and analog displays)
dynamics (e.g. 0 to 1 %, 0 to 100 %, 95 to 100 % H2) - Status bar
• Integrated correction of cross-interference, no external calcu- - Measuring ranges
lation required • Contrast of LCD panel adjustable using menu
• Open interface architecture (RS 485, RS 232, PROFIBUS) • Permanent LED backlighting
• SIPROM GA network for maintenance and service information • Washable membrane keyboard with five softkeys
(option)
• Menu-driven operation for parameterization, test functions,
• Electronics and analyzer part: gas-tight separation, purge- adjustment
able, IP65, long service life even in harsh environments
• User help in plain text
• EEx(p) for Zones 1 and 2 (in accordance with 94/9/EC
(ATEX 2G and ATEX 3G), and Class I Div 2 (CSA) Ex(n) • Graphic display of concentration trend; programmable time
intervals
■ Application • Bilingual operating software German/English, English/
Spanish, French/English, Spanish/English, Italian/English
Fields of application
Input and outputs
• Pure gas monitoring (0 to 1 % H2 in Ar)
• One analog output per medium (from 0, 2, 4 to 20 mA; NAMUR
• Protective gas monitoring (0 to 2 % He in N2) parameterizable)
• Hydroargon gas monitoring (0 to 25 % H2 in Ar) • Two analog inputs configurable (e.g. correction of cross-inter-
• Forming gas monitoring (0 to 25 % H2 in N2) ference or external pressure sensor)
• Gas production: • Six binary inputs freely configurable (e.g. for measurement
- 0 to 2 % He in N2 range switchover, processing of external signals from sample
- 0 to 10 % Ar in O2 preparation)
• Chemical applications: • Six relay outputs freely configurable (e.g. failure, maintenance
- 0 to 2 % H2 in NH3 request, limit alarm, external solenoid valves)
- 50 to 70 % H2 in N2 • Each can be expanded by eight additional binary inputs and re-
• Wood gasification (0 to 30 % H2 in CO/CO2/CH4) lay outputs (e.g. for autocalibration with max. four test gases)
• Blast furnace gas (0 to 5 % H2 in CO/CO2/CH4/N2) Communication
• Bessemer converter gas (0 to 20 % H2 in CO/CO2) RS 485 present in basic unit (connection from the rear; for the
• Monitoring equipment for hydrogen-cooled turbo-alternators: rack unit also behind the front plate).
- 0 to 100 % CO2/Ar in air
- 0 to 100 % H2 in CO2/Ar Options
- 80 to 100 % H2 in air • RS 485/RS 232 converter
• Versions for the analysis of flammable and non-flammable • RS 485/Ethernet converter
gases or vapors for use in hazardous areas (Zone 1 and • RS 485/USB converter
Zone 2)
• Connection to networks via PROFIBUS DP/PA interface
• SIPROM GA software as the service and maintenance tool
Display of
concentrations as
numbers and bargraph Display of current
measuring ranges
Display of
start-of-scale and
full-scale values
ESC key
to abort inputs
Keyboard to
enter values
INFO key
for help in plain text
CLEAR key
to delete inputs
ENTER key MEAS key
to accept to return to
input values measurement mode
3XUJLQJJDV 6DPSOHJDV
3XUJLQJJDV 3XUJLQJJDV 6DPSOHJDV
(OHFWURQLFFRPSDUWPHQW $QDO\]LQJFRPSDUWPHQW
0
*1'
9-pin connector
(RS 485)
9 (device 1)
0
0
*1'
9-pin connector
(RS 485)
9 (device 2)
0
0
*1'
9-pin connector
(RS 485)
9 (device 3)
0
Power consumption Approx. 20 VA Sample gas pressure < 1 % of the current measuring
range with a pressure change of
Fuse values 100 ... 120 V: 1.0T/250 100 hPa
200 ... 240 V: 0.63 T/250
Power supply < 0.1 % of the current measuring
Gas inlet conditions range with rated voltage 10 %
Sample gas pressure 800 ... 1 100 hPa (absolute) Electrical inputs and outputs
Sample gas flow 30 ... 90 l/h (0.5 ... 1.5 l/min) Analog output 0/2/4 ... 20 mA, isolated;
load max. 750
Sample gas temperature Min. 0 to max. 50 °C, but above
the dew point Relay outputs 6, with changeover contacts,
freely parameterizable, e.g. for
Temperature of the measuring cell Approx. 60 ºC measuring range identification;
Sample gas humidity < 90 % relative humidity load: 24 V AC/DC/1 A, isolated
Dynamic response Analog inputs 2, dimensioned for
0/2/4 … 20 mA for external pres-
Warm-up period < 30 min (the technical specifica- sure sensor and correction of
tion will be met after 2 hours) cross-interference
Delayed display (T90) <5s Binary inputs 6, designed for 24 V, isolated,
Damping (electrical time constant) 0 ... 100 s, parameterizable freely parameterizable, e.g. for
measurement range switchover
Dead time (purging time of the gas Approx. 0.5 s
path in the unit at 1 l/min) Serial interface RS 485
Options AUTOCAL function with
8 additional binary inputs and
relay outputs each, also with
PROFIBUS PA or PROFIBUS DP
Climatic conditions
Permissible ambient temperature -30 … +70 °C during storage and
transportation, 5 … 45 °C during
operation
Permissible humidity (dew point < 90 % relative humidity as
must not be undershot) annual average, during storage
and transportation
■ Dimensional drawings
1
s
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CALOMAT 6, 19“ unit, pin assignment of AUTOCAL board and PROFIBUS connectors
9-pin
interface
connector
(option): e.g.
PROFIBUS
Power supply
and fuses
37-pin connector
Binary inputs and
relay outputs (option)
25-pin connector
Binary inputs and
Gas connections: stubs 6 mm or ¼" relay outputs
■ Technical specifications
1
General (based on DIN EN 61207 / IEC 1207. All data refers to the Measuring response (relating to sample gas pressure 1 013 hPa
binary mixture H2 in N2) absolute, 0.5 l/min sample gas flow and 25 °C ambient temperature)
Measuring ranges 4, internally and externally switch- Output signal fluctuation (maximum < 0.75 % of the smallest possi-
able; automatic measuring range accuracy achieved after 2 hours) ble measuring range according to
changeover also possible rating plate, with electronic
damping constant of 1 s
Largest possible measuring span 100 vol.% H2 (for smallest mea- ( = 0.25 %)
suring span, see "Function")
Zero point drift < 1 %/week of the smallest pos-
Measuring ranges with suppressed Any zero point within sible measuring span according
zero point 0 ... 100 vol.% can be to rating plate
implemented; smallest possible
measuring span: 5 % H2 Measured-value drift < 1 %/week of the smallest pos-
sible measuring span according
Operating position Front wall, vertical to rating plate
Conformity CE mark in accordance with Repeatability < 1 % of the current measuring
EN 61326/A1 and EN 61010/1 range
Design, enclosure Detection limit 1 % of the current measuring
Degree of protection IP65 according to EN 60529 range
º
s &$/20$7
■ Schematics
1
Pin assignment (electrical and gas connections)
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0 *1'
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1&
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CALOMAT 6, field unit, connector and terminal assignment of the AUTOCAL board and PROFIBUS connectors
a b c d 5 7
1 3
2 4
8
6
If the CALOMAT 6 is supplied with a specially cleaned gas path for high oxygen context ("Cleaned for O2 service"), please ensure
that you specify this when ordering spare parts. This is the only way to guarantee that the gas path will continue to comply with the
special requirements for this version.
■ Overview ■ Design
1
19" rack unit
• With 4HE for installation
- in hinged frame
- in cabinets with or without telescope rails
- With closed or flow-type reference chambers
• Front plate for service purposes can be pivoted down
(laptop connection)
• IP20 degree of protection, with purging gas connection
• Internal gas routes: Pipe made of stainless steel
(mat. no. 1.4571)
• Gas connections for sample gas inlet and outlet and for refer-
ence gas: Internal thread 1/8" – 27 NPT
• Purging gas connections: Pipe diameter 6 mm or 1/4"
• With closed or flow-type reference chambers
Field device
• Two-door enclosure (IP65) for wall mounting with gas-tight
The CALOMAT 62 gas analyzer is primarily used for quantitative separation of analyzer and electronic parts, purgeable
determination of one gas component (e.g. H2, N2, Cl2, HCl, NH3) • Individually purgeable enclosure halves
in binary or quasi-binary gas mixtures.
• Gas path with screw pipe connection made of stainless steel
The CALOMAT 62 is specially designed for use in corrosive gas (mat. no. 1.4571), or Hastelloy C22
mixtures. • Purging gas connections: Pipe diameter 10 mm or 3/8"
• Gas connections for sample gas inlet and outlet and for refer-
■ Benefits ence gas: Internal thread 1/8" – 27 NPT
• Universally applicable hardware basis • With closed or flow-type reference chambers
• Integrated correction of cross-interference, no external calcu-
Display and control panel
lation required
• Large LCD field for simultaneous display of:
• Open interface architecture (RS 485, RS 232, PROFIBUS)
- Measured value (digital and analog displays)
• SIPROM GA network for maintenance and servicing informa- - Status bar
tion (option) - Measuring ranges
• Electronics and analyzer unit: gas-tight isolation, purging is • Contrast of the LCD field adjustable via the menu
possible, IP65, long service life even in harsh environments
• Permanent LED backlighting
(field device)
• Washable membrane keyboard with five softkeys
■ Application • Menu-driven operator control for parameterization, test func-
tions, adjustment
Fields of application • Operator support in plain text
• Chlorine-alkali electrolysis • Graphical display of the concentration progression; time inter-
• Metallurgy (steel production and processing) vals parameterizable
• H2 measurement in LNG (Liquefied Natural Gas) process • Bilingual operating software German/English,
• Ammonia synthesis English/Spanish, French/English, Spanish/English,
Italian/English
• Fertilizer production
• Petrochemicals Input and outputs
• One analog output per medium (from 0, 2, 4 to 20 mA; NAMUR
Special versions parameterizable)
Special applications • Two analog inputs configurable (e.g. correction of cross-inter-
In addition to the standard combinations, special applications ference or external pressure sensor)
are also available upon request (e.g. higher sample gas pres- • Six binary inputs freely configurable (e.g. measurement range
sure up to 2 000 hPa absolute). changeover, processing of external signals from the sample
preparation)
• Six relay outputs, freely configurable (e.g. failure, mainte-
nance request, threshold alarm, external magnetic valves)
• Each can be expanded by eight additional binary inputs and
relay outputs (e.g. for autocalibration with max. four test
gases)
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Purging gas Reference gas Sample gas
5 6 7 8 22 21 12 11
Purging gas Purging gas Reference gas Sample gas
(flow-type, option)
Electronics side Analyzing side
CALOMAT 62, principle of operation, example of a non-flow-type refer- Effect of 1 % gas component with nitrogen as the residual gas,
ence chamber expressed in % H2
Important features Moreover, it must be noted that - in addition to a zero offset - the
gradient of the characteristic can also be affected by the resid-
• Four freely-programmable measuring ranges, also with sup- ual gas. However, this effect is negligible in the case of variations
pressed zero, all ranges linear in the interfering gas concentration below 10 %.
• Smallest spans down to 1 % H2 (with suppressed zero: 99 to
100 % H2) possible Taking these facts into consideration and due to the fact that the
cross-interference analyzers cause further measuring inaccura-
• Measuring range identification cies, a larger error in measurement occurs than with binary gas
• Electrically isolated measured-value output 0/2/4 to 20 mA mixtures despite correction of cross-interference.
(also inverted)
• Automatic or manual measuring range switchover selectable;
remote switching is also possible
• Measured value can be saved during adjustment
0
*1'
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(RS 485)
9 (device 1)
0
0
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(RS 485)
9 (device 2)
0
0
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(RS 485)
9 (device 3)
0
EMC In accordance with standard Ambient temperature < 2 %/10 K referred to smallest
(Electromagnetic Compatibility) requirements of NAMUR NE21 possible span according to label
(08/98) and EN 61326 Accompanying gases Deviation from zero point (for
Electrical safety In accordance with EN 61010-1; influence of interfering gas, see
overvoltage category II section "Cross-interference")
Power supply (see nameplate) 100 V AC -10 % ... 120 V AC Sample gas flow 0.2 % of the current measuring
+10 %, 48 ... 63 Hz span with a change in flow of
0.1 l/min within the permissible
or flow range
200 V AC -10 % ... 240 V AC Sample gas pressure < 1 % of the current span with a
+10 %, 48 ... 63 Hz change in pressure of 100 hPa
Power consumption Approx. 30 VA Power supply < 0.1 % of the current span with
Fuse values 100 ... 120 V: 1.0T/250 rated voltage 10 %
200 ... 240 V: 0.63T/250 Electrical inputs and outputs
Gas inlet conditions Analog output 0/2/4 ... 20 mA, isolated;
max. load 750
Sample gas pressure 800 ... 1 100 hPa (absolute)
Relay outputs 6, with changeover contacts,
Sample gas flow 30 ... 90 l/h freely parameterizable, e.g. for
Sample gas temperature Min. 0 to max. 50 °C, but above measuring range identification;
the dew point load: 24 V AC/DC/1 A, isolated
Temperature of the measuring cell 70 ºC Analog inputs 2, dimensioned for 0/2/4 ... 20 mA
for external pressure sensor and
Dynamic response (the dynamic and measuring response refers to the correction of cross-interference
measurement of H2 in N2)
Binary inputs 6, designed for 24 V, isolated,
Warm-up period < 30 min at room temperature freely parameterizable, e.g. for
(the technical specification will be measuring range switchover
met after 2 hours)
Serial interface RS 485
Delayed display (T90) Approx. 35 s (including dead
time) Options AUTOCAL function with 8 addi-
tional binary inputs and 8 addi-
Damping (electrical time constant) 0 ... 100 s, parameterizable tional relay outputs, also with
Dead time (the diffusion to the Approx. 34 s PROFIBUS PA (on request) or
probes is the determining variable) PROFIBUS DP (on request)
Dead time (special application) 10 ... 15 s Climatic conditions
Permissible ambient temperature -40 ... +70 °C during storage and
transportation, 5 ... 45 °C during
operation
Permissible humidity (dew point < 90 % relative humidity as
must not be fallen below) annual average, during storage
and transportation
173 128
101.6
37.7
177
173
149.5
M4
CALOMAT 6
86.5
27.5
351.5
9
465 20 384.5
483
440
320
345
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55
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■ Schematics
1
Pin assignment (electrical and gas connections)
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CALOMAT 62, 19" rack unit, pin assignment of the AUTOCAL board and PROFIBUS connectors
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CALOMAT 62, 19" rack unit, gas connections and electrical connections
■ Dimensional drawings
1
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CALOMAT 62, field device, pin and terminal assignment of the AUTOCAL board and PROFIBUS connectors
a b c d 5 7
11 21 9
12 22 10
8
6
■ Design
1
• 19" rack unit with 4 HU for installation Input and outputs
- in hinged frame • One analog output for each measured component
- in cabinets with or without telescopic rails
• Two programmable analog inputs
• Front plate can be swung down for servicing purposes
(laptop connection) • Six binary inputs freely configurable (e.g. for measurement
range switchover, processing of external signals from sample
• Gas connections for sample gas inlet and outlet as well as preparation)
combustion gas and combustion air; pipe diameter 6 mm
or ¼" • Six relay outputs freely configurable (failure, maintenance re-
quest, maintenance switch, limit alarm, external solenoid
• Gas and electrical connections at the rear valves, measuring point switchover)
• Internal gas paths: stainless steel (mat. no. 1.4571) • Extension with eight additional binary inputs and eight addi-
Display and control panel tional relay outputs for autocalibration with up to four calibra-
tion gases
• Large LCD field for simultaneous display of:
- Measured value Communication
- Status bar
- Measuring ranges RS 485 present in basic unit (connection from the rear).
• Contrast of LCD panel adjustable using menu Options
• Permanent LED backlighting • RS 485/RS 232 converter
• Washable membrane keyboard with five softkeys • RS 485/Ethernet converter
• Menu-driven operation for parameterization, test functions, • RS 485/USB converter
adjustment • Incorporation in networks via PROFIBUS DP/PA interface
• User help in plain text • SIPROM GA software as service and maintenance tool
• Graphic display of concentration trend; programmable time
intervals
LED backlit graphic Status line for display Two code levels
display and of analyzer status according to NAMUR
membrane keyboard (programmable) (maintenance and
with noticeable click specialist level)
Operation with
menu control
using five softkeys
Display of
concentrations as
numbers and bargraph
Display of current
measuring ranges
Display of
start-of-scale and
full-scale values
ESC key
to abort inputs
Keypad to
enter values
INFO key
for help in plain text
CLEAR key
to delete inputs
ENTER key MEAS key
to accept to return to
input values measurement mode
Gas path
Combustion
gas H2
Mechan. Solenoid Restrictor
Sample chamber pressure valve
Pressure sensor
regulator
Gas outlet
Combustion air
Pressure sensor
Mechan.
pressure
Restrictor regulator
Damping Pump 1
Sample gas
Filter
Zero gas
Calibration
gas
FIDAMAT 6 total hydrocarbon analyzer, gas path with pump and with connection for combustion air
Combustion air
Pressure sensor
Mechanical
pressure
Restrictor regulators
Sample gas
Zero gas
Calibration gas
Purging
FIDAMAT 6 total hydrocarbon analyzer, gas path without pump and with connection for combustion air
OVEN
Sample gas
• Two control levels with their own authorization codes for the n-hexane 1.01
prevention of accidental and unauthorized operator interven- iso-octane 1.04
tions
Ethine (acetylene) 0.91
• Automatic, parameterizable measuring range calibration
Propene 0.84
• Operation based on the NAMUR recommendation
Methanol 0.87
• Customer-specific analyzer options such as:
- Customer acceptance Ethanol 0.83
- TAG labels Ethanoic acid 1.13
- Drift recording
Methyl acetate 0.67
• Wear-free, corrosion-proof filter housing
Benzene 1.01
• No blocking of the sample gas capillaries through the use of a
quartz restrictor Ethyl benzene 0.96
• Purge function in the event of analyzer or power supply failure p-xylene 1.03
(avoids build-up of toxic and corrosive substances in the de- Dichloromethane 1.13
vice)
Trichloroethene 1.01
• Low consumption of combustion air
Tetrachlorethene 1.07
• Response factors comply with the minimum requirements in
accordance with German air purity guidelines and the Work- Chloroform 0.72
ing Group of the German automotive Industry Chlorobenzene 1.15
• Simple handling using a numerical membrane keyboard and
operator prompting
Cross-interferences (examples)1)
Interfering Concentration of the Induced
component interfering component cross-interference
O2 in N2 (21 vol. %) < 0.3 mg/m3
SO2 in N2 (258 mg/m3) < 0.15 mg/m3
NO in N2 (310 mg/m3) < 0.5 mg/m3
NO2 in synth. air (146 mg/m3) < 0.1 mg/m3
CO in N2 (461 mg/m3) < 0.15 mg/m3
CO2 in N2 (18 vol. %) < 0.1 mg/m3
HCl in N2 (78 mg/m3) < 0.3 mg/m3
1) With measuring range 0 to 15 mg/m3.
Power consumption • Approx. 150 VA during opera- Sample gas pressure < 2 % of the current measuring
tion, range range/1 % pressure
change (within 600 ... 1 100 hPa)
• Approx. 350 VA during warm-up
phase Power supply < 1 % of the current measuring
range with rated voltage 10 %
EMC In accordance with standard
(Electromagnetic Compatibility) requirements of NAMUR NE21 Position influence < 1 % with < 15° inclination
(08/98) Electrical inputs and outputs
Electrical safety In accordance with EN 61010-1, Analog output 0/2/4 ... 20 mA, isolated;
overvoltage category II max. load 750
Fuse values • 100 ... 120 V: 4.0T/250 Relay outputs 6, with changeover contacts,
• 200 ... 240 V: 2.5 T/250 freely parameterizable, e.g. for
measuring range identification;
Gas inlet conditions
load: 24 V AC/DC/1 A, potential-
Permissible sample gas pressure free
• Without pump < 2 000 hPa abs. Analog inputs 2, dimensioned for 0/2/4 to 20 mA
for external pressure sensor and
• With integrated pump 600 ... 1 100 hPa correction of influence of accom-
Sample gas flow 18 ... 60 l/h (0.3 ... 1 l/min) panying gas (correction of cross-
interference)
Sample gas temperature 0 ... 200 °C
Binary inputs 6, designed for 24 V, floating,
Sample gas humidity < 90 % RH (RH: relative humidity) freely parameterizable, e.g. for
Dynamic response measuring range switchover
FIDAMAT 6 with pump and heated oven, with combustion air connection
1
Gases Operating pressure
Inlet pressure Pump startup Flow through FID Flow through bypass
Without With
hPa (abs.) hPa (abs.) hPa (abs.) ml/min ml/min
Combustion gas 3 000 ... 5 000 2 000 20 ~ 25 —
Combustion air 3 000 ... 5 000 1 420 20 1 500 ~ 320 ~ 500
Sample gas ~ 1000 — 1 500 2 ~3 ~ 1 000
Zero gas 3 500 ... 4 000 — 1 500 2 ~3 ~ 1 000
Calibration gas 3 500 ... 4 000 — 1 500 2 ~3 ~ 1 000
FIDAMAT 6 without pump, with heated oven, with combustion air connection
Gases Operating pressure
Inlet pressure Sample/calibration gas Flow through FID Flow through bypass
Without With
hPa (abs.) hPa (abs.) hPa (abs.) ml/min ml/min
Combustion gas 3 000 ... 5 000 2 000 20 ~ 25 —
Combustion air 3 000 ... 5 000 1 480 5 — ~ 320 ~ 300
Sample gas 1 500 ... 2 000 — 1 500 2 ~3 ~ 500
Zero gas 1 500 ... 2 000 — 1 500 2 ~3 ~ 500
Calibration gas 1 500 ... 2 000 — 1 500 2 ~3 ~ 500
The supply gases (combustion gas, combustion air) must have a degree of purity of 5.0 in order to guarantee correct measurements.
The degree of purity must be increased in the case of very small hydrocarbon concentrations (< 1 ppm).
■ Dimensional drawings
1
101.6
177
86.5
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9 483 426.5 347 155.5 27.5
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FIDAMAT 6, 19" rack unit, pin assignment of the AUTOCAL board and PROFIBUS connectors
2 3
8 4 5 9-pin interface
connector (option)
1 6 7 (e.g. PROFIBUS)
37-pin connector:
binary inputs and
relay outputs
(option board)
Power supply
and fuses
Gas connections
1 ... 7 Swagelok, 6 mm or ¼ “
8 Stubs , 6 mm or ¼ “
9-pin
Combustion air connector:
Calibration gas Combustion gas Zero gas RS 485
2 3
4 5 9-pin interface
8
connector (option)
6 7 (e.g. PROFIBUS)
37-pin connector:
binary inputs and
relay outputs
(option board)
Power supply
and fuses
25-pin connector:
binary inputs and
Sample inlet Flushing relay outputs
Sample gas outlet Outlet 15-pin connector:
binary inputs and
Gas connections analog inputs/outputs
2 ... 7 Swagelok, 6 mm or ¼ “
8 Stubs , 6 mm or ¼ “
If the device was supplied with a specially cleaned gas path for high oxygen context ("Clean for O2 service"), please ensure that you
specify this when ordering spare parts. This is the only way to guarantee that the gas path will continue to comply with the special
requirements for this version.
■ Overview ■ Application
1
Fields of application
• Emission measurements
- Measurement of low NO concentrations in power plants or
gas turbines
- Monitoring of NOx in denitrification plants by direct
measurement of NO and NO2, as well as summation to NOx
in the analyzer
- Efficient measurement in desulfurization plants
- Monitoring of very small SO2 and NO concentrations
- Emission measurements in the paper and cellulose indus-
tries
• Process monitoring
- Measurement of SO2 in process gases in the paper and
petrochemical industries
- Optimization of NOx emissions in exhaust gas in the
automotive industry
The function of the SIPROCESS UV600 gas analyzer is based on
- H2S and SO2 measurements in the residual gas purification
UV resonance absorption spectrometry. It also is used to
of sulfur recovery units
measure very low NO, NO2, SO2 or H2S concentrations in gases.
• H2S measurement
- In typical emission applications
■ Benefits - Taking account of possible cross-sensitivities (e.g. from
• For NO, NO2, SO2: Very low cross-sensitivity with other gases mercaptan)
• All modules are thermostatically-controlled, and thus Special versions
independent of the ambient temperature
Special applications
• Simultaneous measurement of NO and NO2 with subsequent
calculation of total. Therefore neither an NO2 converter nor a In addition to the standard combinations, special applications
CLD analyzer is required. are also available upon request, e.g. as regards the material in
• Measurement in the UV range: the gas path and the sample chambers.
- No cross-sensitivity with H2O and CO2
- Very low SO2 and NO measuring ranges possible
• UV resonance absorption spectrometry:
- Measurement of very low NO concentrations
- Very low cross-sensitivity possible
• Very long service life of UV lamp (usually 2 years)
• Low drifts and high stability thanks to four-channel measuring
method with double generation of quotient
• True reference measurement for low-drift, stable results
• Interface for remote monitoring in networks and linking to
process control systems
• Optional calibration unit
- Filter wheel with calibration cells which can be automatically
swung into the optical path
- Low consumption of calibration gas
- Manual or automatic calibration possible
1 ■ Design
• 19" rack unit with 4 HU for installation Inputs and outputs
- in hinged frame • 2 configurable analog inputs
- in cabinets with or without telescopic rails
• 4 configurable analog outputs
• Internal gas paths: hose made of FKM (VitonTM) or pipe made
of PTFE or stainless steel • 8 digital inputs
• Gas connections for sample gas inlet and outlet and for • 8 digital outputs
reference gas: fittings, pipe diameter of 6 mm or ¼" Communications
Display and control panel Connection via SIPROCESS-UV600-specific software tool
• Large LCD panel for simultaneous display of measured value
and device status Materials wetted by sample gas
• Sensor buttons with context-based functions Component Material
• Display protected by glass pane Analyzer unit (sample chamber) Aluminum or stainless steel
mat. no. 1.44041), epoxy resin
• Contrast of the LC display can be adjusted
Optical window CaF2 or quartz1), epoxy resin
Gas path, gaskets FKM (Viton), PTFE, stainless steel
mat. no. 1.45711)
Chamber Aluminum or stainless steel1)
Gas inlet/outlet PVDF, stainless steel,
mat. no. 1.44011)
Moisture sensor Stainless steel mat. no. 1.4571,
platinum, epoxy resin
Diaphragm pump
• Central body PVDF
• Diaphragm FKM (Viton), EPDM
1)
Depending on the version
UV
module
■ Mode of operation
1
The measuring principle of the SIPROCESS UV600 is based on
the molecule-specific absorption of gases in the ultraviolet
wavelength range. Radiation of a wavelength appropriate to the
measurement is passed through the sample, and the selective
absorption which is proportional to the concentration of the
measured component is determined.
Measuring method
An electrodeless discharge lamp (1) emits broadband in the
ultraviolet spectral range. A filter wheel unit (2) generates the
ultraviolet radiation suitable for the respective measured
component. Either interference filter correlation (IFC) or gas filter
correlation (GFC), or a combination of the two methods, can be
used for this purpose.
Interference filter correlation (IFC)
The sample and reference radiations are generated alternately
with two different interference filters being swung into the beam
path (filter wheel 2a).
Gas filter correlation (GFC)
Especially when NO is the measured component, the reference
radiation is generated by swinging in a gas filter which is filled
with the associated gas (filter wheel 2b).
IFC and GFC
The two filter wheels are combined in order to measure NO in
combination with other measured components.
Design of the analyzer module
After passing through the filter unit, the beam is directed via a
lens (3), a beam divider (4) and a mirror (4) into the sample
chamber (6) and reference chamber (7).
The sample beam passes through the sample chamber (6), into
which sample gas flows, and its intensity is weakened in line with
the concentration of the measured component. The reference
beam is directed via a mirror (5) into the reference chamber (7).
This is filled with a neutral gas.
The detectors (9) receive the sample and reference beams in
succession. These measured signals are amplified and
evaluated using electronics.
The measuring system is temperature-controlled to minimize
external temperature influences.
The physical state of the measuring system is recorded simulta-
neously through time-offset detection of the reference beam,
and compensated if necessary.
A quotient is generated for each detector from the determined
signal values, and the ratio of these quotients determined. This
double generation of quotients means that symmetrical signal
drifts are compensated in the best possible manner in addition
to proportional signal drifts.
Note
The sample gases must be fed into the analyzers free of dust.
Condensation in the sample chambers must be prevented.
Therefore, the use of gas modified for the measuring task is
necessary in most application cases.
Additional measures depending on the application must be
taken when introducing gases with flammable components at
concentrations above the lower explosive limit (LEL). Please
contact the technical department in such cases.
1 ■ Function
IFC 2a M
2a
2b
GFC 2b M
IFC + GFC
M
10
2a
2
2b
M
3 M
6 8
4 9
7 8
5 9
■ Technical specifications
1
General information Electrical characteristics
Measuring ranges 3, automatic measuring range Line voltage (optional, see nameplate) 93 ... 132 V AC, 186 ... 264 V AC
switching
Line frequency (AC) 47 ... 63 Hz
Detection limit (2) < 1% of span
Permissible overvoltages (transient Up to overvoltage category II in
Smallest possible span Dependent on order configuration surges in the power supply network) accordance with IEC 60364-4-443
NO: 0 ... 10 / 0 … 20 / 0 … 25 /
0 … 50 vpm Power consumption Approx. 50 VA, max. 300 VA
NO2: 0 … 101) / 0 ... 20 / 0 … 25 / EMC interference immunity In accordance with EN 61326-1,
0 … 50 vpm (electromagnetic compatibility) EN 61326-2-1, EN 61000-6-2,
SO2: 0 … 101) / 0 ... 20 / 0 … 25 / EN 61000-6-4 and EU Directive
0 … 50 vpm 2004/108/EC. In the case of electro-
H2S: 0 … 25 / 0 … 50 vpm magnetic radiation in the frequency
Largest possible span Dependent on order configuration range from 750 MHz ± 20 MHz,
NO, NO2, SO2: 0 … 300 to increased measuring errors can
0 ... 1 000 vpm occur for small measuring ranges
H2S: 0 … 500 to 0 ... 1 000 vpm Electrical safety In accordance with EN 61010-1
UV lamp Internal line fuses
• Design EDL, electrodeless discharge lamp • primary 6.3 A, not replaceable
• Service life 2 years (17 500 h) • secondary 8A
Conformity CE mark Gas inlet conditions
Design, enclosure Permissible sample gas pressure Relative to ambient/atmospheric air
Degree of protection IP40 pressure:
-200 ... +300 hPa (-0.2 ... +0.3 bar)
Weight approx. 17 kg
Sample gas flow 20 ... 120 l/h (333 ... 2 000 ml/min)
Requirements of location of use
Sample gas temperature 5 ... 55 °C
Installation location Within closed building
Measuring response
Atmospheric pressure in the 700 …1 200 hPa
environment (relating to sample gas pressure 1 013 hPa absolute, 0.5 l/min sample gas
flow and 25 °C ambient temperature)
Relative humidity 10 ... 95%, non-condensing
Reference point drift < ± 1%/week of respective span
Permissible contamination Pollution degree 1
Zero point drift
Maximum geographic altitude of 2 500 m above sea level
location of use • Standard measuring ranges < ± 1%/week of respective span
• Small measuring ranges < ± 2%/week of respective span
Permissible ambient temperature ( 2x smallest measuring range)
• Operation +5 ... +45 °C (41 ... 113 °F) • Measured components NO, NO2, < ± 1%/day of respective span
• Transport and storage -10 ... +70 °C (14 ... 158 °F) SO2
Operating position Front wall, vertical, max. ± 15° angle Repeatability (reproducibility) < ± 1% of respective span
for each spatial axis
(maximum permissible inclination of Linearity error < ± 1% of respective span
the base surface during operation Electric inputs and outputs
wtih constant operating position)
Analog output 4, 0 ... 24 mA; floating (electrically
Permissible vibration/shock isolated), residual ripple 0.02 mA,
• Vibration displacement 0.035 mm (in the range 5 ... 59 Hz) resolution 0.1% (20 A), max.
• Amplitude of the starting accelera- 5 m/s2 (in the range 59 … 160 Hz) load 500 , max. voltage ± 50 V
tion Relay outputs 8, with changeover contacts, max.
voltage ± 50 V loading capacity:
Max. 30 V AC / max. 48 V DC /
max. 500 mA
Analog inputs 2, 0 ... 20 mA, reference potential
GND, signal strength max. 30 mA,
overcurrent protection max. ± 1 A,
voltage max. ± 50 V
Digital inputs 8, switching range 14 ... 42 V
(external control voltage),
max. voltage ± 50 V
Serial interface RS485, Ethernet (LAN)
1)
Only for daily recalibration and air-conditioned environment ( +/- 2 °C)
Product description
1
Additional versions Order code
Please add "-Z" to Article No. and specify Order code.
Second IO module A13
Calibration unit for 1st sample gas component B11
Calibration unit for 1st and 2nd sample gas components B12
Calibration unit for all 3 sample gas components B13
Flow monitor C11
Humidity monitor C12
Pressure sensor (sample gas) C14
Special setting (only in conjunction with an application no., Y12
e.g. special measuring range)
Extended special setting (only in conjunction with an Y13
application no., e.g. determination of cross-interferences)
Prepared for QAL1 (MCERTS), standard measured-value output in mg/m3 Y17
Spare parts recommendation for preventative maintenance Quantity for Quantity for Article No.
2 years 5 years
Article No.Safety filter FI64 1 2 A5E03707235
Power supply units, 24 V DC, 10 A 1 A5E03707236
Distribution board 1 A5E03707240
FKM hose d = 3/5, length = 1 m 2 5 A5E03707757
MEDL UV lamp with heater 1 1 ... 2 A5E03707918
Motor flange 3 1 A5E03707919
Motor flange 2 1 A5E03707920
Gas filter with holder, for measurement of NO 1 2 A5E03707921
SIPROCESS UV600 chamber H = 300 mm, aluminum 1 A5E03707925
Calibration chamber with holder for NO 1 A5E03707941
Calibration chamber with holder for SO2 and H2S 1 A5E03707942
Calibration chamber with holder for NO2 1 A5E03707943
Heater with 380 mm long cable, for SIPROCESS UV600: 1 2 A5E03707968
MEDL, chamber, motor flange
Moisture sensor 1 2 A5E03707969
Spare parts set - pressure sensor with gasket and O-ring 1 A5E03707970
Flow sensor with temperature sensor 1 2 A5E03707971
Diaphragm pump type 123, 24 V DC / 50 Hz 1 A5E03707986
Diaphragm assembly, EPDM for types 110-125 1 2 A5E03707987
O-ring for gas pump suspension 1 2 A5E03707988
1 ■ Dimensional drawings
ป
■ Schematics
1
Electrical connections
Interfaces:
A RS 485 / external input/output
B RS 485 / external input/output Signal connections of the Signal connections of the
C Reserved for service second, internal input/output internal input/output module
D Ethernet (LAN) module (optional) (standard)
A
B
D
C
SIEMENS
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zu YWTYWW}h pwG[W
jlyt
xGzWX
zGhn GGGGGGGGGGGGGGGGGGGGGGGGGGGtGGn
Power connection
XY
[ \
Z ^
X
1 Pin assignments
*1' ',& ', ', ', ', ', ', ', ', '2 '2 '2 '2
N
N
N
N
N
N
N
N
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'&9
;
SIPROCESS UV600, pin assignments of digital inputs X3 (DI1 to DI8) and digital outputs X4 (DO1 to DO4) and X5 (DO5 to DO8)
Characteristics of the digital inputs: Characteristics of the digital outputs:
• Floating optocouplers with common reference potential (DIC) • Floating relay changeover contacts
• Switching range 14 ... 42 V DC (external control voltage) • Single-pole changeover switch, three connections
• The digital inputs can be operated either with positive or • Maximum voltage: ± 50 V
negative voltage • Connect inductive loads (e.g. relays, solenoid valves ...)
• With inverted switching logic, the logic function of the control via spark-quenching diodes only
input is active if no current is flowing through the control input • Maximum load-carrying capacity (standard): Max. 30 V AC,
• Maximum voltage: ± 50 V max. 48 V DC, max. 500 mA.
N
; ;
P$
˖
SIPROCESS UV600, pin assignment of the analog inputs X7 (AI1 and AI2) and analog outputs X7 (AO1 to AO4)
Characteristics of the analog inputs: Characteristics of the analog outputs:
• The input signal is an analog current signal • Analog outputs are floating (electrically isolated) and provide
(standard 0 ... 20 mA, maximum 30 mA) a load-independent current signal
• The signal current must be provided by an external current • Signal range 0 ... 24 mA
source • Residual ripple 0.02 mA
• Load (internal resistance) of analog input: 10 • Resolution 0.1%
• Reference potential GND (see figure, analog inputs) • Accuracy 0.25% of full-scale value
• Overcurrent protection: ± 1 000 mA • Maximum load 500
• Max. voltage: ± 50 V • Maximum voltage ± 50 V
• Adjustable start or error state
Note for electrical isolation:
The electrical isolation is canceled if the negative poles of the
analog outputs are connected to GND.
2/2 Introduction
2/2 Introduction to TDLS:
LDS 6 and SITRANS SL
2/3 LDS 6
2/3 General information
2/10 19" central unit
2/20 Cross-duct sensor CD 6
2/30 Documentation
2/30 Suggestions for spare parts
2/31 SITRANS SL
2/31 In-situ O2 and CO gas analyzer
2/48 Documentation
Siemens PA 01 · 2015
© Siemens AG 2014
■ Overview
In-situ process gas analysis The SITRANS SL gas analyzer for highly sensitive measurement
of oxygen and carbon monoxide has a more integrated design
Process gas analyzers are used for continuous determination of without fiber-optic cables and with only one pair of cross-ducts
the concentrations of one or more gases in a gas mixture. Deter- sensors - a transmitter unit and a detector unit. In this case the
mination of the concentration of gases in a process is used to receiver has a local user interface (LUI) which is controlled using
control and monitor process flows, and is therefore decisive for IR remote control.
the automation and optimization of processes and ensuring
2 product quality. In addition, process gas analyzers are used to
check emissions, thus making an important contribution to
A maintenance-free reference gas cell integrated in both
analyzers drastically reduces the need for recalibration
environmental protection, as well as for ensuring compliance (SITRANS SL) or even makes its superfluous (LDS 6). Remote
with statutory directives. scanning and diagnostics of the analyzers is possible using the
Ethernet interface present as standard.
In-situ analytical procedures feature physical measurements in
the flow of process gas directly in the actual process gas line. In The list of gas components measurable using NIR diode laser
contrast to extractive gas analysis, a sample is not taken and technology already comprises:
routed on to the analyzer via a sample line and sample prepa- • For the LDS 6 analyzer:
ration. Only in exceptional cases, the process conditions make O2, NH3, HCl, HF, H2O, CO, CO2, ...
it necessary to condition the sample gas stream in a bypass line
with respect to process temperature, pressure and/or optical • For the SITRANS SL analyzer: O2, CO
path length. Further conditioning of the process gas, such as The list is being permanently extended as laser technology is
drying or dust precipitation, is unnecessary. The analyzer developed further. The LDS 6 O2 analyzers additionally allow
carrying out in-situ measurements must always take into account simultaneous non-contact determination of high process gas
changing process conditions (if these occur) and be able to temperatures.
automatically process them in the calibration model. Computed
temperature and pressure compensation is frequently required Gas measurements with diode lasers feature exceptional selec-
for this. In addition, the analyzer must be extremely rugged since tivity and flexibility. Neither high process temperatures nor high
its sensors have direct contact with the process gas. The fast and varying concentrations of particles in the gas have an
and non-contact measurement of gas concentrations directly in influence on the quality of the result within wide ranges. For
the process is the domain of in-situ diode laser gas analyzers. example, it is possible with the LDS 6 to determine trace
concentrations of NH3, HCl or HF directly in moist process gases
The gas analyzer LDS 6 combines the compact and service- even before any gas purification stage.
friendly design, simple operation and network capability of the
Series 6 analyzers with the well-known exceptional performance These features together with fast measurements free of dead
data of in-situ gas analysis - namely high ruggedness and avail- times mean that diode laser gas analysis with the LDS 6 or the
ability as well as low maintenance - by using diode laser SITRANS SL is an extremely interesting alternative to estab-
technology and fiber-optics. Up to three CD 6 in-situ cross-duct lished extractive analyses.
sensors (which are also optionally available in an intrinsically-
safe version for operation in hazardous areas) can be combined
with an LDS 6 analyzer in the compact 19" rack unit enclosure.
The distance between the analyzer’s control unit - typically in an
existing instrument room or the process plant’s control room -
and the max. three measuring points can be up to 700 m in each
case.
■ Overview ■ Application
LDS 6 is a diode laser gas analyzer with a measuring principle Applications
based on the specific light absorption of different gas compo- • Process optimization
nents. LDS 6 is suitable for fast and non-contact measurement
of gas concentrations or temperatures in process or flue gases. • Continuous emission monitoring for all kinds of fuels
One or two signals from up to three measuring points are pro- (oil, gas, coal, and others)
cessed simultaneously by the central analyzer unit. The in-situ • Process measurements in power utilities and any kind of
2
cross-duct sensors at each measuring point can be separated incinerator
up to 700 m from the central unit by using fiber-optic cables. The • Process control
sensors are designed for operation under harsh environmental
conditions and contain a minimum of electrical components. • Explosion protection
• Measurements in corrosive and toxic gases
• Quality control
• Environmental protection
• Plant and operator safety
Sectors
• Power plants
• Steel works
• Cement industry
• Chemical and petrochemical plants
• Automotive industry
• Waste incinerators
• Glass and ceramics production
• Research and development
Special applications
LDS 6, typical installation with cross-duct sensors In addition to the standard applications, special applications are
available upon request.
■ Benefits
The in-situ gas analyzer LDS 6 is characterized by a high avail-
ability and unique analytical selectivity, and is optimally suitable
for numerous applications. LDS 6 enables the measurement of
one or two gas components or - if desired - the gas temperature
directly in the process:
• With high dust load
• In hot, humid, corrosive, explosive, or toxic gases
• In applications showing strong varying gas compositions
• Under harsh environmental conditions at the measuring point
• Highly selective, i.e. mostly without cross-sensitivities
LDS 6 properties:
• Little installation effort
• Minimum maintenance requirements
• Extremely rugged design
• High long-term stability through built-in, maintenance-free
reference gas cell, field calibration is unnecessary
• Real-time measurements
Moreover, the instrument provides warning and failure
messages upon:
• Need for maintenance
- Erroneous reference function
- Bad signal quality
• Violation of a lower or upper alarm level for the measured
variable
• Transmitted amount of light violating an upper or lower limit
■ Design
The gas analyzer LDS 6 consists of a central unit and up to three Inputs and outputs
in-situ sensors. The connection between the central unit and the • One to three measurement channels with hybrid connections
sensors is established by a so-called hybrid cable, which con- for the sensors at the measuring points
tains optical fibers and copper wires. An additional cable con-
nects the transmitter and receiver parts of the cross-duct sensor. • 2 analog inputs per channel for process gas temperature and
pressure
Central unit
2
• 2 analog outputs per channel for gas concentration(s). For se-
The central unit is housed in a 19" rack unit housing with 4 fixing lected versions, the transmission can be read out as an alter-
points for mounting: native.
• In a hinged frame • 6 freely configurable binary inputs per channel for signaling
faults or maintenance requests from external temperature or
• In racks with or without telescopic rails pressure transducers or sensor purging failure.
Display and control panel • 6 freely configurable binary outputs per channel (signaling of
• Large LCD field for simultaneous display of measurement fault, maintenance requirements, function control, transmis-
result and device status sion limit alarm, concentration limit alarm, store analog output)
• Contrast of the LCD field is adjustable via the menu Communication
• LED background illumination of the display with Network connection: Ethernet (T-Base-10) for remote diagnos-
energy-saving function tics and maintenance.
• Easy-to-clean membrane touch pad with softkeys
• Menu-driven operation for parameterization and diagnostics
• Operation support in plain text
Menu-driven
operator control
with five softkeys
Numeric display
of concentrations
ESC key
to cancel entries
Numeric keypad
for entering digits
INFO key
for help in plain text
CLEAR key
to delete the
digits entered ENTER key MEAS key
to adopt to return direct to
the numbers measurement mode
■ Function
Operating principle
LDS 6 is a gas analyzer employing single-line molecular absorp- The result is a fully resolved single molecular line which is ana-
tion spectroscopy. A diode laser emits a beam of near-infrared lyzed in terms of absorption strength and line shape. The influ-
light, which passes through the process gas and is detected by ence of cross-sensitivities on the measurement is negligible,
a receiver unit. The wavelength of the laser diode output is tuned since the quasi-monochromatic laser light is absorbed very se-
to a gas-specific absorption line. The laser continuously scans lectively by only one specific molecular line in the scanned
2 this single absorption line with a very high spectral resolution. spectral range.
Laser light
Electrical signals P1
Reflected LED light
Measured
volume
Channel 1
CPU and Laser
display control E/O
Signal Diode
processing laser
P2
E/O Measured
Optocoupler volume
P0 Channel 2
E/O
E/O
E/O PR
Reference
cell
P3
Measured
volume
Channel 3
E/O
Central unit
Sensor connecting cable Transmitter unit
+2
2
Sample
gas
inlet
Temperature
Hybrid cable sensor
Sample gas
Supplementary 1+SSP
channel (option) outlet
Supplementary
channel (option)
Receiver
Typical transmitted light setup of LDS 6, in bypass
A flow cell is available by special application for the LDS 6 which Absorption spectra of water and ammonia
has been specially optimized for use with the LDS 6 and its Typical measurable gases for LDS 6 are:
transmitted-light sensors with respect to handling and measur-
ing performance. It is designed to reduce surface effects, and is • Oxygen (O2) for low and high pressure
therefore also highly suitable for polar gases like ammonia. This • Hydrogen fluoride (HF) + water
flow cell is available in heated and non-heated versions. Wheel • Hydrogen chloride (HCl) + water
mounted and wall mounted versions are available.
• Ammonia (NH3) + water
• Water vapor (H2O)
Transmitter unit • Carbon monoxide (CO)
Central unit Heating
Sensor connecting cable
$EVRUSWLRQOLQH
Measuring configuration of LDS 6 with heated flow cell
General information
LDS 6 is connected to the measuring points by fiber optics. The
laser light is guided by a single-mode fiber from the central unit
to the transmitter unit of the in-situ sensor. The sensor consists of
a transmitter and a receiver; the distance between them defines
the measurement path. In the receiver box, the light is focused
onto a suitable detector. The detector signal is then converted
into an optical signal and transmitted via a second optical fiber
to the central unit, where the concentration of the gas compo-
nent is determined from the detected absorption signal.
/DVHUOLQH
LDS 6 usually measures a single gas component by means of
the absorption capacity of a single fully resolved molecular ab-
sorption line. The absorption results from conversion of the radi- Typical spectral bandwidth of an absorption line compared to the band-
ation energy of the laser light into the internal energy of the mol- width of the laser light.
ecule. In the working range of the LDS 6, both rotation-vibration
transitions and electronic transitions - such as with O2 - can be
triggered.
■ Technical specifications
Electrical characteristics
Analytical performance
Power supply 100 ... 240 V AC 50 ... 60 Hz,
Measuring range Adjustable
automatically adapted by the sys-
Detection limit (DL): Depending on sample gas com- tem; with a 3-channel central unit,
Calculated in accordance with ponent: see table for standard an additional external power sup-
VDI 2449, measured on every sup- applications. ply +24 V DC, 50 VA is included
in the scope of delivery
2
plied analyzer during the tempera- For application code ET and FT:
ture test (between 5 ... 45 °C) in in accordance with the require- Power consumption 50 W
accordance with VDI 4203. ments of 17th and 27th BImSchV
EMC According to EN 61326 and stan-
Smallest recommended measuring Depending on sample gas com- dard classification of NAMUR
range (with 1 m path length) ponent: see table for standard NE21
applications.
Electrical safety According to EN 61010-1,
The maximum applicable measuring ranges can be found in the table overvoltage classification II
of standard combinations. These can only be applied if the individual
process conditions allow it. Please contact the Technical Support from Fuse specifications 100 ... 240 V: T2.5L250V
Siemens for checking the applicability. Dynamic response
Accuracy 2 % / 5 %, depending on sample Warm-up time at 20 °C ambient Approx. 15 min
gas component and application temperature
code. At best: detection limit. See
table for standard applications. Response time Min. of 1 s, depending on appli-
cation
For application code ET and FT:
in accordance with the require- Integration time 1 … 100 s, adjustable
ments of 17th and 27th BImSchV
Influencing variables
Linearity Better than 1 %
Ambient temperature < 0.5 %/10 K of the measured
Repeatability 2 % of the measured value or value
minimum detection limit (which-
ever is largest) Atmospheric pressure Negligible
For application code ET and FT: Process gas pressure compensa- Recommended
in accordance with the require- tion
ments of 17th and 27th BImSchV Process gas temperature compen- Recommended
Calibration interval No recalibration required thanks sation
to internal reference cell Process gas pressure range See table for standard applica-
General information tions
Concentration units ppmv, Vol%, mg/Nm3 Power supply changes < 1 %/30 V
Display Digital concentration display Electrical inputs and outputs
(5 digits with floating decimal Number of measurement channels 1 … 3, optional
point)
Analog output 2 per channel, 4 ... 20 mA, float-
Laser protection class Class 1, safe to the eye ing, ohmic resistance max. 750
Certificates CE marking, TÜV, MCERTS Analog inputs 2 per channel,
Design, enclosure designed for 4 ... 20 mA, 50
Degree of protection IP20 according to EN 60529 Binary outputs 6 per channel, with changeover
contacts, configurable, 24 V
Dimensions 177 x 440 x 380 mm AC/DC/1 A, floating
Weight Approx. 13 kg Binary inputs 6 per channel, designed for 24 V,
Mounting Horizontal floating, configurable
Communication interface Ethernet 10BaseT (RJ-45)
Climatic conditions
Temperature range 5 … 45 °C during operation,
-40 … +70 °C during storage
and transportation
Atmospheric pressure 800 … 1 200 hPa
Humidity < 85 % relative humidity,
above dew point
(in operation and storage)
2
with II 1 G Ex ia op is IIC T4 Ga, II 1 D Ex ia op is IIIC T135 °C Da
Measured component Possible with application code
of the respective channel
O2 B, C, P A
NH3 A, E, F, T C
NH3/H2O A, E, F, T D
HCl A, H, T E
HCl/H2O A, H, T F
HF A, H G
HF/H2O A, H H
CO C J
CO/CO2 D K
CO2 A L
H2O A, T M
Application code of Application examples channel 11)
measured component channel 1
A Emission monitoring, non-certified A
B Emission monitoring, combustion B
optimization
C Safety monitoring with appropriate C
plant concept
D Process control D
E SNCR-DeNOx E
F SCR-DeNOx F
H Filter optimization H
P Process control (high pressure) P
T Emission monitoring, QAL1 according EN T
15267-3 (TÜV and MCERTS), in combination
with measured component variants C, D, E,
F, M
CD 6, sensor alignment kit
With 0
Without 1
Application code of Application examples channel 21)
measured component channel 2
X Channel 2 not used X
A Emission monitoring A
B Combustion optimization B
C Safety monitoring with appropriate C
plant concept
D Process control D
E SNCR-DeNOx E
F SCR-DeNOx F
H Filter optimization H
P Process control (high pressure) P
T Emission monitoring, QAL1 according EN T
15267-3 (TÜV and MCERTS), in combination
with measured component variants C, D, E,
F, M
1)
The examples shown represent possible applications where appropriately configured LDS 6 solutions can be used. The user is responsible for the prevailing
conditions (plant concept (possibly redundant), application of appropriate components required in addition, compliance with possible directives, etc.).
2 B
C
Combustion optimization
Safety monitoring with appropriate
B
C
plant concept
D Process control D
E SNCR-DeNOx E
F SCR-DeNOx F
H Filter optimization H
P Process control (high pressure) P
T Emission monitoring, QAL1 according EN T
15267-3 (TÜV and MCERTS), in combination
with measured component variants C, D, E,
F, M
Language (supplied documentation, software)
German 0
English 1
French 2
Spanish 3
Italian 4
■ Dimensional drawings
101.6
178
LDS 6
465 355
483 432
177
428
351.5
437
483
440
■ Schematics
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Ethernet
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RJ-45
■ More information
The following table lists the measuring conditions for standard Please note that the values for the detection limit and the maxi-
applications. The listed values for the measuring range and de- mum measuring range refer to a path length of 1 m. Longer path
tection limit (DL) are only approximate values. The exact values lengths will improve the detection limit, but not linearly. due to
at the respective measuring point depend on the totality of all in- limiting effects such as dust load. The maximum applicable
fluencing variables and can be determined by Siemens for the measuring ranges can only be used if permitted by the process
specific case. conditions such as dust load.
2 Standard application Process gas Process gas Min. Max. measuring (Max. measur- (DL x path (DL x path Accu-
Effective optical path temperature pressure measuring range ing range x length) length) racy3)
length: 0.3 … 12 m Tmin … Tmax pmin … pmax range (also depen- path length) under stan- At
(with 1 m dent on eff. opt. dard con- 1 013 hPa
Dust load2): ditions1) with cross-
< 50 g/Nm3 eff. opt. path path length:
length) see following without interference
column) cross-inter- of gas 2
ference of
other gases
Gas Gas Gas Appl. Gas 1 Gas 1 Gas 1 Gas 1 Gas 1 Gas 1
1 2 code code
O2 A B6) 600 … 1 200 °C 950 … 1 050 hPa 0 … 15 vol% 0 … 100 vol% 240 vol%*m 0.3 vol%*m 5%
At 600 °C
C 0 … 600 °C 950 … 1 050 hPa 0 … 5 vol% 0 … 100 vol% 75 vol%*m 0.1 vol%*m 2 %4)
P 0 … 200 °C 950 … 5 000 hPa 0 … 5 vol% 0 … 100 vol% 75 vol%*m 0.1 vol%*m 2%
NH3 C A 0 … 150 °C 950 … 1 050 hPa 0 … 25 ppmv 0 … 500 ppmv 2 500 ppmv*m 0.5 ppmv*m 0.9 ppmv*m 2 %
At 15 vol%
H2O, 55 °C
T 0 … 150 °C 950 … 1 050 hPa 0 … 25 ppmv 0 … 500 ppmv 2 500 ppmv*m 0.5 ppmv*m 0.9 ppmv*m 2 %
At 15 vol%
H2O, 55 °C
E 250 … 350 °C 950 … 1 050 hPa 0 … 45 ppmv 0 … 500 ppmv 2 500 ppmv*m 0.9 ppmv*m 1.4 ppmv*m 2 %
At 250 °C at 15 Vol%
H2O, 250 °C
F 300 … 400 °C 950 … 1 050 hPa 0 … 50 ppmv 0 … 500 ppmv 2 500 ppmv*m 1 ppmv*m 1.5 ppmv*m 2 %
At 300 °C at 15 Vol%
H2O, 300 °C
NH3 H2O D A 0 … 150 °C 950 … 1 050 hPa 0 … 25 ppmv 0 … 100 ppmv 1 200 ppmv*m 0.5 ppmv*m 0.9 ppmv*m 2 %
At 15 vol%
H2O, 55 °C
T 0 … 150 °C 950 … 1 050 hPa 0 … 25 ppmv 0 … 100 ppmv 1 200 ppmv*m 0.5 ppmv*m 0.9 ppmv*m 2 %
At 15 vol%
H2O, 55 °C
E 250 … 350 °C 950 … 1 050 hPa 0 … 45 ppmv 0 … 100 ppmv 1 200 ppmv*m 0.9 ppmv*m 1.4 ppmv*m 2 %
At 250 °C At 15 vol%
H2O, 250 °C
F 300 … 400 °C 950 … 1 050 hPa 0 … 50 ppmv 0 … 100 ppmv 1 200 ppmv*m 1 ppmv*m 1.5 ppmv*m 2 %
At 300 °C At 15 vol%
H2O, 300 °C
HCl E A 0 … 150 °C 950 … 1 050 hPa 0 … 30 ppmv 0 … 6 000 ppmv 1 200 ppmv*m 0.6 ppmv*m 2.2 ppmv*m 5 %
At 15%
H2O, 55 °C
T 120 … 210 °C 950 … 1 050 hPa 0 … 10 ppmv 0 … 60 ppmv 720 ppmv*m
H 150 … 250 °C 950 … 1 050 hPa 0 … 50 ppmv 0 … 6 000 ppmv 1 200 ppmv*m 1.0 ppmv*m 3.1 ppmv*m 5 %
At 150 °C at 15 Vol%
H2O, 150 °C
HCl H2O F A 0 … 150 °C 950 … 1 050 hPa 0 … 30 ppmv 0 … 100 ppmv 1 200 ppmv*m 0.6 ppmv*m 2.2 ppmv*m 5 %
At 15%
H2O, 55 °C
T 120 … 210 °C 950 … 1 050 hPa 0 … 10 ppmv 0 … 60 ppmv 720 ppmv*m
H 150 … 250 °C 950 … 1 050 hPa 0 … 50 ppmv 0 … 100 ppmv 1 200 ppmv*m 1.0 ppmv*m 3.1 ppmv*m 5 %
At 150 °C At 15 vol%
H2O, 150 °C
Footnotes: See page 2/18.
Standard application Min. measuring Max. mea- (Max. (DL x path (DL x path Accu- Purging gas Purging 2
Effective optical path range suring range measuring length) length) racy4) mode gas
length: 0.3 … 12 m (with 1 m eff. opt. (usually also range x under At 1 013 hPa medium
path length) dependent on path standard with cross-
Dust load3): < 50 g/Nm3 eff. opt. path length) conditions interference
1) 2)
length: see of gas 1
following
column)
Gas 1 Gas 2 Gas Appl. Gas 2 Gas 2 Gas 2 Gas 2 Gas 2 Gas 2 Stan- Optio-
code code dard nal
O2 A B6) E, F G, H Steam +
air, N2
C D B N2
P D B N2
NH3 C A C G Air
T C G Air
E E G Air
F E G Air
NH3 H2O D A 0 … 5 vol% 0 … 30 vol% 240 vol%*m 0.1 vol%*m 0.1 vol%*m 5% C G Air
HCl E A C G Air
T C G Air
H E G Air
HCl H2O F A 0 … 5 vol% 0 … 30 vol% 360 vol%*m 0.1 vol%*m 0.1 vol%*m 5% C G Air
Standard application Process gas Process gas Min. Max. measuring (Max. measur- (DL x path (DL x path Accu-
Effective optical path temperature pressure measuring range ing range x length) length) racy3)
length: 0.3 … 12 m Tmin … Tmax pmin … pmax range (also depen- path length) under stan- At
(with 1 m dent on eff. opt. dard con- 1 013 hPa
Dust load2): ditions1) with cross-
< 50 g/Nm3 eff. opt. path path length:
length) see following without interference
column) cross-inter- of gas 2
ference of
other gases
HF G A 0 … 150 °C 950 … 1 050 hPa 0 … 5 ppmv 0 … 1 500 ppmv 200 ppmv*m 0.1 ppmv*m 0.6 ppmv*m 5 %
At 15 vol%
H2O, 55 °C
H 150 … 250 °C 950 … 1 050 hPa 0 … 5 ppmv 0 … 1 500 ppmv 200 ppmv*m 0.11 ppmv*m 0.6 ppmv*m 5 %
At 150 °C At 15 vol%
H2O, 150 °C
HF H2O H A 0 … 150 °C 950 … 1 050 hPa 0 … 5 ppmv 0 … 200 ppmv 200 ppmv*m 0.1 ppmv*m 0.6 ppmv*m 5 %
At 15 vol%
H2O, 55 °C
H 150 … 250 °C 950 … 1 050 hPa 0 … 5 ppmv 0 … 200 ppmv 200 ppmv*m 0.11 ppmv*m 0.6 ppmv*m 5 %
At 150 °C At 15 vol%
H2O, 150 °C
CO J C 0 … 600 °C 950 … 1 050 hPa 0 … 1.5 vol% 0 … 100 vol% 40 vol%*m 300 ppmv*m 1 500 ppmv 2 %
*m
at 50 vol%
CO2, 20 °C
CO CO2 K D 0 … 400 °C 800 …1 400 hPa 0 … 3.0 vol% 0 … 100 vol% 35 vol%*m 0.06 vol%*m 0.5 Vol% 2 %5)
at 50 vol%
CO2, 20 °C
CO2 L A 0 … 150 °C 950 … 1 050 hPa 0 … 7.5 vol% 0 … 100 vol% 40 vol%*m 300 ppmv*m 2%
H2O M A 0 … 150 °C 950 … 1 050 hPa 0 … 5 vol% 0 … 30 vol% 240 vol%*m 0.1 vol%*m 5%
T 0 … 150 °C 950 … 1 050 hPa 0 … 5 vol% 0 … 30 vol% 240 vol%*m 0.1 vol%*m 5%
1)
All technical data apply to an optical path distance of 1 m in a nitrogen atmosphere under standard conditions 25 °C (or Tmin) and 1 013 hPa. The effective
detection limit, the measuring range and the accuracy can be influenced by process parameters such as pressure, temperature and gas composition. Not all
combinations of maximum pressure and temperature can be realized with the minimum measuring ranges. If the process conditions deviate from the specifi-
cations of the standard applications, special applications are also possible on request.
Please complete the application questionnaire which can be found on the Internet at www.siemens.com/insituquestionnaire.
2)
At 0.3 m effective optical path length, average diameter of the dust particles: 15 µm, specific weight of the dust particles: 650 kg/m3
3)
At least: Detection limit
4)
Up to 200 °C, 5 % above this
5)
Up to 60 vol% CO or up to 60 vol% CO2. Higher CO or CO2 concentrations on request.
6)
At high process temperatures, the use of an IR filter A5E00534668 is recommended for the CD 6 sensor (see page 2/26).
Standard application Min. measuring Max. mea- (Max. (DL x path (DL x path Accu- Purging gas Purging
Effective optical path range suring range measuring length) length) racy4) mode gas
length: 0.3 … 12 m (with 1 m eff. opt. (usually also range x under stan- At 1 013 hPa medium
path length) dependent on path dard condi- with cross-
Dust load3): < 50 g/Nm3 eff. opt. path length) tions1) 2) interference
length: see of gas 1
following
column)
H E G Air
HF H2O H A 0 … 5 vol% 0 … 30 vol% 360 vol%*m 0.1 vol%*m 0.1 vol%*m 5% C G Air
CO J C E G Air, N2
CO CO2 K D 0 … 7.5 vol% 0 … 100 vol% 75 vol%*m 0.15 vol%*m 0.5 vol% at 2 … 5 %5) C G Air
50 vol% CO,
20 °C
CO2 L A C G Air
H2O M A C G Air
T C G Air
1)
At 20 °C, 1 013 hPa
2)
If the smallest permissible process gas temperature of the application is Tmin > 20 °C, the detection limit refers to Tmin and standard pressure (1 013 hPa)
3)
At 0.3 m optical path length, average diameter of the dust particles: 15 µm, specific weight of the dust particles: 650 kg/m3
4)
At least: Detection limit
5)
Depends on temperature (higher values at higher temperatures)
6)
At high process temperatures, the use of an IR filter A5E00534668 is recommended for the CD 6 sensor (see page 2/26).
Special applications
If the process conditions deviate from the specifications of the standard applications, special applica-
tions are also possible on request. Please complete the application questionnaire which can be found at
www.siemens.com/insituquestionnaire on the Internet.
■ Overview
Cross-duct sensors CD 6 and cables for non-Ex applications Purging on the process side with moderate flow
The standard cross-duct sensor consists of a transmitter unit Is selected e.g. for pure gas applications, emission monitoring,
and a detector unit with the same dimensions. The transmitter inerting monitoring. The purging gas flow can be adjusted be-
unit provides a connector for the fiber-optic cable. The laser light tween 0 and approx. 120 l/min at each sensor head using a nee-
is transmitted through this cable. The receiver unit contains a dle valve (included in delivery).
photodetector and an electronics PCB, and is connected to the
2 detector unit by a sensor cable.
The sensors are mounted onto flanges. The easiest way to avoid
condensation and dust deposits on the sensor windows is to use
a purging gas, e.g. with instrument air. Purging must be selected
depending on the application. The cross-duct sensors can
therefore be configured for the respective situation. The applica-
tion reference table provides recommendations for suitable
purging with standard applications.
If a component is to be measured which is also present in mea-
surable quantities in the purging medium - such as oxygen or
moisture - it is necessary to use purging gases such as nitrogen,
superheated process steam or similar. In such cases it is usually
also necessary to purge the sensor heads, since the ambient air Moderate purging on the process side
must also be displaced here out of the laser beam path. A differ- Purging on the process side with increased flow
entiation is therefore made between purging on the process side
and purging on the sensor side. Through omission of needle valve. This type of purging is se-
lected in crude gas applications with higher concentrations of
Note: For measurement of O2 at gas temperatures above particles and/or condensation as well as in non-purified flue
600 °C, it may also be possible to tolerate air as the purging me- gases in combustion plants. The purging gas flow is typically set
dium since its influence on the measurement can be compen- between 200 and 500 l/min on each sensor head depending on
sated. In contrast, the combination O2/temperature always re- the input pressure of the purging medium.
quires O2-free purging.
Applications with oxygen (high-pressure)
For oxygen measurements with a higher process gas pressure
(1 to 5 bar), the sensor CD 6 can be used together with a suitable
window flange as the process connection. This window flange is
also available in the standard sizes DN 65/PN 6, DN 80/PN 16 or
ANSI 4"/150 lbs. The optical surface to the process is made of
borosilicate glass. Flanges can be equipped with window purg-
ing, but without purging tubes. Possible purge modes for the
window flanges are "A-C" (no purging or moderate purging on
the process side). Window flanges are tested for leakage before
delivery using overpressure, and show leakage rates of less
than 10-5 mbarl/s.
Increased purging on the process side
For ordering this application, the MLFB code of the central unit
with the application code "P" must be selected. The process in- Purging on the process side with high flow
terface suitable for the sensors can be chosen by selection of Through use of air blower or dry process steam. Connectors with
the corresponding code in the 6th configurable position of the hose adapters are included in the delivery. An additional
MLFB number. Swagelok adapter must be ordered if a high flow of steam or in-
The most important sensor purging configurations are presented strument air purging is required (option A27). This type of purg-
below: ing is selected in crude gas applications with very high concen-
trations of particles and/or condensation such as in the furnaces
of combustion plants. If instrument air is not available, an air
blower is also an alternative for purging in applications with
lower demands. On the process side, dry steam can be used as
the inert purging gas instead of nitrogen (Tmax. 240 °C). The
purging gas flow is automatically set between 500 and <1 000
l/min on each sensor head depending on the purging air blower
or the steam pressure.
Increased purging on the process side, with hose connection adapter Sensor configuration with high purging on the process side, with 6 mm
joint for use with steam, and with N2 purging on the sensor side
Purging on sensor side
The purging media used on the process side flow through purg-
Can be combined with any purging mode on the process side, ing gas tubes into the process gas flow. The tubes extend a few
and is always selected if the ambient air must never have an in- centimeters into the process area, and usually provide a flow
fluence on the measurement. The volumes within the sensor from the side. This results in a wedge being generated in the in-
head are then continuously purged with an O2-free gas. The flow let zone of the purging gas. The effective measuring path in the
of purging gas required in this case is approx. 1 to 6 l/min and is process gas is therefore well-defined as the distance between
set using a needle valve (included in delivery). The combination the ends of the two purging gas inlet tubes.
shown here of purging with superheated process steam on the
process side and with nitrogen from a compressed gas bottle on
the sensor side may satisfy the necessity for O2-free purging Cross-duct sensor CD 6: Options and accessories
e.g. also in combustion plants with boilers without own nitrogen
network. Sensor alignment kit
Note Includes a battery-operated visible light source, a centering aid
with crosshair, and two hook spanners for opening the optics
With purging on the process side, it may be necessary to use tube of the sensors.
non-return valves to ensure no process gas can enter the purg-
ing gas line in the event of failure of the purging gas supply. This Please note: the sensor alignment kit is not explosion protected.
applies especially in the case of cascaded process and sensor
purging where there is otherwise the danger that, for example,
corrosive process gases could enter the sensor enclosure.
Process wall
2° (maximum)
Electrical connections:
2 230 V AC 50 Hz
or 115 V AC 60 Hz
Ø12
Air
filter
1 ¼” hose connection
CD 6 sensor for
blower air purging
■ Technical specifications
Cross-duct sensor CD 6 Accessories
General information Purging
Design Transmitter and detector units, Nitrogen is permissible as the purging gas for the sensor side. Nitrogen,
connected by a sensor cable steam, air and gases which are not subject to the pressure equipment
directive Cat. 2 are permissible as purging gases for the process side.
Materials Stainless steel, aluminum
Installation
Laser protection class
Vertical or parallel to the gas flow
Class 1, safe to the eye
Purging with instrument air, N2
• Max. overpressure in the sensor < 500 hPa
2
• Quality
Explosion protection II 1 G Ex ia op is IIC T4 Ga,
II 1 D Ex ia op is IIIC T135 °C Da - Instrument air According to
A defined leak rate can only be ISO 8573-1:2010 [2:3:3]
guaranteed when using high- Note: It is sufficient if the pressure
pressure window flanges. Other- condensation point is min. 10 K
wise it may be necessary for the below the minimum ambient tem-
owner to carry out an evaluation perature.
in accordance with ATEX
DEMKO 06 ATEX 139648X; - Nitrogen Purity better than 99.7 %. For oxy-
IECEx UL 13.0029X gen measurements, an O2 con-
tent < 0.01 % in the purging gas
Design, enclosure (optical path length 1 m, min.
5 % oxygen in the process gas)
Degree of protection IP65
• Maximum flow rate 500 l/min
Dimensions Diameter: 163, L: 450 mm (process purging)
Purging gas tube in mm 400 (370 net) x 44 x 40 • Dew point Benchmark: < -10 °C, condensa-
800 (770 net) x 44 x 40 tion on the optics must be
1 200 (1 170 net) x 44 x 40 avoided
2
both ends with SMA connectors.
Cable is flame-retardant, very
good resistance to oil, gasoline,
acids and alkalis, outer sheath
UV-resistant
Cable sheath Oil-resistant polyurethane
Dimensions • For > 500 m, an external power
supply must be additionally or-
dered
• For installation in hazardous
zones, non-intrinsically-safe ca-
bles have to be spatially sepa-
rated from intrinsically-safe lines
• Diameter < 8.5 mm
• Length • Use in non-hazardous and
Ex Zone 2: Up to 700 m
• Use in Ex Zone 0 and Zone 1:
Up to 250 m
Weight 75 kg/km
Maximum tensile force 200 N
Maximum lateral pressure 1 000 N/cm
Impact resistance 200 N/cm
Maximum tensile strength 500 N
Minimum bending radius 12 cm
Climatic conditions
Ambient temperature -40 ... +70 °C during transport,
storage and operation
-5 ... +50 °C during laying
Humidity < 95 % rel. humidity, above dew
point (in operation and storage)
2
25 E
Customer-specific length (specified in complete meters) Z
Language (supplied documentation)
German 0
English 1
French 2
Spanish 3
Italian 4
■ Dimensional drawings
Ø 163 Ø 163
2
105
105
395
395
Ø 6 mm fitting
400 (800, 1 200)
Cross-duct sensor CD 6, moderate purging (instrument air), version Cross-duct sensor CD 6, increased purging (instrument air), version
according to Article No. 7MB6122-**C1*-0***, dimensions in mm according to Article No. 7MB6122-**E1*-0***, dimensions in mm
Ø 163 Ø 163
105
105
2
Test valve
395
395
Cross-duct sensor CD 6, blower purging, version according to Cross-duct sensor CD 6, sensor and process side purging, version
Article No. 7MB6122-**G1*-0***, dimensions in mm according to Article No. 7MB6122-**H1*-0***-Z A27, dimensions in mm
Ø 163
105
Fitting
431
for Ø 6 mm
OD hose
Check valve
Cross-duct sensor CD 6, purged version according to CD 6 high-pressure sensor for oxygen, dimensions in mm
Article No. 7MB6122-*WC14-2***, dimensions in mm
■ More information
For demanding applications it is recommended to keep purging For the suitability of different parts (version 1 or version 2) please
tubes, window modules and detector electronics in stock (quan- consult the instrument manual or contact Siemens directly. In
tities stated per measuring point, i.e. per pair of sensors). general, all new analyzers are compatible with spare parts of
version 2.
■ Overview ■ Benefits
SITRANS SL is a diode laser gas analyzer with a measuring prin- The in-situ SITRANS SL gas analyzer features high operational
ciple based on the specific light absorption of different gas com- availability, unique analytical selectivity, and a wide range of
ponents. SITRANS SL is suitable for fast, non-contact measure- possible applications. SITRANS SL permits measurement of a
ment of gas concentrations in process or flue gases. An analyzer gas component directly in the process:
consisting of transmitter and receiver units (sensors) is used for • With high dust load
each measuring point. The hardware for further processing of
• In hot, humid, corrosive, explosive, or toxic gases
2
the measured signal into a concentration value, as well as the
monitoring, control and communication functions, are integrated • In applications showing strong varying gas compositions
in these two main modules. The sensors are designed for oper- • Under harsh environmental conditions at the measuring point
ation under harsh environmental conditions.
• Highly selective, i.e. mostly without cross-sensitivities
Special features of the SITRANS SL:
• Little installation effort
• Minimum maintenance requirements
• Extremely rugged design
• High long-term stability through built-in, maintenance-free
reference gas cell
• Real-time measurements
Moreover, the analyzer provides warning and error messages:
• When maintenance is required
- With large variations in the reference signal
- With poor signal quality
• If the transmission violates an upper or lower limit
SITRANS SL
■ Application
Applications Sectors
• Control of combustion processes • Chemical and petrochemical plants
• Process optimization • Power plants
• Plant and operator safety • Waste incinerators
• Process measurements in all types of power and combustion • Iron and steel industry
2 plants
• Process control
The following table lists the measuring conditions for standard
applications. The listed values for the measuring range and de-
• Explosion protection tection limit are only approximate values. The exact values at the
• Measurements in corrosive and toxic gases respective measuring point depend on the totality of all influenc-
ing variables and can be determined by Siemens for the specific
• Quality control case. Please note that the values for the detection limit and the
maximum measuring range refer to a path length of 1 m. Longer
path lengths will improve the detection limit, but not linearly. due
to limiting effects such as dust load. The maximum applicable
measuring ranges can only be used if permitted by the process
conditions such as dust load.
Standard application Process gas Process gas Min. Max. Max. DL x path Repeata- Purging
Effective optical path temperature pressure measuring measuring measuring length bility3) gas
length: 0.3 … 8 m Tmin … Tmax pmin … pmax range range range x path (under medium
Dust load2): < 50 g/Nm3 (with 1 m (also dependent length standard
1)
eff. opt. path on eff. opt. path conditions
length) length: see fol- without
lowing column) cross-inter-
ference of
other gases)
Sample Gas Appl.
gas com- code code
ponent
O2 A B 0 … 600 °C 900 ... 1 100 hPa 0 … 1 vol% 0 … 100 vol% 75 vol%*m 200 ppmv*m 2% N2
O2 A C 0 … 200 °C 700 … 5 000 hPa 0 … 1 vol% 0 … 100 vol% 75 vol%*m 200 ppmv*m 2% N2
CO J C -20 … 700 °C 700 ... 2 000 hPa, 0 … 100 ppmv 0 … 6 000 ppmv 2 000 ppmv*m 0.6 ppmv*m 2% Air, N2
max. 300 °C
800 ... 1 200 hPa,
above 300 °C
Reference table: Standard applications. The specified pressures are absolute.
DL = detection limit
1) At 20 °C, 1 013 hPa, without dust
2) With 0.3 m effective optical path length
Average diameter of the dust particles: 15 µm
Specific weight of the dust particles: 650 kg/m3
The influence of dust load is extremely complex, and depends on the path length and particle size. The optical attenuation increases exponentially at longer
path lengths. Smaller particles also have a very large influence on the optical attenuation. With high dust load, long path length and small particle size, the
technical support at Siemens should be consulted.
3) Referred to measuring range.
With stable or externally measured and software-compensated process gas temperature and pressure conditions.
Special applications
In addition to the standard applications, special applications are available upon request. If the process
conditions deviate from the specifications of the standard applications, special applications are also
possible on request. Please complete the application questionnaire which can be found at
www.siemens.com/insituquestionnaire on the Internet.
■ Design
The SITRANS SL gas analyzer consists of a pair of cross-duct
sensors, a transmitter unit and a detector unit, both with the
same dimensions. The complete analyzer is integrated in these
two enclosures. The transmitter unit contains the laser source
whose light is transmitted to the receiver through the measure-
ment path. The detector unit contains a photodetector including
2
electronics as well as a reference cell. The detector unit is con-
nected to the transmitter unit by means of a sensor cable. A fur-
ther cable on the receiver is used to connect the power supply
and the communication interfaces. The receiver enclosure con-
tains a local user interface (LUI) with an LC display which can be
read through a window in the cover. The LUI is operated by re-
mote-control.
Transmitter and detector units
Local user interface (LUI) of SITRANS SL in the detector unit
Special features of the transmitter and detector units: (display of measured value)
• In-situ cross-duct sensors, designed as transmitter and detec-
tor units, connected via sensor cable
• Powder-coated aluminium; stainless steel
• Degree of protection IP65
• Adjustable process connection plates
• Flange sizes (provided by customer): DN50/PN25,
ANSI 4’’/150 lbs
• Purging gas connections (see "Purging")
• Optional: Explosion-protected version in accordance with
- Ex II 2G Ex de op is IIC T6
Ex II 2D Ex tD A21 IP65 T85°C
Parts in contact with the process gas The sensor connecting cable available as a cable set for the
ATEX version as standard, and for non-Ex applications option-
Only the stainless steel and borosilicate window flange of the ally, is offered in lengths of 5, 10 or 25 m. This (optional) cable
sensor is wetted by the process gas. This has optional connec- set also enables permanent installation of an Ethernet cable
tions for purging the process gas side with an appropriate gas- used for service and maintenance purposes.
eous medium.
A rugged cable sleeve should be used as UV protection for in-
Display and control panel stallations in open cable ducts or channel systems.
Special features of the detector unit: The statutory directives must be observed in the event of instal-
• Display for simultaneous output of result and device status lation in hazardous areas.
• LED backlighting of display For the ATEX version of SITRANS SL, the sensor connecting ca-
ble must be connected between the two Ex-e terminal boxes se-
• Remote operation using membrane keypad and softkeys
cured on the transmitter and receiver units.
which are easy to clean
• Menu-driven operation for parameterization and diagnostics
• Remote operation via infrared interface for safe use in hazard-
ous zones
2
requirement, function monitoring, alarms for limit violations of Note:
measured value or transmission) In contrast to the other interfaces, the Ethernet plug-in connector
• Optional: 1 PROFIBUS DP interface with: on standard non-Ex devices is only accessible following removal
- Output of concentration as cyclic data of the detector unit cover. With the help of the sensor connection
- Alarm output, alarm classification cable set (optional with non-Ex devices), an Ethernet cable can
- Input for temperature and/or pressure data for compensation be permanently installed via the terminal box of the sensor con-
The PROFIBUS DP protocol provides DPV0, cyclic data. Mea- necting cable. The Ethernet connection via the sensor connect-
sured values are provided with additional quality data. ing cable can also only be used for temporary service and main-
tenance purposes.
NOTICE:
In an Ex environment, Ethernet connections may only be made
or removed with the permission of the plant operator!
■ Function
Operating principle
SITRANS SL is a gas analyzer employing single-line molecular to a gas-specific absorption line. The laser continuously scans
absorption spectroscopy. A diode laser emits a beam of infrared this single absorption line with a very high spectral resolution.
light which passes through the process gas and is received by The degree of absorption and the line shape are used for the
a detector unit. The wavelength of the laser diode output is tuned evaluation.
Transmitter Receiver
Optics tube (transmitter) Optics tube (receiver)
Laser Detector
Optics Optics Measured Reference Optics Optics
Laser electronics volume cell Reference cell
Electric filter
Electric
interface
Customer Local
interface display
Gas concentration
Flue gas
Process flange composition
- Dimensions Steam Purging tube length
Dust load
Wavelength [nm] - Temperature Gas velocity
Gas temperature
Absorption spectrum of measured signal and reference signal with Transmitter unit Gas pressure Receiver
SITRANS SL
SITRANS SL is designed for measuring oxygen (O2) and carbon
monoxide (CO) at high sensitivity. Measuring
path length
Typical application specifications:
Oxygen concentration 0 ... 21 vol %
Sensor cable
Process pressure/temperature con- 700 ... 5 000 hPa
$EVRUSWLRQOLQH
/DVHUOLQH
Purging tube
(optional)
Sensor connecting
cable (optional)
Remote control
ATEX cable
gland
Cable gland
Conduit connection 1/2” NPT Conduit connection 1/2” NPT Ui: 30.2 V DC
(not shown) (not shown) Pi: 10 VA
Remote control
FM label FM label
Conduit connection 1/2” NPT
(not shown)
2 through which the symmetry axis is aligned. The axis can be off-
set by 1 degree, which means that the process flanges must
be welded onto the process wall with at least this accuracy - see
following figure.
PROCESS
Maximum deviation
± 1°
Process flange
Wall thickness
(incl. insulation)
Dimension B
Dimension A, is measured following installation
Purging tube
Measurement of the optical path length between the ends of the purging gas tubes
Maintenance and fault messages Note
The SITRANS SL carries out continuous self-monitoring, and Specific requirements for the measuring point can make the uti-
outputs alarms and warnings to indicate maintenance require- lization of special sensor equipment necessary. The possibilities
ments or a system fault. The information is output as plain text on for adapting the sensors are:
the LUI display, where symbols identify the category and the se- • Special materials for purging tubes (on request)
verity of the fault.
• Various types/sizes of sensor flanges
Alarm categories: • Explosion-protected sensor configurations
• Maintenance (system must be cleaned or repaired)
Essential characteristics
• Process value (problem with external sensor, or process con-
ditions outside the permissible range for SITRANS SL) • Long-term stability through use of an internal reference cell;
calibration interval at least one year
• Configuration (SITRANS SL is not correctly configured)
• Dynamic background correction for varying dust loads
Severity:
• Isolated signal outputs of 4 to 20 mA
• Fault (measurements could not be carried out)
• User-friendly, menu-driven operation
• Warning (measurements may be inaccurate, or the system will
soon shut down measuring mode if an intervention is not • Selectable time constants (response time)
made) • Password-protected user interface
• Advanced warning/information • I/O operation in accordance with NAMUR recommendations
(measurements are carried out) • Monitoring of overall optical transmission
The two binary (relay) outputs can be configured freely for the • Sensor enclosure resistant to wear and corrosion
alarm output. • Simple local operation using remote-control unit with numeric
The response of the analog outputs in the event of an alarm is keypad and menu prompting
configurable; possible actions are:
• Off (current measured value is displayed)
• Last measured value (freezing of last value displayed)
• Standard level (setting to predefined value)
• 3 mA (NAMUR NE43 fault status)
In addition, the transmission is available as an output variable.
■ Technical specifications
Analytical performance Electrical characteristics
Measuring range Internally adjustable Power supply 24 V DC nominal (18 ... 30.2 V DC)
Detection limit at standardized O2: 200 ppmv Power consumption, maximum 10 VA
conditions: CO: 0.6 ppmv
25 °C gas temperature, 1 000 hPa, EMC In accordance with EN 61326-1
1 m effective optical path length, 3 s Electrical safety In accordance with EN 61010-1
2
integration time and constant ambi-
ent conditions. Fuse specifications T1.6L250V
Linearity Better than 1 % Dynamic performance
(under standard conditions)
Warm-up time at 20 °C ambient Approx. 15 min
Repeatability O2: 1 % of the measuring range temperature
(under standard conditions) CO: 0.5 % of the measuring range Response time (T90) Approx. 2 s,
General information depends on application
Design Transmitter and detector units, Integration time 0 ... 100 s, selectable
connected by a sensor cable Influencing variables
Materials • Sensor enclosure: treated Variations in ambient temperature < 0.5 %/10 K of the measuring
aluminium/stainless steel range
• Process interface: acid-resistant Process gas temperature With compensation: < 1 %/100 K
stainless steel of the measuring range
• Window: hardened borosilicate
glass Variations in atmospheric pressure Negligible
Degree of protection IP65 according to EN 60529 RS 485 PROFIBUS DPV0 version Two-wire interface, up to 3 Mbit/s,
-7 … 12 V
Dimensions For each unit
(transmitter, detector) RS 485 Modbus version Two-wire interface, up to
• Diameter: 165 mm 115 200 bit/s, -7 … 12 V
• Length: 357 mm Cable to customer interface
Purging tube Length, outer diameter, inner (not included in standard delivery, ATEX or optional)
diameter: Analog connection cable 10 x 2, with shielding in twisted-
340, 48, 44 mm (with ATEX configuration: only pair configuration (depending on
Weights supplied cables may be used!) type and number of I/Os used)
■ Accessories
SITRANS SL sensor alignment kit Calibration test kit
The SITRANS SL sensor alignment kit includes a battery-oper- The SITRANS SL has already been factory-calibrated. If it is de-
ated lamp, a centering aid with crosshair, and two hook span- sirable or necessary to check the calibration, this can be per-
ners for loosening the sensors from the flange connection plates. formed using an external calibration test kit following removal of
the transmitter and detector units. This procedure has no influ-
Please note: ence on the optical adjustment of the unit since the flange con-
The SITRANS SL sensor alignment kit is not explosion-pro-
tected! Therefore it must never be used in a hazardous area
nection plates remain mounted on the customer flange. The cal-
ibration test kit for O2 consists of a stainless steel calibration
2
without approval by the plant operator! tube and a thermometer. To carry out the calibration, it is
mounted between the transmitter and receiver. The calibration
tube for O2 can then be filled with air or a calibration gas.
7KHUPRPHWHU
7UDQVPLWWHU 5HFHLYHU
Calibration tube for O2
1HHGOHYDOYHV
$7(;DGDSWHUFDEOH
■ Dimensional drawings
Note
the SITRANS SL sensors must be accessible from the side. A
space of at least 60 cm must be provided next to the SITRANS
SL transmitter and detector units in order to facilitate mainte-
nance and servicing.
Process interface
Purging tube
163
Process flange
2°
SITRANS SL, transmitter/detector unit (same housing for DN50/PN25 process interface version), dimensions in mm
Ø 3/4"
Ø 18 (for 5/8 screwed gland)"
(for M16
screwed gland)
Ø 7½"
Ø 125
Ø 50
Ø 4"
Ø 9"
Connection dimensions of process flanges provided by customer DN50/PN25 and ANSI 4’’/150 lbs
■ Schematics
Electrical connections
Non-EEx version: connection cable - customer interface
Terminal block in the receiver enclosure Function/voltage Ethernet cable
1 + Power supply
19 … 30.2 V, 10 VA1)
2
2 -
3 Normally closed under power4) Binary output 0 (relay)
30 V, 0.5 A3)
4
5 Normally closed under power4) Binary output 1 (relay)
30 V, 0.5 A3)
6
7 + Binary input 0
0 … 30 V2)
8 -
9 + Analog output 0 (measurement)
30 V, 24 mA3)
10 -
11 + Analog output 1 (measurement)
30 V, 24 mA3)
12 -
13 PROFIBUS A line Modbus D1 RS 485
(RxD/TxD_N - data inverted) (RxD/TxD_N - data inverted) (PROFIBUS/Modbus)
14 PROFIBUS B line Modbus D0 -7 ... +12 V DC
(RxD/TxD_P - data not inverted) (RxD/TxD_P - data not inverted)
15 PROFIBUS/Modbus shield
16 T x+ Ethernet5) White/orange
17 T x- Orange
18 Rx+ White/green
19 Rx- Green
20 + Analog input 0 (temperature)
0 … 30 mA2), 120
21 -
22 + Analog input 1 (pressure)
0 … 30 mA2), 120
23 -
24 Grounding
25 Grounding
Ground Grounding
Ground Grounding Shielding
1)
This is the maximum power consumption of the SITRANS SL
2)
These are the maximum input values
3)
These are the maximum output values
4)
Note:
"Normal operation" stands for normal operation of the analyzer. The system is connected to the voltage source and is running without problems;
no error message generated or displayed.
"Normal under power" refers to the status of the relay under the above-named normal operation. The relay contact of the alarm signal is closed.
5)
We recommend that the Ethernet connection is not made via the cable to the Ethernet terminals in the detector unit. Instead, the Ethernet connection should
be made via the sensor cable connection set which is optionally available for the detector unit.
2
4 Com - Gray
5 Sync + Synchronization with transmitter White
Imeas
9
V0
Rload
10
Documentation
Z
Y
X
3/2 Introduction
3/18 MicroSAM
3/27 SITRANS CV
Siemens PA 01 · 2015
© Siemens AG 2014
■ Overview
Process gas chromatography is one of the most powerful
measuring and analysis methods for process engineering. It is a
procedure which is both discrete and extractive. This procedure
is frequently used for online monitoring of processes since the
sequences are easy to automate and a large number of compo-
nents can be measured simultaneously.
Process gas chromatography can be used to separate and
quantify the components of almost all homogenous gaseous or
liquid mixtures. It must be possible to vaporize the liquid compo-
nents without decomposition. The individual components of a
discrete sample pass through the column system at different
velocities, and are recorded in succession by a detector.
The time between sample introduction and registering of a
substance at the detector (the retention time) is characteristic of
the substance and is used to identify it. The magnitude of the
3 detector signal is a measure of the volume concentration of the
component in the gas or liquid.
■ Overview ■ Benefits
MAXUM edition II with its combination of different analytical
components offers a wide range of analytical possibilities. It is
therefore possible to solve highly different measuring tasks with
just one product. This reduces the costs for investment, training
and stocking of spare parts.
The MAXUM edition II platform offers:
• Numerous oven configurations permit an optimum solution for
almost every application
• Numerous types of detector and valve for the optimum
analytical solution
• Intelligent electronics, local operation and central workstation
for fast and simple operation, monitoring and maintenance
• Powerful software for best results
• Comprehensive I/Os and serial interfaces for internal and
central interfacing
• Versatile networking possibilities for central maintenance and
3
secure data transfer
The MAXUM edition II is a universal process gas chromatograph • Many analytical possibilities as result of large application
for flexible process applications with a wide variety of analytical database
possibilities. The MAXUM edition II combines various functional
modules with a flexible oven concept and can therefore also • Large and experienced support team provides global support
optimally solve complex applications. Hardware and software features
The MAXUM edition II is used in all sectors of the chemical Simultaneous applications
industry, petrochemicals and refineries. It analyzes the chemical
composition of gases and liquids in all production phases. The Use one MAXUM edition II to provide the functionality of multiple
MAXUM edition II is suitable for installation in an analysis cabinet GCs.
close to the process or in a close laboratory. Thanks to the
flexible application possibilities, it can be used to analyze the Parallel chromatography
initial material, the end product and also secondary products. Separate complex analytical tasks into simple parallel tasks and
The MAXUM edition II can also be used for many applications shorten analysis times.
with environmental measurements.
Low operating costs
The MAXUM edition II has extremely rugged and specially
designed hardware and software. It automatically takes a Flexible oven concept results in low consumption of air and
sample from the process, and injects this onto the chromato- energy.
graphic columns.
With its powerful software and hardware, it satisfies the highest
demands for measurement repeatability, and can be operated
for a long time without manual interventions. Using powerful
communications tools, the MAXUM edition II can send its results
to process control systems. The comprehensive networking
facilities can be applied to use several MAXUM edition II
chromatographs together in large networks.
Extension of functionality
■ Application
Network Access Unit (NAU)
Chemical industry
• A MAXUM edition II without analytical section
• Monitoring of benzene in styrene in the ppb range
• Available with or without HMI
• Traces of residual gases in ultra-pure gases
• Has 7 slots for optional I/O plug-in cards
• Determination of traces of hydrocarbons in air separation
• Offers central MODBUS connection of several chromato-
plants
graphs to the control system
• Fast analysis of CS2 and H2S in seconds
• Fast measurement of C6 to C8 aromatic compounds including
the measurement of C9+ aromatics
■ Function
• Monitoring of hydrogen in chlor-alkali plants Supply with carrier gas, combustion gas and auxiliary gases
• Measurement of sulfurous components A gas chromatograph must be supplied with carrier gas and,
if applicable, combustion gas and other auxiliary gases
• Measurement of C9 to C18 paraffins depending on the analytical configuration. The carrier gas is
• Determination of vinyl chloride in room air in a 60-second used to transport the sample through the analytical system.
cycle Auxiliary gases are used to operate valves, as combustion
3 • Gas analysis during manufacture of vinyl chloride monomer
(VCM)
gases for flame ionization detectors, and to purge the oven.
Injection system
Oil & gas The injection system is the link between the continuous process
• Crack gas analysis stream and the discrete analytical process. It is responsible for
• Natural gas: Trace analysis for components such as injecting an exactly defined portion of the sample in a repro-
mercaptans, H2S or COS ducible and pulsed manner (as far as possible) into the carrier
gas stream.
• Fast determination of benzene in naphtha
The injection can be carried out in the conventional manner
• Determination of high boiling aromatics in a distillation fraction using valves or by means of a live injection:
• Fast measurement of acetylene in ethylene • Gaseous samples (0.1 to 5 ml)
• Total sulfur in petrol and diesel • Completely vaporizable liquid samples (0.1 to 10 µl)
Water/waste water Gas injection valves
• Determination of halogenated hydrocarbons
Model 50 10-port valve:
• Simultaneous determination of chlorinated hydrocarbons,
aromatics and alcohols in water • Combined gas injection and backflushing valve
• Wastewater monitoring with PGC and stripper • Activation by pressure on the membrane without moving parts
• Can be used as gas injection valve or for column switching (6-
Power engineering port connection)
• Power generation in coal-fired power plant. • > 3 million switching cycles without maintenance
Automotive industry Model 11 6-port valve:
• Fast analytical measurement of methane in car exhausts • Can be used as gas injection valve, liquid injection valve or for
• High-speed chromatography for small molecules in propel- column switching
lants • Membrane controlled by tappet
• One million switching cycles without maintenance
■ Design
Chromatographic measuring equipment consists of a sampling
system matched to the application, sample preparation with
switchover to various sample streams if necessary, and the gas
chromatograph with the analytical and electronic hardware as
well as data processing, operation and communications
software.
The MAXUM edition II gas chromatograph is divided into three
sections depending on the version:
• The upper section contains the electronics with the power
supply, controllers and analog electronics
• The middle section contains the pneumatics and some of the
detectors (not with MAXUM edition II modular oven version)
• The bottom section contains the oven and the complete
analytical components responsible for the separation
The MAXUM edition II is available prepared for wall mounting or
for free mounting on a rack.
NV- NV+
Air
SV1
3
Q+ Q-
Sample
DV
A Sample
Carrier gas
Heating
NV1 WLD
R
M
Split
Live injection
Liquid injection valve FDV
Features:
• Vaporization temperature 60 to 350 °C
• Injection volume 0.1 to 9.5 l
• Sample temperature -20 to +150 °C
• Material of parts wetted by sample: Stainless steel, mat.
no. 1.4571, Hastelloy, Monel or special materials
• Control pressure 400 to 600 hPa
• Max. sample pressure 6 000 kPa, recommended 50 to
100 kPa
• Connections for pipe: 3.14 mm (1/8") outer diameter
3 • temperature-programmed mode
chromatographically traced "online".
Columns
Both types of oven are available as
• single ovens or The columns are the central component of the chromatograph.
They resolve the gas mixture or the vaporized liquid into its
• dual ovens. individual components. The following distinction is made:
With the dual ovens, two separate heating circuits provide • Packed/micropacked columns with inner diameter of 0.75 to
independent oven temperatures. It is then possible to use two 3 mm
different temperatures for the respectively installed columns for • Capillary columns with inner diameter of 0.15 to 0.53 mm
one application or to carry out two or more applications in one
chromatograph with different temperatures for the separation. Packed columns are mechanically stable and simple to handle.
Capillary columns have a significantly higher separating perfor-
In order to measure sample components with highly different mance, often with a shorter analysis period and lower analysis
volatilities, a temperature program is frequently used for the temperature.
chromatographic separation. In this case the column
narrow-bore 0.15 mm
Packed column 3 mm
narrow-bore 0.32 mm
wide-bore 0.53 mm
Types of column
D D D D D D D
&RQWUROJDV
6DPSOHJDV
3
Live switching
Solenoid valve control module Detectors
• Contains all control elements in one module in order to reduce Thermal conductivity detectors (TCD) and flame ionization
downtimes during repairs to a minimum detectors (FID) are mainly used in process chromatography.
• Has 3-way and 4-way distributors for control of many different Specific detectors such as flame photometer detector (FPD),
types of valve electron capture detector (ECD), photo-ionization detector
• Uses separate, plug-on pipe connectors to permit implemen- (PID), or helium ionization detector (HID) are used to a lesser
tation of variable gas supplies extent.
Electronic pressure controller module (EPC) The detector modules described above can be combined
together in many different manners in the MAXUM edition II.
• Permits exact control of pressure without mechanical pressure
regulator. Shortens the setup time since the pressure is set by • A maximum of three detector modules can be used in the
an operator input. airbath oven.
• Permits programmable pressure changes for fast chromatog- • Up to three modules (depending on the type) can be used in
raphy and modern applications. the airless oven, the dual airless oven and the ovens with
temperature programming.
• Controls the supply of carrier gas and combustion gas. Avoids
drift and deviations which can occur with mechanical • Thermal conductivity detectors (TCD) are used in the modular
pressure control. oven system.
• In the case of multiple modules such as the TCD, the
measuring cells can be operated in parallel at offset times in
order e.g. to increase the number of analyses within a specific
time.
• Multiple modules can each be used with a column system for
one sample stream. This shortens the total cycle time with
multi-stream applications.
• Parallel use of two identical column systems provides
redundant measurements which can be compared with each
other, thus reducing the necessity for calibration.
3'+,'
3'(&'
3'3,'
■ Technical specifications
MAXUM edition II classic oven Configuration
General Oven options • Single isothermal oven or divided
oven with two independent isother-
Smallest measuring ranges • Thermal conductivity: mal zones
(depending on application) 0 ... 500 ppm • Single oven or two independent,
• Flame ionization: 0 ... 1 ppm airless ovens. The dual version has
Temperature range in oven Application-specific, depending on two separate oven areas with sep-
temperature class 5 ... 350 °C arate doors which operate com-
depending on oven version and pletely independently.
temperature class Detector modules for Thermal conductivity, flame ioniza-
Temperature control ± 0.02 °C tion, flame photometry, helium ion-
ization, photo-ionization and
EMI/RFI design • CE-compatible; certified accord- electron capture
ing to 2004/108/EC
(EMC directive) Number of detector modules • 1, 2 or 3 in any combination of
• CE-compatible; certified detector module types for airbath
according to 2006/95/EC ovens
(low-voltage directive) • 1, or 2 in any combination of detec-
3
• Tested according to tor module types for airless ovens,
EN 61010-1 / IEC 1010-1 up to 3 in special configurations
Calibration Comparison measurement with Sampling and column valves Diaphragm valves, diaphragm pis-
external standard ton valves, sliding vane rotary
• Type Manual or automatic valves, slider valves, or liquid injec-
tion valve
• Zero value Automatic baseline correction
• Span Standard sample cylinder (single or Valveless option Live switching
multipoint calibration possible) Columns Packed, micropacked or capillary
Design, enclosure columns
Mounting • Spacing on left: 460 mm from walls Regulation of gas supply Up to 8 electronic pressure regula-
and other devices tor channels and up to 6 mechanical
• Spacing on right: 460 mm in all pressure regulators
cases Electrical characteristics
• Spacing at front: 654 mm in all
cases Power supply • Single-phase AC, 100 ... 130 V
• Wall-mounted units or 195 ... 260 V (selectable),
• Center-to-center: 1 120 mm in all 47 … 63 Hz
cases • Single oven: max. 14 A
• Dual oven: 2 circuits,
Weight 77 kg max. 14 A each
Degree of protection IP54, Category 2 Gas inlet conditions
Danger class Standard configurations: Sample flow 5 ... 100 ml/min (depending on
• Certified according to ATEX with application)
air or nitrogen purging for Zones 1
and 2 (EEx pyedmib IIB + H2) Sample filter size 0.1 ... 5 µm with gaseous samples
• Suitable for use in non-hazardous depending on type of valve
areas and with non-dangerous Max. 0.3 µm with liquid samples
conditions
• Certified according to CSA C/US Minimum sample pressure 35 kPa, standard
for use in Class 1, Div. 1, Groups Maximum sample pressure 200 kPa standard, higher pressure
B, C, D with air or nitrogen purging as option
• Certified according to CSA C/US
for use in Class 1, Div. 2, Groups Maximum sample temperature 121 °C standard; higher tempera-
B, C, D. ture as option
Important note! Materials wetted by sample Stainless steel and Teflon; other
Use in non-hazardous areas materials as option
requires purging of the electronics Liquid injection (valve)
area with air or nitrogen.
PDD is not certified for hazardous Vaporization temperature 60 ... 350 °C depending on applica-
areas. tion and temperature class
Injection volume 0.1 ... 9.5 l
Sample temperature -20 ... +150 °C
Material of parts wetted by sample Stainless steel, mat. no. 1.4571,
Hastelloy, Monel or special materials
Control pressure 400 ... 600 kPa
Sample pressure Max. 6 000 kPa, recommended
50 ... 100 kPa
Connections for pipe 3.14 mm (1/8") outer diameter
3
application) • Typical consumption quantity:
2 000 l/month per detector
Electrical inputs and outputs module
Standard input and output • 2 analog outputs; Combustion air • Reference air (< 1 ppm THC,
• 4 digital outputs (1 for output of O2 concentration 20 … 21 %).
system faults, 3 are user-configu- Supply through instrument air with
rable); catalytic purification (optional).
• 4 digital inputs; • Typical consumption quantity:
• 3 serial outputs 26 000 l/month
Card slots for optional inputs and 2 Corrosion protection • Purging with dry air to protect the
outputs via internal I2C bus electronics
• Air bath oven with stainless steel
Input and output cards A IO 8: 8 analog outputs, 8 analog
lining
inputs, 2 digital inputs
• Airless oven made of aluminum
D IO: 6 digital inputs and 8 digital • Steel lining painted on outside
outputs (epoxy powder coating)
AD I/O: 4 digital inputs and 4 digital Communication
outputs, 4 analog inputs and 4 ana-
log outputs Serial output RS 232, RS 485, e.g. Modbus
Digital inputs Optocoupler with internal power Ethernet Standard 10/100 BaseT Ethernet
supply (12 … 24 V DC); switchable with 4 RJ 45 connectors
by dry contacts. e.g. Modbus TCP IP or OPC
Alternative: switchable by external Optional
power supply 12 … 24 V DC (only ESBF board
dry relay contacts), external power
supply, negative connection linked Fiber-optic 100Base FX multimode
to ground, for a specific digital with ST connection
input. 3 x RJ45 and 1 x optical or
Digital outputs Dry changeover contacts, max. con- Scalance network components e.g.
tact rating: for redundant connections.
1 A with 30 V DC.
Diode bypass suppression should
be used for inductive loads.
Analog inputs -20 ... +20 mA into 50 or
-10 ... +10 V Rin = 0.1 M, alternate
insulation up to 100 V
Analog outputs 0/4 ... 20 mA into max. 750 , com-
mon negative pole, electrically iso-
lated from ground; freely-
connectable to ground
Termination Screw terminal for shielded or solid
cable with a maximum area of
18 AWG or 0.82 mm2
■ Dimensional drawings
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■ Overview ■ Application
Chemical industry
• Analysis of ethylene in 1.2-dichloroethane (EDC) for process
control
• Fast determination of nitrogen in acetylene for process control
• Hydrocarbon analysis of starting product (LPG) of a cracker
• Safety measurement of ethylene oxide during unloading of
tankers
• Multicomponent analysis in ethylene oxide
• Analysis of methanol, water and dimethylether in a pilot plant
• Monitoring of coolant: Trace monitoring in chloromethane
• Analysis of nitrogen and hydrogen in pure gas of a chlor-alkali
plant
Oil & gas
3 • Hydrogen analysis in recycled gas and other process gases
• Analysis of inert gases and low-boiling paraffins/olefins in
combustion gas
• Analysis of hydrogen and low-boiling hydrocarbons in
The MicroSAM is a miniaturized process gas chromatograph reformer/platformer plant
(GC) in an Ex d enclosure. Through consistent use of micro- • Trace analysis of impurities in acetylene from a cracker
system technology (silicon wafer technology), all analytical
components are concentrated in the smallest possible area. • Analysis of ethane in ethylene from a cracker
The design particularly enables a distributed installation close to • Measurement of calorific value in exhaust gas for quality
the process. control in a power plant
• Analysis of ethylene in methane in an ethylene plant
■ Benefits • Analysis of propadiene and propine in the C2 splitter of a
• The distributed field installation reduces investment costs, steam cracker
and opens up new fields of application, e.g.: • Analysis of low-boiling hydrocarbons in an ethylene plant/
- Installation in plant areas where mounting within an analyzer visbreaker
shed is not possible
- Installation at remote locations without extended infra- • Analysis of exhaust gas in flares
structure • Analysis of gas loop in a propylene oxide plant
• Reduction in laboratory analyses through online measure- • Analysis of CO in crack gas in an LDPE
ments (low-density polyethylene) plant
• Low space requirements in analysis cabinets reduce • Analysis of refinery gas in a pilot plant
investment costs • Analysis of calorific value in natural gas preparation plants
• Low maintenance effort and gas/energy consumption reduce
operating costs Iron & steel
• High-resolution capillary columns permit fast analyses Analysis of exhaust gas in blast furnaces.
• Live injection permits representative sample injections Pharmaceutical industry
• Maintenance-free, valveless separating column switching • Analysis of O2, N2, CO2 and water in fermenting processes
with electronic pressure controllers • Analysis of alcohols in nitrogen for vacuum drying plants
• The use of several micro thermal conductivity detectors
(multidetection) provides exact measuring results and also Metals, aggregates, cement
validation possibilities Analysis of mine gas for inert gases and hydrocarbons.
• Versatile networking possibilities for central maintenance and
secure data transfer
• Remote monitoring with Windows-based software and
Ethernet communication
• Simplified servicing through replacement of modules
3
(e.g. on all column/purging outputs and injection) Detector
The micro TCDs (based on silicon wafer technology) work on the
■ Function principle of continuous measurement of the different thermal
conductivities of the carrier gas and the components to be
Live injection measured.
The MicroSAM has a two-stage injection system. Using a micro The measurement can be carried out without falsification by
injection valve, a defined quantity of sample is first brought up to avoiding catalytic effects on the heating wires and maintaining a
the carrier gas pressure. This eliminates the pressure- constant flow velocity. This permits consistent in-line detection,
dependent error in the dosing quantity present with conventional i.e. without qualitative or quantitative losses of substances.
systems. In the second stage, the sample is transferred to the
column by a valveless micro injection system (live dosing). The Application modules
result is an "active" injection.
The application modules contain live injection and live switching.
The injection volume can be varied time-controlled, and exactly The modules D06, D08 and D11 have one separating column
matched to the column requirements. less than the modules D01, D02 and D09. The modules D06,
D08 and D11 have one detector less than the modules D01 and
Valveless live column switching D02. The application modules are suitable for separation of the
Because of the high dead volume of conventional valves, only components described below. However, when defining the
the valveless version can be considered for a miniaturized suitable application module for an actual, customer-specific
system. In this case, the generation of differences in flow using measuring task, technical evaluation by our Support Team is
several electronic pressure regulators at appropriate positions of required.
the column setup causes a change in the flow directions. D01, D02 and D08:
(The system operates according to the Wheatstone principle, These modules contain separating columns that can be
but pneumatically.) The functions "Cut" and "Backflushing" can impaired in their separating performance by humidity in the
then be implemented free of dead volume. carrier gas. For this reason, a carrier gas dry filter (filter set:
Article No. A5E00400116) is integrated for these modules on the
support bracket of the MicroSAM or supplied as a separate part
as standard.
The application modules are suitable for separation of the
components described below.
Detector Column 1 Detector Column 2 Detector Circuit Column 3 Detector
D01
Injection TCD Sil5 C3, C4, C5, TCD PoraPLOT/Porabond Q TCD Live Molecular filter TCD
C6+ CO2, C2, H2S, H2O H2, (Ar+O2), N2,
C1, CO
D02
Injection TCD Sil5 C5+ TCD SilicaPLOT TCD Live Molecular filter TCD
C2, C3, C4 (saturated, H2, (Ar+O2), N2,
unsaturated), C5+ C1, CO
D09
Injection - Sil5 TCD Sil5 TCD Live Porabond Q TCD
Non-polar aromatic Non-polar aromatic All components
and aliphatic hydro- and aliphatic except molecular
carbons hydrocarbons filter components
■ Technical specifications
Design, enclosure Sample and injection
Weight 15 kg Sample streams 3
Degree of protection IP65 (NEMA 4X) Calibration sample streams 1
Mounting Phase Gaseous
Installation on Post, pipe or wall Required filtration Degree of separation 99.99 % for
< 0.1 m particles
Distance from wall or next chromato- 300 mm (12")
graph Material with which the sample comes Stainless steel, fused silica,
into contact polyimide
Distance from ceiling or floor 200 mm (8")
Injection "Valveless" live injection
Explosion protection ATEX and IEC Ex: II 2 G Ex d IIC T4
Gb • Controller With multifunctional diaphragm
valve
Class I, Zone 1, Group IIB + H2 T4 • Injection volume adjustable using 2 ... 50 µl
Class I, Div 1, Groups B, C, D T4 switching times
Factory Sealed • Max. operating temperature 165 °C
3
Support bracket Oven
• Mounting part, dimensions (D x H) 380 x 110 mm Number/type 1/isothermal
• Gas connections 8
Purging with N2 Possible
• Bracket for gas connection, dimen- 146 x 110 mm
sions (D x H), bracket on right side, Dimensions (DxH) 160 x 10 mm
mounted at right angle
Heating capacity 20 W
Electrical characteristics
Temperature range 60 … 155 °C
Power supply 24 V DC (18.5 ... 30.2 V)
Temperature stability ± 0.1 K (60 ... 155 °C)
Power consumption
Temperature accuracy ± 3 K (60 ... 155 °C)
• Typical 18 W
• Maximum 60 W Retention time variations per 10 °C Approx. 0.3 %
• Electrical safety IEC 61010 / DIN VDE 0411 change in ambient temperature
EMC immunity According to IEC 60801/ Heating-up period from 30 ... 100 °C 10 minutes
DIN VDE 0843 Columns and gases
• Conducted interferences on AC
supply lines Column type Capillary columns 0.15 ... 0.25 mm/
internal
- According to Part 4 (burst) 2 kV
- According to Part 5 (ms pulses), 1 kV Separating column switching Multidimensional chromatography
line against line with backflushing and cut in live sys-
- According to Part 5 (ms pulses), 2 kV tem
line against ground Multifunctional diaphragm valve For injection and backflushing
• Conducted interferences on signal
lines Gas connections Swagelok 1/8"
- According to Part 4 (burst) 1 kV Pressure regulators Max. 4 single-channel electronic
• Immunity to static discharge pressure regulators
- According to Part 2 (ESD) 8 kV Solenoid valves for control of dia- 2 NC contacts, 2 NO contacts
• Immunity to fields phragm valve
- According to Part 3 and Part 6 10 V/m Carrier gas H2, N2, He, Ar
• Noise suppression According to CISPR 11 / EN 55011 / • Gas purity (minimum requirement) > 99.999 % (5.0)
DIN VDE 0875 Limit class B
• Solid components < 0.1 m
• Fuse T2.5 A
• Required filtration Degree of separation 99.99 % for
Gas inlet conditions < 0.1 m particles
Permissible sample pressure 10 … 60 kPa above atmosphere • Consumption 10 ... 60 ml/min
• Inlet pressure 500 …700 kPa (g)
Sample flow 20 … 100 ml/min 600 kPa (g) recommended
Max. sample temperature 120°C Important:
A continuous carrier gas supply is
Solid components < 0.1 mm required for error-free operation (fre-
Climatic conditions quent carrier gas failure has a nega-
tive effect on the life cycle of the
Permissible ambient temperature - 20 ... 50 °C (depending on oven detectors and the internal device
temperature) pressure regulator. In addition, an
external two-layer pressure regula-
Permissible storage/transport temper- - 30 ... 70 °C
tor for the carrier gas pressure is
ature
strongly recommended.
Permissible relative humidity Max. 90 %
Instrument air Not required
3
3 sample streams + 1 calibration stream; controlled by 4 internal Note:
digital outputs (relay contact 0.4 A / 24 V DC)
If the delivery is to include a protective casing from the Set CV
Pos. 8_0: For gaseous sample range, please refer to this category in Catalog PA 01. There you
This position contains a basic unit prepared for integration of the can find more information on the I/O Extender and its specifi-
analyzer modules. cation within this total solution.
J0X – Acceptance and customer information H0X - Various calculations and functions using
BASIC interpreter integrated in the GC
The scope of delivery is checked and the documentation and
operation of the device explained in detail during the factory The BASIC programs are either preset ex-works or can be
acceptance. created and modified by the customer.
This also comprises presentation of the analytical solution H01 – MicroSAM BASIC Editor
including communication, chromatograms, piping plan and gas The MicroSAM BASIC Editor allows individual programming of
path plan. If present, inspection of the sample preparation and calculations and functions by the user.
discussion of the documentation are carried out.
Please supplement the order for J02 to J04 by the desired option
from E0x.
Only experienced MicroSAM users should consider the option
for starting up the MicroSAM in the context of remote accep-
tance, e.g. using a telephone conference (on request).
E0x – Repeatability test
Proof of repeatability over a period of 2 h is included as
standard. Longer proof of repeatability for the unit can be
ordered using the supplements E02 to E04.
3
dance with the standard: calorific value, relative density and Isobutane 0.5 0.5 0.1
compressibility factor.
Isopentane 0.3 0.3 –
The calorific value is calculated as standard in BTU/ft3 (S) Isopentane – – 0.1
referred to the reference temperature 60 °F. Calculation on the
basis of other reference variables or tables (in accordance with Carbon dioxide 2 2 –
the standard) requires unambiguous specification by the Methane Approx. 85 Approx. 0.1
customer. 84.5
The BASIC program is preset ex works; a customer modification Methyl acetylene – – 0.1
is only possible with the supplement H01. n-butane 0.5 0.5 0.1
■ Dimension drawings
156 200 70
12
300
3
20
40 34
85 306 20
L = 4 000 mm
1 5
40
220
40
4 8
D 10 (4x)
MicroSAM, dimensions in mm
■ Overview ■ Design
Enclosure
• EEx-d version standard
• Heating adjustable from 60 to 165 °C (isothermal)
• Decentralized installation close to sampling point
Analytical modules
The compact analytical modules contain all the functional
components of a chromatograph. The SITRANS CV operates
with:
• Live injection
• Valveless live switching on microchip basis
• Standardized analytical modules
• Multidetection through use of up to 8 micro thermal
3
conductivity detectors in smallest possible areas
(e.g. on all column/purging outputs and injection)
Like the MicroSAM, the unit’s high analytical capability can be By using narrow-bore capillary columns, the separation at high
attributed to narrow-bore capillary columns, live injection, live resolution is carried out within a much shorter time, approx.
switching and in-line detection. factor 2 to 3 compared to standard capillary columns.
Electronic pressure regulators
■ Application A high pressure stability together with rapid changing rates in
• Analysis of natural gas in power plants: the hPa range are required for precise and fast switching. This is
- For quality control achieved in the electronic pressure regulators by means of a
- For turbine optimization piezo actuator.
- Pipeline monitoring
Detector
• Analysis of natural gas when opening up sea beds
(off-shore plants). The micro TCDs (silicon wafer technology) work on the principle
• Analysis of bio-natural gas in preprocessing plants of continuous measurement of the different thermal conductiv-
ities of the carrier gas and the components to be measured.
• Analysis of natural gas in liquefaction and regasification plants
(LNG Regasification and Storage) The measurement can be carried out without falsification by
avoiding catalytic effects on the heating wires and maintaining a
• Determination of calorific value in natural gas for power plants,
constant flow velocity. This permits consistent in-line detection,
in gas transfer stations, or during turbine optimization
i.e. without qualitative or quantitative losses of substances.
• Analysis of calorific value in natural gas preparation plants
Modules
The standardized application modules generally feature live
injection and live switching functions, detectors and separation
columns.
Detector Column 1 Detector Column 2 Detector Circuit Column 3 Detector
C09 Sil5 TCD Sil5 TCD Live Porabond Q TCD
Injection Non-polar aromatic and Non-polar aromatic All components except
aliphatic hydrocarbons and aliphatic hydrocar- molecular filter compo-
bons nents
C01 TCD Sil5 TCD PoraPLOT/Porabond Q TCD Live Molecular filter TCD
Injection C3, C4, C5, C6+ CO2, C2, H2O H2, (Ar+O2), N2, C1,
CO
C13 TCD RTX-1 TCD HayeSepN TCD Live
Injection C3, i-C4, n-C4, neo-C5, N2, CH4, CO2, C2
i-C5, n-C5
Sum C6+ as sum peak
3
in the backflush
For analysis of natural gas with backflush summation, the Measurements within the scope of the possible working ranges
following components and working ranges are measured: (Table 1 "Measured components and performance parameters
Component Possible working range (%)
for Pos. 8_0 (Master setup, standard analysis of calorific value in
accordance with ISO 6976-1995)", right column, and Table 2
Methane 50 ... 100 "Measuring range of the additional measured component
Nitrogen 0 ... 25 oxygen of the extended analysis of calorific value (see Article
No. 7KQ3105-1)") are possible. However, checking of the
Carbon dioxide 0 ... 20
repeatability and correctness has not been carried out by the
Ethane 0 ... 20 official German body "Physikalisch technischer Bundesanstalt
Propane 0 ... 15 (PTB)".
i-butane 0 ... 10 Concentration range (mol.%) Repeatability according to ISO
n-butane 0 ... 10 6974-5 (2001); Mol fraction (%),
absolute
Neopentane*
50 < xi < 100 0.03 ... 0.035
i-pentane 0 ... 1
1 < xi < 50 0.011 ... 0.03
n-pentane 0 ... 1
0.1 < xi < 1 0.006 ... 0.011
Hexane+ 0 ... 3
3
xi < 0.1 < 0.006
Helium Concentration can be entered as a
fixed value in the component list Table 5: The repeatability of the measured components complies with
ISO 6974-5 (2001) – Annex B (Article No. 7KQ3105-0, 7KQ3105-1)
H2S No measured component
High/low calorific value Calculated The repeatability of the calorific value and standard density
achieve a relative standard deviation of < 0.01 %. SITRANS CV
Density and relative density Calculated
for the analysis of biomethane achieves a relative standard
Wobbe index Calculated deviation of < 0.05 %.
Compressibility factor Calculated The calibration gas is an extremely important factor for consid-
Normalization factor Calculated eration in terms of the MPE (maximum permissible error), and
has a significant effect on the accuracy of the overall measuring
Table 4: Component and measuring ranges for the analysis, including system. For this reason, SITRANS CV - based on a comparative
backflush summation measuring procedure - can never be more accurate than the
* Because the neopentane concentration is very small in practice, this calibration gas used. Other parameters besides the accuracy
component is not calibrated and is measured with the relative response data on the calibration gas certificate are important for the
factor of isopentane. For this reason, a possible working range is not
indicated. accuracy of a system. Examples of these include the optimum
gas composition, the ambient temperatures of the calibration
Analyses within the checked working range as well as the quality gas cylinders during transportation and operation, potential
parameters resulting from these (upper and lower calorific condensation of, for instance, higher hydrocarbons in a
values, density and relative density, Wobbe index, compression calibration gas cylinder, and the functionality of the sample
and normalization factors) correspond to the requirements listed preparation system.
below.
Under optimum conditions, the SITRANS CV achieves an MPE of
< 0.1 % for the calorific value and the standard density, whereby
the system for measuring biomethane produces an MPE of
< 0.5 %.
SITRANS CV is designed for measuring with various configura-
tions; the calibration gases required for this purpose are shown
below. (Table 6, Measurement and calibration gas components):
3 Propane
Isobutane
M CR
M CR
M CR
M CR
-
-
M CR
M CR
M CR
M CR
Butane M CR M CR - M CR M CR
Neopentane M*1 M*1 - - M*1
Isopentane M CR M CR - - M CR
Pentane M CR M CR - - M CR
Group C6+ M*2 CR M*2 CR - - -
Group C6+ backflush - - - - M*2 CR
Extended application 7KQ 3105- B02
Separate measure- M*3 CR*3 M*3 CR*3 - - -
ment of Group C6 and
Group C7+
Separate Groups C6, M*4 CR*4 M*4 CR*4 - - -
C7, C8, C9
Caution! Use of the SITRANS CV with a carrier gas different to that of the supplied solution can lead to faults and to the destruction
of the analysis module. Depending on the composition of the calibration gas, external heating for the calibration gas cylin-
der may be necessary.
M Measured
CR Required as calibration component; composition see catalog PA 01 – SITRANS CV - Function
M*1 Neopentane is measured with the response factor of isopentane;
for direct calibration of neopentane: see operating instructions
M*2 Group C6+ is measured with the relative response factor of n-hexane
M*3/CR*3 Groups C6 and C7+ are measured separately and calibrated with n-hexane and n-heptane, respectively
M*4/CR*4 Group C6, Group C7, Group C8, Group C9 are measured and calibrated separately
Table 6: Overview of device versions and available measurement configurations and the calibration gas compositions required for them
■ Technical specifications
Climatic conditions
Permissible ambient temperature -20 ... +55 °C (depending on oven
temperature)
Permissible storage/transport -30 ... +70 °C
temperature
Permissible relative humidity Max. 90 %
Protection against dust and moisture
• According to EN 60529/IEC 60529 IP 65
• According to NEMA 250 NEMA 4X
Power supply
Power supply 24 V DC (18.5 ... 30.2 V)
External fuse T2.5 A
Power consumption, typical 18 W
3
Power consumption, maximum 60 W
SITRANS CV with SIMATIC Extension Unit Dimensions and weights
Width x depth x height 360 x 300 x 220 mm
(approx. 14" x 12" x 9")
Weight 15 kg (35 lb.)
Mounting
Installation on Post, pipe or wall
Distance from wall or next chromato- 300 mm (12")
graph
Distance from ceiling or floor 200 mm (8")
Electromagnetic compatibility
Noise suppression According to CISPR 11 / EN 55011 /
DIN VDE 0875 Limit class B
EMC immunity According to IEC 60801/
DIN VDE 0843
Conducted interferences on AC
supply lines
• According to Part 4 (burst) 2 kV
• According to Part 5 (ms pulses), 1 kV
line against line
• According to Part 5 (ms pulses), 2 kV
line against ground
Conducted interferences on signal
lines
• According to Part 4 (burst) 1 kV
Immunity to static discharge
• According to Part 2 (ESD) 8 kV
Immunity to fields
• According to Part 3 and Part 6 10 V/m
Safety
Electrical safety IEC 61010 / DIN VDE 0411
Explosion protection ATEX and IEC Ex:
II 2 G Ex d IIC T4 Gb
Class I, Zone 1, Group IIB + H2 T4
Class I, Div 1, Groups B, C, D T4
Factory Sealed
Oven
Number/type 1 / isothermal
Purging with N2 Possible
Dimensions (D x H) 160 x 10 mm
Max. heating power 35 VA
Temperature range 60 … 165 °C
Temperature stability ± 0.1 K (60 ... 165 °C)
Temperature accuracy ± 3 K (60 ... 165 °C)
Retention time variations per 10 °C Approx. 0.3 %
change in ambient temperature
Warm-up period from 30 … 100 °C 10 minutes
Multifunctional diaphragm valve For injection and backflushing Calibration Manual or automatic, single level
Gas connections Swagelok 1/8" Repeatability for calorific value and 0.01 % (for natural gas)
density
Pressure regulators Max. 4 single-channel electronic
pressure regulators Accuracy for calorific value and 0.1 % (for natural gas)
density
Solenoid valves for control of 2 NC contacts, 2 NO contacts
diaphragm valve Linear range Typically 104
Calibration sample streams 1 Control system coupling 1 x Modbus RS 485/RS 232 RTU/
ASCII
Phase Gaseous
Inputs/outputs: Basic equipment
Permissible sample pressure 10 … 60 kPa above atmospheric
pressure Digital outputs 4, 3 x samples, 1 x calibration
NOTICE: Sample must not contain (relay contact 0.4 A/24 V DC)
ethine (acetylene).
Digital inputs (24 V to optocoupler) 4, for 1 = sample flow;
Sample flow 20 … 100 ml/min 2 = time synchronization;
3 = revision (results have no effect
Max. sample temperature 120 °C on average values);
Solid components < 0.1 m 4 = calibration
3
(N2, CO2, O2, C1-C5, C6+) Particularly in warmer zones, weather protection is necessary to
For calorific value analysis with biomethane 2 protect the SITRANS CV against direct solar radiation.
(N2, H2, CO2, O2, C1-C4) The chromatograph is designed as standard for temperatures
For calorific value analysis (N2, CO2, C1-C5, C6+) 3 from -20 to +55 °C. A version in a thermostatically-controlled
backflush summation casing is also available as an option for temperatures outside
these limits.
Additional versions Order code
Add "-Z" to Article No. and specify Order code Communication
Russian configuration SITRANS CV has a serial interface (RS 485/RS 232) for MODBUS
communication (RTU/ASCII). Modbus mapping can be flexibly
Russian configuration for extended calorific A01
value analysis used (see manual for more information).
Extended measuring range in combination The operator input is by means of another separate interface via
with position 8_0 and position 8_1 Ethernet (TCP/IP).
N2, C02, C1-C5, C6, C7 (+) B02 Other serial and analog (4 to 20 mA) interfaces are optionally
N2, C02, C1-C5, C6, C7, C8, C9 (+) possible using an external solution package (see Article No.
Acceptance and customer information 7KQ2160).
(in agreement with application laboratory)
Documentation
Factory acceptance, 1 day D01
The documentation includes a SITRANS CV Manual and
Factory acceptance (performance record), 1 day D02 CVControl Operating Manual in English and German. The
Factory acceptance, every additional day D03 documents can be found on the enclosed CD.
Proof of repeatability Safety manuals in all EU languages are also available on the CD.
Repeatability up to 8 h E01 CVControl operating software
Repeatability up to 24 h E02
The operating software (language: English or Russian) is
Repeatability up to 48 h E03 included in the scope of supply. Windows XP or Windows 7 must
be installed on the computer in order to install this software.
Selection and ordering data Article No.
Analog data transmission and serial interface 7KQ2160- 7 7 7 Application
External module for generation of analog and serial A general system check is made of the basic unit and the
interfaces
integrated application module. The module and basic unit are
Click on the Article No. for the online configuration in described in the manual. In addition to the standard configu-
the PIA Life Cycle Portal. ration, additional country-specific and user-specific sub-config-
Analog values via external unit (standard package) urations are available. The performance record ex works
contains the analysis check, including a repeatability record (4h
2 analog values 0
test).
4 analog values 1
The chromatograph is preconfigured; In addition, three
8 analog values 2 CD-ROMS are enclosed:
1)
16 analog values 3 • SITRANS CV Software (including manuals and CVControl
20 analog values1) 4 Operating Instructions)
MODBUS multiplexer • Country-specific sub-setups
Without multiplexer A • Parameter backup
Without CE certificate B
With CE certificate C
Enclosure
Without protective casing A
With protective casing B
1)
On request
Article No. Pos. 8_0: Applications – Article No. Position 8_3: Applications – Calorific value analysis
Standard calorific value analysis with backflush summation
This application comprises the standard calorific value analysis. This position includes the analysis of the components listed in
The chromatograph's measurement method is set at the factory, Table 4, in which case the components starting from C6, includ-
using a synthetic natural gas mixture. The performance para- ing the isomers, are regarded as the sum peak. This variant is
meters specified in Table 5 and the criteria explained in the especially well suited for natural gases with very low content of
subsequent text apply to the individual components in Table 1 higher hydrocarbons, especially C6+.
and their physical variables.
However, this backflush summation can also be used to effec-
The calculation of the calorimetric variables is possible tively analyze natural gas with typical C6+ fractions. The compo-
according to the following standards: ISO 6976-95, GOST, nents up to and including C6+ can be analyzed within the
AGA 8, where the former is preset. The reference states for the possible concentration ranges according to Table 4.
combustion and for the gas volume that must be specified for
calculation purposes are preset to the standard state (Tb=25 °C, A01 – SITRANS CV for calorific value analysis Pos. 8_0, 8_1, 8_2
Tn = 0 °C) and can be easily changed to other reference states und 8_3 – Russian configuration
during commissioning using the operating software (Tb= This position includes the possibility for ordering SITRANS CV
operating temperature, Tn= standard temperature). with a Russian Ex certificate.
The CVControl software provides the energy units BTU/ft3, IMPORTANT: This Russian version results in a change in the
3 KWh/m3 and MJ/m3. nomenclature from SITRANS CV to MicroSAM.
Article No. Pos. 8_1: Applications – extended calorific value The following also applies to Pos. 8_3:
analysis with oxygen The limits listed in GOST Standard 31371.7-2008 are checked
This position includes the extended calorific value analysis of the during the inspection and supplied with the device documen-
components and possible working ranges from Table 1. Oxygen tation.
is measured in addition to the listed components (see Table 2). B02- SITRANS CV with extended measuring range in combi-
A carrier gas dry filter (Article No. filter set A5E00400116) on the nation with Pos. 8_0
mounting bracket of the SITRANS CV or enclosed separately is This position permits separate measurement of the group
used as standard for this measurement. isomers of the higher hydrocarbons C6 to C7(+) and C6 to C9
The remarks concerning oxygen and CO in footnote 1 of Table 1 (+). In accordance with the designation C7(+) and C9 (+), a
are no longer applicable to this position. The information detailed measurement is carried out up to and including n-C9.
concerning calculation and performance parameters are Important:
identical to Pos. 8_0.
Testing and certification of the SITRANS CV is carried out using
Important: the standard calorific value analysis in accordance with
For correct operation of SITRANS CV in accordance with Pos. Pos. 8_0. If Pos. D02 or D03 has been selected, this does not
8_0 and 8_1, all measured components must be present in the include repetition of the proof of repeatability (4 h test) of the unit
calibration gas. The calibration gases listed in the table "Recom- during the factory acceptance.
mended calibration gases for Pos. 8_0 and 8_1" are recom- The following calibration gases are essential for operation of the
mended (also see Table 6): SITRANS CV including these extended measuring ranges:
Component Pos. 8_0 (mol%) Pos. 8_1 (mol%) Required Calibration gas for C6 Calibration gas
components and C7(+) measurement for C6 and C9(+)
Oxygen 0.5
(mol%) measurement
Nitrogen 4 4 (mol%)
Carbon dioxide 1.5 1.5 Nitrogen 4.00 4.00
Methane 88.9 88.4 Carbon dioxide 1.50 1.50
Ethane 4 4 Methane 89,00 89,00
Propane 1 1 Ethane 4.00 4.00
Isobutane 0.2 0.2 Propane 1.00 1.00
n-butane 0.2 0.2 Isobutane 0.20 0.20
Neopentane 0.05 0.05 n-butane 0.20 0.20
Isopentane 0.05 0.05 Neopentane 0.10 0.10
n-pentane 0.05 0.05 Isopentane 0.05 0.05
n-hexane 0.05 0.05 n-pentane 0.05 0.05
Table 7: Recommended calibration gases for Pos. 8_0 and 8_1 n-hexane 0.05 0.05
n-heptane 0.05 0.05
A summary of the various country-specific setups, i.e. standard
settings including measured components and calibration gases, n-octane 0.05
can be found on the parameter backup CD in the "Readme.pdf" n-nonane 0.05
document.
Table 8: Components and concentrations of the calibration gases for the
Article No. Pos. 8_2: Applications – Calorific analysis with extended measuring ranges
biomethane
Further information regarding startup of SITRANS CV including
This position contains the analysis of the components and C7(+) and C9(+) measurement can be found in the manual and
working ranges of the biomethane listed in Table 3. Based on the on the enclosed document CD (country-specific setup
measured concentrations of the components, the quality param- "Readme.pdf" file)
eters – such as heating values – are determined in accordance
with the international standards ISO, GOST and AGA analo-
gously to positions 8_0 and 8_1.
D01 - Acceptance and customer information - Factory Component Gas #1 (Mol.%) Gas #2 (Mol.%) Gas #3 (Mol.%)
acceptance, visual check, 1 day
Methane Residual Residual Residual
The scope of supply is checked and the documentation and (approx. 75) (approx. 85) (approx. 96.5)
operation of the unit explained as part of the factory acceptance Nitrogen 15.5 5 2.5
process. The factory acceptance does not include repetition of
Carbon dioxide 0.5 2 0.1
the proof of repeatability (4 h test) of the unit.
Oxygen 0.5 2 4
D02 - Acceptance and customer information - Factory
acceptance with performance record, 1 day Ethane 8 4 0.5
Propane 0.5 2 0.15
The scope of the tests to be carried out is described in Table 9
"Scope of tests during factory acceptance". When ordering D02, i-butane 0.15 0.5 0.03
please supplement the desired option from E0x. n-butane 0.15 0.5 0.03
Record of component isolation Through a final check of existing Neopentane 0.08 0.3 0.03
documentation and according to i-pentane 0.08 0.3 0.03
current chromatograms, 5 analyses
n-pentane 0.08 0.3 0.03
Stability test (repeatability) According to order E01 ... E03
Performance criteria according to Hexane 0.05 0.1 0.015
3
page 3/28 ff.
Table 10: Recommended calibration gases for linearity test during
Checking the Modbus connection Checking or simulation of Modbus acceptance
communication can be carried out
using a flow computer provided by The calibration gases have the following uncertainties:
the customer, for example.
Calculation test Comparison of the values calculated Proportions of Uncertainty (or smaller)
by CVControl with a customer com- component materials (Mol.%)
parison procedure (optional) 0.1 ... 0.25 ± 5.00 %
Auto-calibration function The two functions are explained the- 0.25 ... 1 ± 1.00 %
Auto-optimization of method oretically and practically during pre-
sentation of CVControl. 1 ... 10 ± 0.50 %
Alarm and event messages Simulation of alarm situations; 10 ... 100 ± 0.20 %
as per customer requirement
Table 11: Uncertainties of calibration gases
Table 8: Scope of test during factory acceptance
Notes on 7KQ2160-..
SITRANS CV is a standard product. Only in this manner is it
possible to guarantee short delivery times and attractive prices. Analog and serial data transmission
All performance records required retrospectively require higher SITRANS CV does not provide internal analog outputs. These
overhead. However, will will be happy to come to an agreement properties can be provided by the SIMATIC Extension Unit.
regarding implementation. This uses the Modbus output of the chromatograph in order to
D03 - Acceptance and customer information - Factory generate up to 8 active analog outputs (standard, more analog
acceptance, each additional day outputs on request).
Only in conjunction with D01 or D02 Modbus multiplexers are available in addition, and allow up to
2 Modbus masters to be connected to the SITRANS CV. The
E0x - Repeatability test distance from the SITRANS CV should not be more than
Proof of repeatability over a period of 4 h is included as 1 200 m. In the case of an installation without enclosure (without
standard. Longer repeatability records for the unit can be explosion protection), we deliver the components for generation
ordered by means of the supplementary item E0x. of analog outputs mounted on a rail, otherwise in the Ex d
enclosure.
E01 to E03 - Repeatability test, 8 h – 24 h – 48 h
Pos. 08_ 0 - 5 – Analog values via external unit
Only in conjunction with D02
This position includes:
Linearity tests can be carried out in the factory on request. The • Mounting rail
standard calibration gases required for this (Table 10: "Recom-
mended calibration gases for linearity test during acceptance") • Power supply
are provided free of charge. If the customer specifies other • SIMATIC S 7-300 and SIMATIC S7, Micro Memory Card 3.3 V
calibration gases with different compositions or higher uncer- NFLASH, 64 KB
tainty requirements, they must provide these gases for accep- • Analog output module with terminating connector
tance purposes. As an option, Siemens can procure these
special calibration gases (subject to a charge). • Protocol converter
On request, proof of the complete functionality of the Pos. 09_ A – C: Modbus multiplexer
SITRANS CV is possible within the certified temperature and (only applicable together with 0-4)
ambient conditions.
The Modbus signal can be routed using the Modbus multiplexer
and connected to two Modbus masters. B specifies supply of
the components without CE certificate.
Pos. 10_ A - B: Enclosure
This position includes the option for installation of the SIMATIC
extension unit in the hazardous area (Zone 1 and Zone 2). A
protective casing Ex d with standard cable glands including the
modules required for the analog outputs and the Modbus multi-
plexer (if applicable) are provided for this purpose.
■ Dimensional drawings
156 200 70
12
300
3
20
40 34
85 306 20
L = 4 000 mm
1 5
40
220
40
4 8
D 10 (4x)
4/2 Introduction
Analysis of biogas
4/49 Set BGA
Siemens PA 01 · 2015
© Siemens AG 2014
■ Overview
Standardization and the supply of complete packages are two
trends that are currently on the up. This can be attributed to the
fact that the same application is frequently required in different
industrial sectors and overhead can be minimized in this case.
Furthermore, customers often want to purchase turnkey systems
to minimize the risk of any technical problems.
With its Analytical Application Set initiative, Siemens is making
use of its wealth of experience to offer standardized packages
that are designed with a single application in mind. Its range of
applications can cover a variety of industrial sectors.
It is now possible to simply configure and order complete appli-
cations straight from the catalog, thereby sharply reducing the
amount of time taken between the request and order. All Analyt-
ical Application Sets are tested in advance and provide a high
level of safety and reliability. The different versions cover a broad
spectrum of potential applications and ensure that the sets can
be configured for both minimum and maximum requirements.
The order structure makes it possible to choose from different
versions and module components, as well as configure the sys-
tem and order it directly.
■ Overview
The combustion of different fuels causes not only the develop- Siemens expertise in the area of products and solutions for
ment of carbon dioxide and water vapor but also other environ- process analysis helps you meet all requirements for continuous
mentally harmful exhaust gas substances (e.g. dust, nitrogen emission monitoring quickly and smoothly in accordance with
oxides and carbon monoxide, etc.) Emission limit values are de- regional law. This solution package even ensures a secure
termined for these substances according to the state of combus- investment in case of regulatory adjustments.
tion engineering. The compliance with these limits does not only
protect the environment from air pollutants but also ensures op- According to individual requirements, Siemens offers cold-ex-
timum combustion in the combustion plants. Emission measure- tractive, hot-extractive, and in-situ automated monitoring sys-
ments are a central element for complying with these limit val- tems.
ues. The portfolio is completed by emission evaluation systems for
These measurements are required to document whether legal data storage, visualization, remote transmission - permitted ac-
requirements relating to emission limits are complied with. Emis- cording to TA-Luft, 13., 17., 27., 30. and 31. BImSchV
sion measurements still serve as warranty from plant construc- Siemens does not only offer standard solutions but also com-
tors to operators that the plant runs in accordance with the spec- plete emission analysis systems, e.g. in turnkey analysis con-
ification and the law. tainers.
There are two reasons why the measuring and monitoring of flue
gases for emission components is one of the key topics in con-
tinuous gas analysis. First, because of the necessity to comply
with the legal regulations and directives. Second, because pro-
cess plant operators draw conclusions regarding process effi-
ciency from the gas analysis, for example, in boiler control.
So called Continuous Emission Monitoring Systems (CEMS) are
used for the determination of the exhaust gas components. In
Europe, they are usually called Automated Measurements Sys-
tems (AMS). DIN EN 15267 determines corresponding minimum
requirements and testing procedures for automated monitoring 4
systems for the measurement of gases and particulate sub-
stances in the exhaust gas of stationary sources as well as for
the measurement of the volume flow of the exhaust gas. It pro-
vides detailed procedures for the realization of the requirements
for the first quality assurance level (QAL1) of DIN EN 14181 and,
if required, the access data for the third quality assurance level
(QAL3).
■ Overview ■ Design
Tested component design
The complete system consists of the following tested individual
components:
• Sampling probe: M&C, type: SP2000; Bühler/Siemens,
type: GAS222/7MB1943-2F
• Heated sample gas line: Winkler/Siemens, type: 7MB1943-2A
• Temperature controller: Siemens, type: SIRIUS
• Two-stage compressor gas cooler: M&C, type: CSS;
Bühler, type: EGK 2-19
• Sample gas pump: Bühler/Siemens, type: P2.3/7MB1943-3C
• NOX converter: M&C, type: CG-2; Bühler/Siemens,
type: BUENOX/7MB1943-2D
Performance-tested measuring ranges
Component Analyzer Smallest certi- Additional
module fied measur- measuring ranges
ing range
Set CEM CERT is a standardized and certified continuous emis-
sion monitoring system which is suitable for use in many plants CO (in test phase) U23-7MB2355 0 ... 150 mg/m³ 0 ... 750/
3 000 mg/m³
requiring European legislation (13. BImSchV, 27. BImSchV, TA
Luft, 2001/80/EC and IED 2010/75/EC, Annex V) approval. The (in test phase) U23-7MB2357 0 ... 150 mg/m³ 0 ... 750/
innovative CEMS meets the current quality standards of EU di- 3 000 mg/m³
rectives EN 14956, EN 15267 and EN 14181 (QAL1/2/3, AST). U23-7MB2358 0 ... 250 mg/m³ 0 ... 1 250 mg/m³
4 ■ Benefits
NO (in test phase) U23-7MB2355 0 ... 100 mg/m³ 0 ... 750/
2 000 mg/m³
• The tested measuring ranges can be selected for a variety of (in test phase) U23-7MB2357 0 ... 100 mg/m³ 0 ... 750/
2 000 mg/m³
ranges to ensure use in different areas of application for the
CEMS (TÜV approved). U23-7MB2358 0 ... 400 mg/m³ 0 ... 2 000 mg/m³
• The complete modular package allows the certified use of (in test phase) UV600 0 ... 50 mg/m³ 0 ... 100/
system components from different manufacturers (TÜV 1 000/2 000 mg/m³
approved). SO2 (in test phase) U23-7MB2355 0 ... 400 mg/m³ 0 ... 2 000 mg/m³
• Simple and fast to configure (in test phase) U23-7MB2357 0 ... 400 mg/m³ 0 ... 2 000 mg/m³
• Very low costs of procurement and operation U23-7MB2358 0 ... 400 mg/m³ 0 ... 2 000/7 000 (in
operation) mg/m³
Modular design
(in test phase) UV600 0 ... 75 mg/m³ 0 ... 130/1 500/
• Up to 2 analyzers with different measuring ranges can be 2 000 mg/m³
configured
NO2 (in test phase) UV600 0 ... 50 mg/m³ 0 ... 500 mg/m³
• Selection of versions for indoor or outdoor installation
O2, (paramag.) U23 0 ... 25 vol %
• Selection of sample gas cooler and NOX converter from
O2, (electrochem.) U23 0 ... 25 vol %
leading manufacturers
• Electric heaters and air conditioners can be configured to
extend the ambient temperature range ■ Function
• Selection of versions with appropriate sampling probes,
heated sample gas lines The complete tested modular measuring equipment is com-
posed of the sampling probe, the heated sample gas line, a two-
stage sample gas cooler, a gas pump and the multi-component
■ Application analyzers, ULTRAMAT 23 and SIPROCESS UV600.
• Emission monitoring of power plants fueled with solid, An electrochemical or a paramagnetic oxygen measuring cell
gaseous or liquid fuels can be used for the measurement of oxygen.
• Emission monitoring of so-called TA Luft plants (e.g. emission The gas path splits in parallel after the sample gas cooler. This
monitoring of glass melting furnaces or steel plants) separately supplies each analyzer with sample gas. One advan-
• Emission monitoring in crematorium facilities (27. BImSchV) tage for maintenance is that each analyzer can be individually
serviced without affecting the other. The sample gas coolers
used have a moisture alarm in case of malfunction. For addi-
tional protection, each analyzer is protected by a condensation
barrier, which stops the gas flow if moisture penetrates. This
guarantees optimum protection for gas analyzers.
For semi-automatic calibration of the zero and calibration gases,
a 3/2-way solenoid valve is installed between the first and sec-
ond cooling stages. The valve can also be used for AUTOCAL
calibration of the ULTRAMAT 23 (fully automatic timing) as well
as by the integrated PLC (LOGO module).
■ Technical specifications
Climatic conditions Power supply
Ambient temperature +5° ... +40 °C (standard) Supply 1 115 V AC, 50 … 60 Hz (-15 %, +10 %)
• With heater in sheet-steel Min. -5 °C Supply 2 230 V AC, 50 … 60 Hz (-15 %, +10 %)
cabinet
• With heating in GRP cabinet Min. -15 °C Supply 3 400 V AC, 50 … 60 Hz (-15 %, +10 %)
• With air-conditioning Max. +52 °C Power 4 000 VA max.
Relative humidity 75 % (annual average), non-condensing System design
Sample gas conditions Fusing of electronic consum- 1-pole or 2-pole (selectable)
Max. sample gas pressure at 500 hPa (mbar) ers
inlet to sample preparation Sample gas cooler 2-stage
system
Output signals 4 … 20 mA (corresponding to the analyzer
Max. moisture content in sam- 17 vol % (cooler type: CSS) information)
ple gas 25 vol % (cooler type: EGK 2-19)
Additional digital inputs and outputs via PLC
Sample gas temperature Max. 200 °C at cabinet entry (LOGO)
Sample gas flow Approx. 60 l/h per analyzer module Color RAL 7035
Sampling probe (standard) Dust load: < 2 g/m3 Weight Approx. 160 kg
Mounting flange: DN 65, PN 6, form B Sheet-steel cabinet/frame Indoor installation
Including temperature controller with Pt100 GRP cabinet Outdoor installation
With internal sampling tube, stainless steel, Explosion protection classifica- Installation outside the Ex zone
length: 1 m (can be shortened) tion
With filter in probe, to 600 °C Degree of protection IP 54 (avoid direct sunlight for outdoor instal-
Sampling probe for higher On request lation)
temperatures and in other
materials (optional)
Calibration Semi-automatic; AUTOCAL freely adjust-
able on U23 up to max. 24-hour interval 4
Sample gas line, electrically Max. 35 m, longer lengths on request Detailed information on the analyzers
heated
You can find detailed information on the analyzers:
Sample gas must not be flammable or explosive. • in the "Continuous Gas Analyzers, extractive" chapter
- ULTRAMAT 23
- SIPROCESS UV600
Dimensions
Sheet-steel cabinet (with base) 2 000 x 800 x 800 mm (H x W x D)
for indoor installation
GRP cabinet (with base) for 2 060 x 900 x 800 mm (H x W x D)
indoor installation
500 mm spacing on the right or left must be provided for the cable inlet and
connection of the heated sample gas line.
4 Fuse protection
1-pole 0
2-pole 1
Sample gas cooler
Compressor gas cooler, type: CSS; Manufacturer: M&C 1
Compressor gas cooler, type: EGK 2-19, Manufacturer: Bühler 2
NO2/NO converter
Without NO2/NO converter A
NO2/NO converter, type: CG series; Manufacturer: M&C C
Power supply
115 V AC, -15 %, +10 %, 50 Hz A
230 V AC, -15 %, +10 %, 50 Hz B
400 V AC, -15 %, +10 %, 50 Hz (3-phase) C
Additional versions Order code
Add "-Z" to article number and then order code
Accessories
Preparation for data acquisition system, D-EMS (DURAG) A01
Preparation for dust measurement A02
Condensate tank with level monitoring A03
Acidification module (for measuring low concentrations of SO2) A04
Extractive analyzers, the analyzers must be ordered separately
Preparation for the installation of an ULTRAMAT23 C01
Preparation for the installation of two ULTRAMAT 23 C02
Preparation for the installation of a SIPROCESS UV600 C03
Preparation for the installation of two SIPROCESS UV600 C04
Preparation for the installation of an ULTRAMAT 23 and a SIPROCESS UV600 C05
Sample gas line, electrically heated (with temperature controller and circuit breaker)
Length: 5 m D01
Length: 10 m D02
Length: 15 m D03
Length: 20 m D04
Length: 25 m D05
Length: 30 m D06
Length: 35 m D07
■ Dimensional drawings
Converter (option)
800
Option
130
200
Sample
4
gas outlet
Cable glands
VF1 ULTRAMAT 23 electrical input/output
VF2
Air conditioner
(option) SIPROCESS UV600
395
Calibration gas
2000
Sample gas
cooler
300
Heater
mounted on Condensate vent
the side Hinged frame 40HE
(option) right stop
100
■ Overview ■ Application
The monitoring of emission components in flue gases is one of
the most important topics for continuous gas analysis. This is a
result of legislation for monitoring emissions, e.g. for large com-
bustion plants, and also due to the requirements of companies
operating process plants who can draw conclusions on the pro-
cess efficiency from the gas analyses, e.g. with boiler control,
DENOX and DESOX plants.
The market requires a reliable complete system which is spe-
cially designed for the application. The Set CEM 1 (Continuous
Emission Monitoring) offered by Siemens is a system which reli-
ably covers all requirements associated with sampling, sample
preparation, and gas analysis.
It is possible to determine the concentrations of the gaseous
components CO, CO2, NO, NOx, SO2, O2, Ctotal, HCl, HF, NH3
and H2O.
The ULTRAMAT 23 and OXYMAT 6 are used for the extractive,
continuous gas analysis.
The Set CEM 1 is a standardized system specially for monitoring The standardized Set CEM 1 provides great clarity and simple
the emission components in flue gases. configuration facilities. Different versions mean that it is possible
to appropriately adapt the system to the requirements. Stan-
dardization also means that not all imaginable versions can be
■ Benefits included, and that it may not be possible to implement special
Standardized complete system requirements such as armored cables, varying gas composi-
tions, customer-specific documentation or specific conductor la-
4 • Highly exact and reliable monitoring of emission components
in flue gases. System-specific certificate according to
beling without an extra charge.
DIN EN ISO 14956 and QAL 1, according to EN 14181.
• Modular complete package with gas sampling system,
■ Design
sample gas preparation system and gas analyzers from one Starting with a mounting frame with sample preparation system,
source it is possible to add additional units as options. These include:
• Simple and fast to configure • Sampling probe with weather protection hood
• Tried and tested, harmonized and reliable set • Heated sample gas line (for details see catalog PA11)
• Low purchase price and economic operation • Analyzers
Proven, suitability-tested technologies • Air-conditioning unit
• Continuous determination of up to eight measured compo- • NO2/NO converter
nents • Sample preparation extension for an additional ULTRAMAT 23
• In-situ measurements without sampling and preparation, analyzer
using LDS 6 laser diode spectrometer • Single and dual (electrically isolated, not electrically isolated)
• Use of ULTRAMAT 23 with cleanable cells and automatic analog signal processing
calibration with ambient air as well as optional electrochemical • Power supply modules (115 V, 230 V, 400 V)
oxygen measurement • Outer panels with steel-plate door or with window
Optional: • Single-pole and double-pole fusing
• Paramagnetic oxygen measurement with OXYMAT 6 • Condensation bottle
Simple operation • Coalescence filter
• Intuitive operation Sampling probe
• Configuration on large displays using plain text, in several The standard probe is fitted with a DIN flange DN 65, PN 6. The
languages probe is provided with a regulated heater, and has a power con-
Simple maintenance sumption of 400 VA. It is supplied with a weather protection hood
and 2 µm filter. The maximum dust concentration at the sampling
• Maintenance-friendly cabinet design with hinged frame and point should not exceed 2 g/m³. The sampling pipe is 1 000 mm
uniform design long, is made of stainless steel, and has dimensions of 20 x
• Digital display of maintenance requests on LOGO modules 1.5 mm. The sample gas temperature must not exceed 600 °C.
It is also possible to purchase the Set CEM 1 without sample
probe.
The basis of each CEM 1 set is the mounting frame with hinged The double-pole fuse is mainly required in Benelux countries.
frame (40 HU) for installation of up to five 19" rack units. The Removal of condensation
mounting frame includes a standardized sample preparation
system designed for an ULTRAMAT 23. A 19 liter condensation bottle can be provided as an option. It is
also possible to order the system without a condensation bottle
The sample preparation system includes a 3/2-way solenoid if the condensation can be removed on-site.
valve, 3-way switchover ball valve, regulating valve, corrosion-
resistant sample gas pump (power consumption 60 VA), con- NO2/NO converter
densation trap, room air suction filter with filter element, LOGO The mounting frame and cabinets can be optionally extended by
for digital display of individual signals in the cabinet, 24 V DC a 19" rack unit with NO2/NO converter with carbon cartridge. The
power supply unit (power consumption 70 VA). Also included power consumption is 520 VA. The flow rate is 90 l/h. An NO2/
are a sample gas cooler (power consumption 200 VA) with inte- NO converter is required if the share of NO2 in the total NOx is
gral heat exchanger, hose pump, moisture sensor with flow cell greater than 5% and/or if total NOx is to be always determined.
and Teflon filter. Teflon tubes connect the components.
The external dimensions without plinth are 2 000 x 800 x 800 mm Power supply
(H x W x D). A cabinet depth of 600 mm is also optionally avail- The system can be designed either for 115 V AC, 230 V AC or
able (not suitable for LDS 6). Hoses and cables can be con- 400 V AC (-15 %, +10 %) with 50 or 60 Hz.
nected from the left or right. A distance of 500 mm must be pro-
Three phases, neutral and ground must be provided by the cus-
vided on the left or right at the installation site for introduction of
the hoses and cables. tomer at 400 V AC. 4
In addition to the sheet-steel mounting frames for indoor installa- Analog signal processing
tion, an FRP version is also available for outdoor use. The FRP As standard, the analog signals are simply connected to isolat-
cabinet is always provided complete with side panels and plinth. ing terminals. As an option, the analog signals can be pro-
The external dimensions are 2 080 x 800 x 600 mm (H x W x D). cessed twice without electrical isolation by a diode module, or
The GRP cabinet cannot be combined with the LDS 6. twice with electrical isolation.
Preparation of sample preparation system for second Analyzers
ULTRAMAT 23
The standardized set is prepared for an ULTRAMAT 23. The sys-
The standard system with sample preparation system and elec- tem can be supplemented by a second ULTRAMAT 23,
tronics is prepared for one ULTRAMAT 23. If a second OXYMAT 6 and/or LDS 6. Various measured components and
ULTRAMAT 23 is to be fitted, this option must be selected so that measuring ranges can be selected. Other combinations of mea-
the sample preparation system and electronics are extended ac- sured components and measuring ranges are available on re-
cordingly. quest, but you must check that the desired certificates and ap-
Additional filter provals are available. The analyzers, measured components
and measuring ranges used are described briefly below.
In addition to the fine filter and moisture filter which are always
present, a coalescence filter can be optionally fitted in the sam- Details on the analyzers, alternative components and ranges
ple preparation system. can be found under the topics "Continuous gas analyzers, ex-
tractive" and "Continuous gas analyzers, in-situ".
Side panels with doors
ULTRAMAT 23: CO, NO
Optional outer panels can be selected for the sheet-steel mount-
ing frames. This possibility allows use of the CEM 1 set in analy- For measuring two infrared components.
sis cabinets as a rack design on one hand, or on the other as a
Component Smallest tested measuring Switchable to
cabinet design in halls requiring degree of protection IP54. Ei- range
ther a sheet-steel door without window or a glass door can be
selected. CO 0 ... 150 mg/Nm³ 0 ... 750 mg/Nm³
NO 0 ... 100 mg/Nm³ 0 ... 500 mg/Nm³
Base
Plinths with a height of 100 and 200 mm are additionally avail- One or two measuring ranges can be freely set within the limits.
able. The ULTRAMAT 23 carries out automatic self-calibration with
ambient air. The power consumption is 60 VA.
Cabinet cooling and ventilation
Optionally available are a fan with outlet filter, an air-conditioning
unit for indoor installation, and an air-conditioning unit for out-
door installation. The system can be ordered without a fan or air-
conditioning unit if the side panels and the door with window are
omitted.
The fan with outlet filter has a power consumption of 60 VA, and
is fitted in the cabinet wall. The delivery also includes a thermo-
stat with a power consumption of 25 VA.
The air-conditioning unit has a cooling power of 820 VA.
Measuring equipment
LOGO TD
L = max. 35 m
CLF
Option NO CO/NO
Sample gas
Option Water trap
outlet
Converter U23
Option Option
U23
2nd ULTRAMAT 23 (option)
O2
LDS 6
HCL,
H2 O O6E
LDS 6
4
LDS 6 (option)
19 liters
Cabinet heating
Option (option)
■ Function Connections
Hose material Teflon
A sample is extracted via the heated sample gas probe. The
dust concentration may be up to 2 g/m³, the sample gas temper- Cables Not armored, not halogen-free
ature up to 600 °C. The gas is transported to the analysis cabinet Electrical design According to IEC
via a heated sample gas line. The heating prevents condensate. Cable ID Individual core labeling as option
The gas cooler cools and dries the sample in the analysis cabi-
net. Condensate is drained. The level in the condensate trap is Fusing of electronic consumers 1-pole; 2-pole as option
monitored. For safety purposes, a coalescence filter can be pro- Duplication of analog signals • Not electrically isolated as option
vided in addition to the fine filter and moisture filter which are al- • Electrically isolated as option
ways present. The sample gas is analyzed by analyzers such as Installation
the ULTRAMAT 23, OXYMAT 6 and LDS 6. The ULTRAMAT 23
Site
operates on the basis of molecular-specific absorption of infra-
• In sheet-steel cabinet/frame Indoor installation
red radiation or with an electrochemical oxygen measuring cell.
• In GRP cabinet Outdoor installation
The OXYMAT 6 is an analyzer for paramagnetic oxygen mea-
surements. The in-situ LDS 6 laser diode spectrometer operates Ex zone Non-Ex area
according to the molecular-specific absorption of near-IR radia- System design
tion. The delivery may also include an NO2/NO converter which
permits measurement of total nitrogen oxides. In order to qualify Type Mounting frame or cabinet
the set for low or high temperature ranges (-5, +45 °C), it is pos- Cabinet degree of protection IP54
sible to use a cabinet heater or air-conditioning unit. Power sup- Automatic calibration Yes, with ULTRAMAT 23
ply versions are available for 115, 230 or 400 V AC. Electronic
consumers can be provided with single-pole or double-pole fus- Detailed information on the analyzers
ing. The components of the sample preparation system and the You can find detailed information on the analyzers:
analyzers are connected to LOGO modules via a binary signal, • In the "Continuous Gas Analyzers, extractive" chapter
- ULTRAMAT 23
and transmit maintenance requirements. The analog signals can - OXYMAT 6
be processed either singly or twice. Electrical isolation is addi- • In the "Continuous Gas Analyzers, in-situ" Chapter
tionally possible for the double processing. - LDS 6
■ Technical specifications
Dimensions (without plinth) 4
Depth of sheet-steel frame
• 800 mm (without plinth) 2 000 x 800 x 800 mm (H x W x D)
Climatic conditions
• 600 mm (without plinth) 2 000 x 800 x 600 mm (H x W x D)
Ambient temperature 0 ... 35 °C
GRP cabinet (with plinth) 2 080 x 900 x 600 mm (H x W x D)
• With heater in sheet-steel cabinet Min. -5 °C
• With heating in GRP cabinet Min. -15 °C It is necessary to provide a 500 mm gap to the right or left for the
• With air-conditioning Max. 52 °C tube or cable inlet.
Relative humidity 70 %, non-condensing Use of the LDS 6 requires a cabinet with a depth of 800 mm.
1)
Corrosive atmosphere No Higher performance sample gas coolers can be offered upon request (not
TÜV suitability-tested). A higher performance cooler is generally required
Gas inlet conditions for high sulfide content in fuels (e.g. heavy oil).
Max. sample gas pressure at inlet to 500 hPa (mbar)
sample preparation system
Max. moisture content in sample gas 17 vol-% 1)
Max. water dew point 60 ?
Min. sample gas pressure at inlet to 180 °C
sample preparation system
Dust content at inlet to sample prepa- Dust-free
ration system
Sampling probe Sampling tube 20 x 1.5,
1 000 mm long, stainless steel,
flange: DN 65, PN 6
Max. sample gas pressure at sam- 500 hPa (mbar)
pling probe
Max. sample gas temperature at sam- 600 °C
pling probe
Max. dust content at sampling probe 2 g/Nm³
Sample gas must not be flammable or explosive.
Power supply
Supply 1 115 V AC (-15 %, +10 %)
Supply 2 230 V AC (-15 %, +10 %)
Supply 3 400 V AC (-15 %, +10 %)
4 19" rack units possible, not suitable for LDS 6 F01 ... F06,
G01 ... G04
Sampling probe
Without A
Standard sampling probe B
Ventilation/cooling
Without A
Fan with outlet filter B
Cabinet air-conditioning unit C
Cabinet air-conditioning unit for GRP rack D
Heating
Without 0
Cabinet heating 1
Fuse protection
1-pole 0
2-pole 1
Removal of condensation
Without 0
19 l container with level monitoring 1
NO2/NO converter
Without A
NO2/NO converter B
Power supply
115 V AC, -15 %, +10 %, 50 or 60 Hz A
230 V AC, -15 %, +10 %, 50 or 60 Hz B
400 V AC, -15 %, +10 %, 50 or 60 Hz (3 phases, neutral, ground provided C
by customer)
Connection set for heated line
Without controller 0
Standard controller (max. 35 m heated line can be connected) 1
Note:
The heated sample gas line must be ordered separately using Catalog PA 11.
■ Dimensional drawings
Option:
Control cabinet ventilation (when using side walls) **
Standard: voltage 230 V/50 Hz, 1-pole fusing
Either fan and outlet filter
Option:
or air-conditioning unit Option:
voltage 115 V/50 Hz / 400 V/50 Hz, 2-pole fusing
Mounting on left or right Electronic and pneumatic
Spare location inputs and outputs
800 for converter either on left or right
(option)
4 Outlet filter
SIEMENS
LOGO Electrical
0.00
0.00
0.00
0.00
OXYMAT 6E (option)
Sample gas outlet
2000
Siemens
OXYMAT 6E
Spare
-RV3 Calibration
LDS 6E (option)
Siemens gas inlet
Option: LDS 6E
Sample gas inlet
Coalescence filter
Fan
Condensation outlet
350
Hinged frame 40 HU
100
Option:
Side view from right Front view condensation bottle Side view from left
Hinged frame open with level monitoring
19 liters
Standard: without plinth Sample gas cooler Option: Available cabinet sizes:
Option: Cabinet heater Metal: W x H x D: 800 x 2 000 x 600
with plinth 100 or 200 mm high Metal: W x H x D: 800 x 2 000 x 800
FRP: W x H x D: 900 x 2 140 x 600
** FRP cabinet is always with side walls and 80 mm plinth
■ Overview ■ Application
The measurement and monitoring of emission components in
flue gases is one of the most important topics for continuous gas
analysis. This is a result of legislation for monitoring emissions,
e.g. for waste incinerators, and also due to the requirements of
companies operating process plants who can draw conclusions
on process efficiency from the gas analyses, e.g. with boiler and
oven controls, DeNOx and DeSOx plants.
The market requires a reliable complete system which is spe-
cially designed for the application. The Gasmet CEMS (Continu-
ous Emission Monitoring System) offered by Siemens is an ex-
tractive and continuous gas probe measuring system based on
established FTIR spectroscopy method. It reliably covers all re-
quirements associated with sampling, sample processing, and
gas analysis.
The concentration of the following gas components can be de-
termined on the basis of FTIR: CO, CO2, HCl, HF, H2O, NH3, NO,
NO2, N2O, SO2, CH4, C2H4, C2H6, C3H8, C6H14and HCOH. The
Gasmet CEMS is another FTIR-based, standardized complete FTIR measurement can also be used to derive additional values
system for continuous, simultaneous measurement of a large for total organic carbon and NOx. In addition, the Gasmet CEMS
number of emission components in flue gases from power sta- offers space for an optional ZrO2 oxygen analyzer as well as a
tions and waste incinerators. FIDAMAT 6 for determining total organic carbon levels (also
QAL1 certified, if required).
■ Benefits The standardized Gasmet CEMS provides great clarity and sim-
ple configuration facilities. Different versions facilitate individual
Standardized complete system
• Highly accurate and reliable monitoring of emission compo-
nents in flue gases
adaptation to the system requirements in hand. Standardization,
however, also means that not all imaginable versions can be in- 4
cluded, and that it may not always be possible to implement par-
• Modular complete package with gas sampling system, hot ticular requirements such as armored cables, customer-specific
sample processing, measurement at 180 °C, data processing documentation or special conductor labeling without an extra
and analysis charge.
• Numerous analog and digital signal I/Os
• Simultaneous multicomponent analysis of 16 gas components
as standard:
CO, CO2, HCl, HF, H2O, NH3, NO, NO2, N2O, SO2, CH4, C2H4,
C2H6, C3H8, C6H14, HCOH
• Additionally calculated from the FTIR measurement: NOx and
total carbon values
• Approval for FTIR-based emission measurements (QAL 1 in
accordance with EN 14181) possible for ten measured
components
• Can be expanded with one or two additional analyzers for
measuring oxygen and for FID-based total carbon
measurement (also with QAL 1 approval, if required)
• Simple and fast to configure
• Tried and tested, harmonized and reliable set
• Low purchase price and economic operation
Proven, performance-tested technologies
• Continuous determination of up to eleven measured compo-
nents
• Simultaneous FTIR measurement for CO, CO2, HCl, H2O, NH3,
NO, NO2, N2O and SO2
• Optionally: Use of a QAL1 certified ZrO2 oxygen analyzer with
hot sample feed
• Optionally: FID-based total organic carbon measurement with
FIDAMAT 6
Simple operation
• Intuitive operation
• Configuration on a large TFT display using keyboard
Easy maintenance
• Maintenance-friendly cabinet design with 19'' telescopic rails
• Digital display of maintenance requirements
4
A suitable stainless steel (SS 316) probe with DN 65 PN 6 flange line including preassembly on the side of the connection to the
that can be heated to 180 °C is recommended as a sampling Gasmet CEMS sampling unit must be less than 43 mm.
probe for the Gasmet CEMS. This can be offered separately on
request. Gasmet CEMS sampling unit
Since particles of dust can usually be expected in sample gas, The sampling unit is designed for hot-extractive sampling of wet,
you are strongly recommended to use a sampling probe with a corrosive gas streams, and is integrated into the Gasmet CEMS
suitable (pre-)filter element and/or backflushing facility, espe- as a 19" rack unit.
cially with dust concentrations > 2 g/m3.
It encompasses all valves, flow meters, sample gas pumps and
The sample gas temperature should usually not exceed 600 °C; filters required for the measuring task. The temperature of all
the sample gas pressure must be between 400 and 6 000 hPa. parts coming into contact with the sample gas (pumps, filters
and lines) is stabilized to 180 ºC.
For performance-tested applications, a sampling probe
matched to the Gasmet CEMS must be used (e.g. M&C The sample gas does not have to be diluted and does not have
SP2000H or comparable). This can be offered separately on re- to be dried beforehand either. The gas flow and the pressure of
quest. the instrument air supply can be monitored via the Gasmet
CEMS sampling unit by means of an alarm.
The sampling unit is connected to the control PC and is con-
trolled using the Calcmet software, like the FTIR and the other
(optional) analyzers.
Instrument air
in
Zero gas in
Span gas in
Hose and cable inlets are possible from the top, below, left and
right.
At the installation location, sufficient space must be provided to
the front, the right and the rear of the analysis cabinet to allow Minimum space requirements for a Gasmet CEMS for facilitating instal-
opening of the front and rear doors, and facilitate access to the lation and maintenance work
rear door. The air-conditioning unit mounted on the rear also re-
quires sufficient space for air circulation.
To be able to pull out the 19'' rack units to the front on the tele-
scopic extensions, the electrical cables and sample gas lines in
the cabinet must be sufficiently long and flexible. The same ap-
plies to the lines to the CEMS analysis cabinet if it has to be
moved on optional rollers for service and maintenance pur-
poses, for example.
4
Component Smallest measuring Typical measuring Maximum measuring Unit
range range range
Water H2O 0 ... 25 0 ... 25 0 ... 40 Vol.%
Carbon dioxide CO2 0 ... 10 0 ... 20 0 ... 30 Vol.%
Carbon monoxide CO 0 ... 70 0 ... 500 0 ... 10 000 ppm
Nitrous oxide N2O 0 ... 50 0 ... 100 0 ... 500 ppm
Nitrogen monoxide NO 0 ... 100* 0 ... 200 0 ... 2 000 ppm
Nitrogen dioxide NO2 0 ... 100 0 ... 200 0 ... 500 ppm
Sulfur dioxide SO2 0 ... 30* 0 ... 100 0 ... 2 000 ppm
Ammonia NH3 0 ... 20* 0 ... 50 0 ... 500 ppm
Hydrogen chloride HCl 0 ... 10* 0 ... 50 0 ... 500 ppm
Hydrogen fluoride HF 0 ... 17* 0 ... 50 0 ... 100 ppm
Methane CH4 0 ... 50 0 ... 100 0 ... 1 000 ppm
Ethane C2H6 ** 0 ... 100 ppm
Ethylene (ethene) C2H4 ** 0 ... 100 ppm
n-propane C3H8 ** 0 ... 100 ppm
n-hexane C6H14 ** 0 ... 100 ppm
Formaldehyde HCOH ** 0 ... 50 ppm
Total carbon Ctotal, or THC, TOC 0 ... 15 0 ... 40 0 ... 40 mgC/m3
(via FTIR measurement)
Nitrogen oxide NOx Calculated from N2O, NO and NO2
(via FTIR measurement)
* Smallest measuring range only possible at maximum 30 vol.% water concentration
** Dependent on the application
Power
connector
Reference
air Sample in
4
0 to 10 V Sample out
4
=> No QAL1 certificate formally available for HF, but FTIR unit can be configured on request in such a way that the extended measuring uncertainties as
required by European Directive 2000/76/EU and 2001/80/EU are observed with regard to HF measurement. A manufacturer declaration in this regard and
calculation of the extended measuring uncertainties can be offered on request.
=> Possibly lower-cost solution compared to the use of 2 FTIR spectrometer units (see c)), if accepted by authority/test institute.
c) HF and one or more of the other above-listed IR-sensitive gas components are measured with two FTIR spectrometer units.
=> QAL1 certificate available
■ Function
Sample gas (max. 600 °C) is continuously taken via a heated FTIR spectroscopy is outstandingly suitable for multicomponent 4
sample gas probe, and transported via a heated sample line to analysis of numerous gas components. However, the oxygen
the sample pump of the heated sampling unit in the air-condi- concentration important for emission measurements, and the
tioned analysis cabinet. Heating to 180 °C prevents condensa- concentrations of other non-infrared-active gases such as inert
tion in the analysis system. From the sampling unit, the sample gases or hydrogen, cannot be determined in this way.
gas flows via further heated sample gas lines continuously
through the gas cuvette of the actual FTIR analyzer, as well as, For measuring O2, the system can be optionally equipped with
through the gas cuvette of the optional ZrO2 oxygen analyzer. a ZrO2 oxygen analyzer that can be integrated into the Gasmet
CEMS as a further 19" rack unit, and controlled using the Calc-
In the FTIR analyzer, spectra of the gas mix in the infrared spec- met software.
trum range are recorded at intervals of a few seconds. The gen-
erated interferograms are added together and converted to in- The FTIR method offers the possibility of calculating a "total or-
frared spectra using mathematical Fourier transform routines. ganic carbon value" from the individual concentrations of several
The result is the absorption spectrum of the sample gas, aver- hydrocarbons stored in the Gasmet CEMS standard calibration
aged over 60 seconds. The concentrations of the individual library. If direct total organic carbon measurement using the FID
components are calculated using multivariate-multicomponent method is required, a further free 19'' slot of the Gasmet CEMS
analysis. can be optionally equipped with a FIDAMAT 6.
A connected industrial PC, equipped with the special Calcmet The cabinet of the Gasmet CEMS analysis system is equipped
software, handles control of the measurements, analysis of the as standard with an air-conditioning unit mounted on the rear.
measured spectra, control of other programmable sequences, Power supply versions are available for 115 V AC or 400 V AC.
and output of the analog and status signals.
Delivery limit
Gasmet Computer
2- K-Bus
5° RS-232C Ethernet
Analog
Sample Probe
DN65 PN6-B
Sampling Unit
HEATED LINE 2
P1
Heated zone F1 FLA1
Ø6/4 mm OD/ID
A C A C A C A C A C A C A C A C A C A C A C A C A C A C A C A C A C A C A C
B D B D B D B D B D B D B D B D B D B D B D B D B D B D B D B D B D B D B D
1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2
Orifice
SPAN TO PROBE LINE Checkvalve1 Checkvalve2 A
3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4 3 4
7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8 7 8
KL9186 KL1408 KL2408 KL9187 KL9186 KL1408 KL9186 KL1408 KL2408 KL9187 KL2408 KL9187 KL3054 KL3054 KL4428 KL9187 KL4428 KL9187 KL9010
V1 V2 V3 V4 V5 Signals to
Control room
and Field devices
FIC2
FIC3
FIC4
FIC5
4 Sample in
Sample out
Delivery limit
2 4
K1
50 A
1 3
Delivery limit
Devices L
X1:13
F1 F2 F3 F4 F5 Potential PE
N
C10 C10 C16 C6 C6 X1:7 rail X1:1
T 1 3 5 N 1 1 1 1 1
Q1 1 3 5 N F0
63 A 63 A
2 4 6 N ∆n0.03 A
2 4 6 N 2 2 2 2 2
X2:
L1
SUPPLY
L2
TN-S
L3
230 V/400 V
N
min. 25 A
PE
max. 63 A
Delivery limit
■ Technical specifications
General data Sampling unit
Measuring principle • Fourier transform infrared (FTIR) Temperature controller for heated 0 … 180 °C
spectroscopy sample gas lines
• for oxygen: ZrO2 measuring cell
(optional) Type of temperature sensor in sample K type (Ni-Cr-Ni element)
• for total carbon (Ctotal, THC, TOC) gas lines
- FTIR, not performance-tested Gas inlet conditions
(standard) • Max. sample gas pressure at inlet to 1 500 hPa
- FID analyzer, also performance- sample preparation system
tested in accordance with
EN 14181 if required (option) • Sample gas temperature at inlet to 180 … 200 °C, non-condensing
sample preparation system
Performance capability Simultaneous analysis of up to 50 gas • Dust content at inlet to sample prep- Dust-free
components aration system
Standard: 16 components
• Instrument air Oil-free and dust-free instrument air,
T90 time < 180 s, with 20 m sample gas line dew point < -40 °C
• Flow rates • Sample gas: 2 ... 5 l/min
Climatic conditions
• Zero gas: Approx. 0.5 l/min
• Ambient temperature during opera- 0 ... 40 °C, non-condensing • Span gas: Approx. 0.5 l/min
tion • Reference air for optional O2 mea-
• Ambient conditions during storage -20 ... 60 °C, 0 ... 95% relative humid- surement: Approx. 0.7 l/min
and transportation ity, no condensation! • Instrument air to rinse the FTIR
• Site Indoors, dust-free, clean ambient air, spectrometer:
no external vibrations - Normal mode: Approx. 0.5 l/min
- Safety purging: Approx. 4 l/min
Ex zone Non-Ex area (IEC General Purpose) • Reference air for optional O2 mea-
System design surement: Approx. 0.7 l/min
• Type Cabinet configuration • Gas inlets Sample gas (heated to 180 °C), span
gas, zero gas, instrument air
• Cabinet degree of protection IP54
Electrical connections
• Supply voltage (alternative 1) 3 phases 115 V AC (-15%, +10%)/
• Gas outlets FTIR analyzer (heated), O2 analyzer
(heated), span gas for sample probe,
interferometer purging, reference air
4
60 Hz, 32 A + neutral + ground for O2 analyzer
(TN-S) • Gas connections Swagelok 6 mm, for sample gas lines
• Supply voltage (alternative 2) 400 V AC (-15 %, +10%) /50 Hz, with 4/6 mm internal/external diame-
3 phases 230 V AC (-15%, +10%)/ ters of the Teflon core. The external
50 Hz, 16 A + neutral + ground diameter of the sample gas line
(TN-S) including preassembly on the side of
the connection to the sampling unit
• Power consumption Gasmet CEMS with 20 m heated
must be no more than 43 mm.
sample gas line: approx. 7.5 kW
Sample gas pump
Dimensions (with plinth) 2100 x 600 x (800 + 250) mm
(H x W x D) • Material Stainless steel 316
• Diaphragm PTFE
Weight Gasmet CEMS with FTIR and O2 ana-
lyzers: Approx. 320 kg *) • Maximum flow rate 4 l/min
• Heated filter For particles > 2 µm
Electrical inputs/outputs
Valves
Analog inputs/outputs • Solenoid valves Sample gas / backflushing, span gas
• Analog outputs 16 channels, 4 … 20 mA, isolated, via sample outlet, span gas via sam-
freely programmable ple probe, zero gas, instrument air
• Analog inputs 8 channels, 4 … 20 mA, isolated, (safety circuit)
freely programmable • Shut-off valves Sample gas/backflushing, gas infeed
Digital inputs/outputs for maintenance purposes
• Digital outputs 16 channels, 24 V DC, freely pro- FTIR spectrometer unit
grammable
Measuring principle Fourier transform infrared (FTIR)
System alarm, maintenance require- spectroscopy
ment, maintenance, measured value
overshoot, valid measured value Spectral resolution Standard: 8 cm-1
• Digital inputs 16 channels, floating contacts Scan rate 10 scans/s
Temperature alarm sampling probe, Detector Peltier cooled MCT
temperature alarm analysis cabinet,
alarm air-conditioning unit on the Infrared light source SiC, 1 550 K
analysis cabinet, alarm zero gas Beam splitter and window material ZnSe
pressure, alarm O2 analyzer, acti-
vated scan gas infeed via sampling Spectral range 4 200 … 900 cm-1 (2.4 … 11 µm)
probe, activated system standby FTIR gas cuvette Multiple path gas cell with fixed opti-
Optional expansions Up to 255 terminal strips cal path length: 5.0 m
• Material Standard: 100% rhodium-coated alu-
Interfaces (optional) RS 232, RS 422/485, Modbus, minum
PROFIBUS
• Mirror Gold coating
• Cuvette volume 0.4 liters
• Seals Standard: Viton O rings, others: On
request
Window material BaF2
Interferometer purging • Oil-free and particle-free instrument
air, dew point < -40 °C, 0.5 l/min
• Nitrogen (at least 5.0)
4
tive"
Measuring principle FID analyzer
■ Dimensional drawings
3
2 100
4 9
600 50
10 800 + 2
■ More information
Preventive maintenance
The table below offers a general overview of the recommended can be carried out by the operating personnel are described in
tasks for preventive maintenance for a Gasmet CEMS analysis detail in the documentation supplied with each system. For more
system. The actual requirements depend heavily on the individ- comprehensive work, special training courses or service con-
ual conditions of the application and installation. The tasks that tracts are offered.
Maintenance interval Task(s) To be carried out by
Daily Zero gas infeed Automated
1 week Visual inspection of the system and the included analyzers Operating personnel
1 week Visual inspection of the sampling unit Operating personnel
Approx. 30 days Zero gas and span gas infeed Automated
2 to 6 months Inspection and replacement of the filters of the sample probe and the Specially trained operating personnel
sampling unit (included in the annual service with the service contract)
Approx. 3 months Inspection of the oxygen calibration of the ZrO2 oxygen analyzer Automated
(included in the annual service with the service contract)
Approx. 12 months Inspection of the gas cell of the FTIR analyzer Trained service engineer
(included in the annual service with the service contract)
Approx. 12 months If required: Replacement of the diaphragm of the sample pump Trained service engineer
Approx. 12 months Infeed of wet span gases (for NH3, HCl, HF measurement), adjustment Specially trained service engineer
of the "water calibration" (included in the annual service with the service contract,
including provision of the calibration unit required for this
purpose)
18 to 60 months If required: Replacement of optoelectronic components (e.g. laser and Trained service engineer
infrared light source) of the FTIR analyzer
N2
■ Overview ■ Application
The HM-1400 TRX monitors not only the performance of the mer-
cury separators by measuring the total mercury concentration,
but also reports and registers (also online) any violation of the
high limits. As a result it is often possible to intervene directly in
the process of the plant to be monitored and thus ensure reliable
compliance with the specified limit values.
Areas of application
• Waste incineration plants (municipal waste, industrial waste,
hospital waste)
• Sewage sludge and hazardous waste incineration
• Steel plants with scrap metal preparation
• Contaminated soil burning plants (thermal cleanup of soil)
• Crematoriums
• Mercury mines and refineries
• Fluorescent light bulb recycling
Approvals
The HM-1400 TRX is a total mercury monitor for fully automatic
and continuous measurement of emissions of mercury in flue • Suitability-tested by the TÜV North, test report 109 GMT007/
gas ducts. 8000632287 dated 30 June 2011
• Certified according to DIN EN 15267-3
■ Benefits • Itemized in the list of suitable measuring devices for
continuous emission measuring
4
• Extractive measuring procedure
• MCERTS
• Low maintenance dry reactor
• High operational reliability
• Easy maintenance, easy replacement of components
• Low cross sensitivities
• Easy to read LC display
■ Design
Heated
sample probe
Pump
Thermocatalytic
reactor Hg-photometer
Zero gas
filter Liquid
watchdog
Calibration
Gas/liquid
reactor
separator
Option
Stack
Reference
Condensate
standard
■ Function
In the HM 1400 TRX total mercury analyzer the sample gas is
converted into mercury vapor by a combination of thermal and
chemical treatment. It is then continuously measured in a pho-
tometer. The sample gas flow is measured after a sample game
cooler at 2 °C. The concentration is calculated and displayed as
"dry flue gas".
■ Function
The device operates using the double-pass method according
to the auto-collimation principle. The light beam traverses the
Supply box measuring distance twice. The attenuation of the light beam by
the dust content in the measuring section is measured and eval-
uated.
The universal control unit D-ISC 100 can be connected for the
measured value display, which allows up to eight dust and flow-
rate measurement instruments.
The connected equipment can be operated and configured con-
veniently using the D-ISC 100. The display provides an immedi-
ate overview of the current measured values and the status of
the measuring instruments.
■ Technical specifications
Measuring instrument D-R 220
Measurements • Opacity
• Extinction
Measuring ranges
• Opacity 0 ... 25/50/100 %
• Extinction 0 ... 0.2/0.4 ... 1.6
• Dust1) • 0 ... 160 mg/m3
• 0 ... 4000 mg/m3
Measuring principle Transmission
Sample gas temperature Above dew point up to 200 °C,
optional up to 500 °C
Sample gas pressure -50 ... +10 hPa, optional higher
Duct diameter 0.4 ... 10 m
Ambient temperature -20 ... +50 °C
Degree of protection IP65
Measured value output 0/4 ... 20 mA, 400
Digital outputs 2 relay outputs, 30 VA,
max. 48 V/0.5 A
Digital inputs None
Accuracy < 2% of the measuring range
Detection limit < 2% of the measuring range
4
Supply voltage 24 V DC, 0.4 A from the supply unit
Dimensions (H x W x D) measuring 160 x 150 x 314 mm
head
Weight
• Measuring head 2.7 kg
• Reflector 1.6 kg
Supply box
Purge air supply From the supply box
Supply voltage 85 ... 264 V AC, 46 ... 63 Hz, 50 VA
Dimensions (H x W x D) 210 x 300 x 380 mm
Weight 13 kg
Degree of protection IP65
1)
with reference to one meter of path length after gravimetric calibration
■ More information
In general, a dust concentration measuring instrument D-R 220
consists of:
• 1 measuring head D-R 220 M
• 1 zero point reflector
• 1 reflector
• 2 welded tubes with adjustment flange
• 2 purge air adapters with clips
• 1 operating unit (for up to 8 sensors)
• Parameterization software with stick and USB cable
• 1 supply box (incl. purge air blower) 115/230 V, 50/60 Hz
• Operating instructions
• Weather protection covers for measuring head, reflector,
blower, control unit, etc.
Please consult your Siemens sales partner for information on
how to correctly configure and order a D-R 220 measuring in-
strument for a Siemens CEMS project.
■ Overview ■ Design
Optical
measuring unit Reflector
The D-R 290 is an optical opacity/dust monitor for plants with Purge air unit
small to medium dust concentrations.
■ Benefits
• In-situ measuring procedure, continuous measurement Control and
display unit
• Semiconductor source with long service life
• Super-wide band diodes (SWBD), which provides more stable
measuring results in comparison to devices with conventional
LEDs
■ Function
The device operates using the double-pass method according
to the auto-collimation principle. The light beam traverses the
measuring distance twice. The attenuation of the light beam by
the dust content in the measuring section is measured and eval-
uated.
■ Technical specifications
Measuring instrument D-R 290
Measurements • Opacity
• Extinction
Measuring ranges
• Opacity
• Extinction
0 ... 20 to 0 ... 100 %
0 ... 0.1 to 0 ... 1.6 4
• Dust1) 0 ... 80 mg/m3 to 0 ... 4 000 mg/m3
Measuring principle Transmission
Sample gas temperature Above dew point up to 250 °C,
optional up to 1 000 °C, depending
on application
Sample gas pressure -50 ... +20 hPa, optional higher
Duct diameter 1 ... 12 m, optional up to 18 m
Ambient temperature -20 ... 50 °C, optional higher
Degree of protection IP65, Ex optional
Measured value outputs 2 x 0/4 ... 20 mA, 500
Manual or automatic measurement
range switching
optional Modbus RTU, PROFIBUS DP
Digital outputs 6 programmable relay outputs,
permissible load 48 V/0.5 A
Digital inputs 6 programmable isolated inputs
Accuracy < 1 % of measuring range
Detection limit 0.75 % at extinction 0 ... 0.1
Reference point drift < 0.4% of measuring range / month
Zero point drift < 0.4% of measuring range / month
Auxiliary power 95 ... 264 V AC, 47 ... 63 Hz, 30 VA
Dimensions (H x W x D) measuring 363 x 185 x 398 mm
head
Weight 17 kg
Purge air supply
Purge air quantity Approx. 80 m3/h
Auxiliary power 115/230 V AC, 50/60 Hz,
0.37/0.43 kW
Dimensions (H x W x D) 350 x 550 x 500 mm
Weight 12 kg
Degree of protection IP55
1)
with reference to one meter of path length after gravimetric calibration
■ Overview ■ Design
Measuring head Universal control Supply unit with inte-
Mounting flange unit D-ISC 100 grated purge air supply
The D-R 320 is an optical dust monitor for the smallest to medium
dust concentrations in dry emissions and process gas.
■ Benefits
• Continuous measurement of dust concentration
• Easy installation on standard flanges
• Easy setup without manual adjustment
• Automatic background light compensation, no light trap
• Convenient operation, remote access option System components D-R 320
• Automatic control functions Transmitter / receiver unit D-R 320 M
4 •
•
Integrated purge air regulation and purge air control
Long maintenance intervals
The transmitter and receiver optics are integrated together with
the electronics in a compact unit in a rugged housing. The trans-
• Certified to EN 15267-3 mission-reception unit consists of the measuring head, the
swivel adapter, the process connection and the field facing
• Data transmission via Modbus, in compliance with VDI 4201-3 panel. This measuring unit is installed directly above the waste
gas duct, on a DIN 100 PN 6 or ANSI 4" 150 lbs flange. No ad-
■ Application justment is required.
The D-R 320 monitors not only the efficiency of the filter plants Supply unit D-TB 200
by registering the residual dust content, but also reports instan- The supply unit of the dust concentration measuring instrument
taneously when permissible levels of dust or flue gas emissions D-R 320 is used to supply electricity and purge air and provides
are exceeded. As a result it is often possible to intervene directly the connection for the transfer of the measured data. The regu-
in the process of the plant to be monitored and thus ensure reli- lated purge air is used to keep clean the optical interfaces of the
able compliance with the specified limit values. transmission and reception optics of the D-R 320. The device
Areas of application automatically reports any failure of the purging air.
Continuous emission monitoring, for example, on: Optional:
• Incineration plants in general Universal control unit D-ISC 100
• Plants according to IED 2010/75/EU/17. BImschV The connected equipment can be operated and configured con-
• Plants according to 2001/80/EG LCPD/13. BImschV/German veniently using the D-ISC 100. The display provides an immedi-
TA-Luft ate overview of the current measured values and the status of
• Waste, hazardous waste and sewage sludge incineration the measuring instruments.
plants Measured-value acquisition
• Cement manufacturing plants
In the simplest case the measured values and reference values
• Power plants with gas, oil, coal or co-firing are transferred to the plant's control system. The measured val-
• Plants for the incineration of biomass ues and status signals that are sent can also be fed to an emis-
sion calculator system for further processing, either via discrete
Monitoring of: signals (4 to 20 mA and configurable relay contacts) or via
• Ventilation units Modbus according to VDI 4201-3.
• Filter units Quick-closing shutter
Approvals The swivel adapter can be optionally replaced with an adapter
• Suitability-tested by the TÜV Cologne, test report with a fully integrated quick-closing shutter. By using this quick-
936/21217455/A closing shutter the path between the measuring device and the
• Certified according to DIN EN 15267-3 waste gas is closed mechanically, but not airtight in the event of
a fault (failure of power supply or purge air); the measuring de-
vice is temporarily protected against overheating in such cases.
The measuring head takes over the control of the quick-closing
shutter.
Weather protection covers
A weather protection cover is available to protect the measuring
system when it is installed outdoors.
■ Function
The device operates according to the backscattering principle.
The light of a laser diode illuminates the dust particles in the
measuring volume of the flue gas duct. The light reflected by the
particles is measured and evaluated.
The D-R 320 does not require a light trap. The background light
in the stack is detected by means of a special optical system
with an integrated dual detector and automatically compen-
sated without manual adjustment.
The universal control unit D-ISC 100 can be connected for the
measured value display, which allows up to eight dust and flow-
rate measurement instruments.
The connected equipment can be operated and configured con-
veniently using the D-ISC 100. The display provides an immedi-
ate overview of the current measured values and the status of
the measuring instruments.
Control functions
The D-R 320 automatically performs zero and span check as
well as contamination check at regular intervals and on demand.
The device features an automatic contamination correction.
Need for maintenance is immediately indicated by the electron-
4
ics.
■ Technical specifications
Measuring head
Measured variable Dust concentration
Measuring ranges 0 ... 5 mg/m3 to 0 ... 200 mg/m3
Measuring principle Backscattering
Sample gas temperature 0 ... 600 °C
Sample gas pressure -50 ... +50 hPa, optional higher
Duct diameter 0.7 ... 20 m
Ambient temperature -40 ... +60 °C
Degree of protection IP65
Measured value outputs 0/4 ... 20 mA, 400
Modbus RTU bi-directional
Digital outputs 2 relay outputs, permissible load
60 V DC, 30 V AC/0.5 A
Digital inputs None
Auxiliary power 24 V DC/0.5 A
Dimensions (H x W x D) 200 x 190 x 260/410 mm
Weight 15 kg
Supply box
Purge air supply Integrated blower
Supply voltage 115/230 V AC, 50/60 Hz,
0.37/0.43 kW
Dimensions (H x W x D) 480 x 450 x 320 mm
Weight 12 kg
Degree of protection IP65
■ More information
Please consult your Siemens sales partner for information on
how to correctly configure and order a D-R 320 measuring in-
strument for a Siemens CEMS project.
■ Overview ■ Application
By combining four selected measuring functions in a single de-
vice it is possible to automatically calculate the pollutant mass
flow for the preparation of the emission declaration in addition to
monitoring the pollutant dust.
Areas of application
• For measurements in accordance with TIA Air (Technical
Instructions for Maintaining Air Purity) 13., 17. and 27.
BlmSchV
The combined probe sensor D-RX 250 is a single rod measure- • Not suitable for use behind electrostatic precipitators
ment probe for simultaneous measurement of dust concentra-
tion, volume flow, temperature and absolute pressure. Approvals
• Suitability-tested by the TÜV Cologne,
■ Benefits test report 936/800006/A
• Itemized in the list of suitable measuring devices for
• Only one probe/installation opening in the exhaust gas continuous emission measuring
channel
• MCERTS
• Compact design, no moving parts, no consumable parts
• Continuous conversion to normalized dust concentration in
mg/Nm3 and to normalized volume flow in Nm3/h
• LCD display in mg/Nm3, Nm3/h, °C and hPa, one analog
output for each measurement value
• Parameterization at the control unit without the need of a PC or
other tools
■ Design
Max. 1 000 m
■ More information
Please consult your Siemens sales partner for information on
how to correctly configure and order a D-RX 250 combined
probe sensor for a Siemens CEMS project.
■ Overview ■ Application
As in-situ measuring system, the measuring equipment deter-
mines the measured values without sampling directly in the duct
through which gas is flowing.
Areas of application
• Volume flow measurement at high temperatures
• Plants with small or large flue cross-sections
• Volume flow measurement at high pressure
Approvals
The D-FL 100 volume flow measuring system measures the flow • Suitability-tested by the TÜV Cologne,
rate in dry emissions with a probe using the differential pressure test report 936/800006/A
principle. • Itemized in the list of suitable measuring devices for
continuous emission measuring
■ Benefits • MCERTS
• Measuring of emission speed
• Adjustable parameters
• Versions with or without counter-support and for point
measurement
• Calculation of volume flow at standard conditions with evalu-
ation unit D-FL 100-20
• Maintenance interval 6 months
■ Design
Differential pressure
transducer
Flow 4 ... 20 mA
Evaluation unit
4 ... 20 mA
4 ... 20 mA
Flow probe
Flow direction
Approvals Optional:
• Suitability-tested by the TÜV Cologne, test report Universal control unit D-ISC 100
936/21218490/A
The connected equipment can be operated and configured con-
• Itemized in the list of suitable measuring devices for veniently using the D-ISC 100. The display provides an immedi-
continuous emission measuring ate overview of the current measured values and the status of
the measuring instruments.
■ Design Weather protection covers
Weather protection covers are available to protect the measur-
Duct Measuring head ing heads when the measuring system is installed outdoors.
Additional options:
• Absolute pressure transducer
• Temperature transducer
Purge air
Purge air
■ Function
The D-FL 220 measuring system operates according to the
acoustic transit time differential method.
Two identical sensors transmit and receive ultra-sonic pulses re-
ciprocally. The system calculates precisely the gas velocity and
the gas temperature from the transit time difference dependent
on the direction. The volume flow is calculated taking into con-
sideration the cross-section, the sample gas temperature and
the absolute pressure. The D-FL 220 performs internal self-mon-
itoring routines and is very low maintenance.
■ Technical specifications
Measuring system D-FL 220
Measurements • Flue gas velocity
• Volume flow1)
• Temperature
Measuring ranges • 0 ... 40 m/s
• 0 ... 3 000 000 m3/h
• 0 ... 400 °C
Measuring principle Ultrasonic transit-time differential
Sample gas temperature 0 ... 300 °C, optional higher
Sample gas pressure -50 ... +20 hPa, optional higher
Duct diameter 0.5 ... 13 m, temperature-dependent
Ambient temperature -20 ... +50 °C,
measuring head: -40 ... +70 °C 4
Degree of protection IP65
Measured value output 0/4 ... 20 mA, 400
Modbus RTU bi-directional
Digital outputs 2 relay outputs,
permissible load 48 V/0.5 A
Digital inputs None
Accuracy <2%
Detection limit < 0.3% of measuring range
Reference point drift < 0.3% of measuring range / month
Zero point drift < 0.2% of measuring range / month
Auxiliary power 24 V DC/0.5 A
Dimensions standard measuring head Ø 190 x 570 mm
Weight 17 kg
Purge air supply
Purge air quantity Approx. 80 m3/h
Auxiliary power 115/230 V, 50/60 Hz, 0.37/0.43 kW
Dimensions (H x W x D) 350 x 550 x 500 mm
Weight 12 kg
Degree of protection IP55
1)
Optional pressure and temperature correction
■ More information
Please consult your Siemens sales partner for information on
how to correctly configure and order a D-FL 220 measuring sys-
tem for a Siemens CEMS project.
■ Overview ■ Application
The control unit can supply a single sensor or a system consist-
ing of two sensors with power. Several sensors that are con-
nected via a network can also be connected to the D-ISC 100. In
this case each of the sensors must be supplied with power by
means of a separate terminal box, supply unit or evaluation unit.
Modbus links the sensors to each other and to the D-ISC 100.
The display provides an immediate overview of the status of the
connected devices. The current measured values can be dis-
played without the necessity of direct access to the sensors. It is
also possible to visualize the measured values with bar chart
display.
The connected sensors can be queried, controlled and param-
eterized with the control unit. Operation takes place directly via
the membrane keyboard of the control unit. Alternatively, you
can connect a PC via the integrated USB port. In conjunction
with the Web server technology software D-ESI 100, remote sup-
port is possible via the Internet.
The D-ISC 100 universal control unit permits the connection of
The control unit features four slots for extension modules, for ex-
up to 8 sensors combining dust and volume flow measurements
ample, Modbus RTU or analog / digital input and output mod-
on one display.
ules.
■ Benefits You also have the option of including an external converter (e.g.
PROFIBUS DP) inside the unit. This eliminates the need for an
• Connection of up to 8 sensors additional housing in equivalent degree of protection.
4
• Large liquid crystal display (LCD) for display of the measured
values Approvals
• Automatic detection of connected sensors Type-tested according to European directive EN 15267 for con-
tinuous emission measurements in connection with the test re-
• Easy parameter assignment of connected sensors ports no. 936/21217455, 936/21218492 and 936/21218490 of
• Operation locally via membrane keyboard or USB port, or the Technical Inspectorate of the Rhineland region (TÜV Rhein-
remote control via the RS 485 interface land)
• Modular design, four slots available for extension modules
• Slot for external converter ■ Design
• No maintenance costs The following functions can be added to the D-ISC 100 control
• Easy to update via SD card unit by means of plug-in modules:
• Modbus RTU module
• Analog input module with four analog inputs: 0 to 20 mA with
2/4 mA live zero, burden 50
• Analog output module with four analog outputs: 0 to 20 mA
with 4 mA live zero, max. burden 400
• Digital input module with eight digital inputs
• Digital output module with eight digital outputs
■ Technical specifications
Basic unit
Output signal 0 ... 20 mA, zero point 4 mA
Maximum burden 400
Relay outputs 3 x status, isolated (limit value, fault,
control cycle, etc.)
Maximum switching power 48 V/0.5 A
Inputs 1 x function, isolated
Ambient temperature -20 ... +50 °C, optional -40 ... +60 °C
Electrical data
Line voltage 90 ... 264 V, 48 ... 62 Hz
Power Approx. 100 W
Auxiliary power for sensors 24 V DC/2 A
Mechanical specifications
Material Stainless steel 1.4301
Color RAL 5017
Degree of protection IP65
Weight 5 kg
Dimensions (H x W x D) 130 x 330 x 220 mm
Expansion options
Modbus RTU module
Interface RS 485, serial
4
Baud rate 9600 ... 57 600 Bd
Analog input module
Output signal 0 ... 20 mA, zero point 0/2/4 mA
adjustable
Load 50
Analog output module
Output signal 0 ... 20 mA, zero point 4 mA
Maximum burden 400
Digital input module
Inputs 8 x function, isolated
Digital output module
Relay outputs 8 x status, isolated (limit value, fault,
control cycle, etc.)
Converter module
Type PROFIBUS DP
■ More information
Please consult your Siemens sales partner for information on
how to correctly configure and order a D-ISC 100 control unit for
a Siemens CEMS project.
■ Overview
4-20 mA,
Ring memory Modbus,
6 years int, day PROFIBUS, Ring memory
+ protocols OPC, ELAN > 32 days
30 days 1 min + 1 s
1 ... 8
Ring memory
> 32 days
4-20 mA, D-EMS 4-20 mA, D-MS D-EMS 2000 D-EMS 2000 D-EMS 2000
2000 CS 500 KE Client Client Client
Modbus, Modbus,
PROFIBUS, PROFIBUS,
OPC, ELAN OPC, ELAN
TCP/IP TCP/IP
Authority Internet
Ring memory
> 5 years
Individual values
Protocols
4 System
Raid 1
Backup on DCF77
HD/SSD GPS
System Workstation D-EMS 2000
The D-EMS 2000 environmental and process data management system is a modular system for the continuous acquisition, long-term
storage, calculation and visualization of environmental and process data.
■ Benefits ■ Application
• Instrument for monitoring legally prescribed limit values and The D-EMS 2000 standard system is designed for small to me-
recording their observance dium sized industrial sites whose emission data, immission data
• Emission monitoring and remote data transmission to the or process data must be recorded in line with government regu-
authorities lations for measured data logging.
• Corresponds to EU directives 2000/76/EU, 2001/80/EU and Approvals
2010/75/EU
• Suitability-tested by TÜV in accordance with German TA-Luft,
• Adjustable to any plant size through to complete assessment 1., 2., 13., 17., 27., 30. and 31. BImSchV
of complex industrial sites
• Itemized in the list of suitable systems for evaluation of
• Continuous monitoring of 1 to 320 components per system continuous emission measuring
workstation
• Certified according to DIN EN 15267-2
• Interconnection of any number of components via data
networks • MCERTS certified
• Visualization available in 19 languages
■ Design
Measured data acquisition:
• Analog/digital inputs as
- 19" rack with ring memory
- Local DIN rail modules
• Data communication via bus systems, Modbus RTU/ TCP,
PROFIBUS, Elan, OPC UA
■ Function
Data sources
• Emission data
• Immission data
• Meteorological data
• Water data
• Process data
Data export
• Data interface to MS-Excel with option of further measured
data evaluation, e.g. for fulfillment of environmental protection
officer’s reporting duties
• Measured data can be transferred to authorities via standard
remote communication or via Internet
• Merging of measured data e.g. for greenhouse emission
trading
• Remote service interface for fast and cost effective service
Data security
• Industrial type evaluation PC with vibration-proof hard disks in
RAID 1 array and special air cooling with filter system
• Paperless data storage to replace recorders and printers is
possible through integrated data security, which is
guaranteed on several levels in the system
• Intermediate storage of the raw input values at minute
intervals in data communication unit D-MS 500 KE
4
• Storage of raw input values in one-second intervals
• Data backup on external redundant drive
Internet/intranet connection
• Data transmission to an Internet server with HTML standard
masks via standard software (MS Internet Explorer)
• Password protected control of daily emission values including
the classification records
Visualization
• Measured data logging according to official regulations
• Classification tables, daily, monthly and annual records
• Representation of current, prognostic and historic measured
data in bar/linear form
• Pollutant compensation, characteristics curve and correlation
• Automatic alarm and information system
Annual emission declaration
• Automatic preparation of annual emission declaration, from
the individual values stored in the system, according to
11. BlmSchV
• Compatible with official software, import/export module
• Automatic filling in of forms
• Reading in of historical emission declarations
■ More information
Please consult your Siemens sales partner for information on
how to correctly configure and order a D-EMS 2000 environmen-
tal and process data management system for a Siemens CEMS
project.
■ Overview
Ring memory
Authority Internet
6 years int, day
+ protocols 30 days
1 min + 1 s
Backup on DCF77
HD/SSD GPS
4
The D-EMS 2000 CS environmental and process data management system is an affordable compact system for small to medium
plants.
■ Overview ■ Application
The efficiency of biogenic production processes and optimum
operation of the plant largely depends on continuous monitoring
of the biogas composition. The basic version of the Set BGA an-
alyzes CH4 and CO2 using the proven ULTRAMAT 23 IR ana-
lyzer. The concentrations of O2 and H2S are optionally measured
using electrochemical sensors and also converted into output
signals of 4 to 20 mA. In this manner, the Set BGA contributes to
operational safety and explosion protection in addition to pro-
cess optimization.
The modular design of the system takes into account the physi-
cal conditions of the gas with regard to temperature and mois-
ture in that various gas preparation components for heating or
drying the sample gas can be configured as required.
The gas mixture can be explosive at critical concentration ratios
between methane and oxygen. Even if such critical gas compo-
sitions occur extremely rarely, the danger of ignition must never-
theless be avoided. For this reason, the Set BGA is designed
with a high safety standard and even the basic version is
The Set BGA (biogas analyzer) is a standardized system for sta- equipped with flow monitoring and detonation protection in ac-
tionary, continuous operation for the analysis of landfill gas, sew- cordance with EN 12874 in the sample gas path. To increase
age gas or biogas. safety even further, a gas sensor for monitoring the ambient air
can be connected as an option.
■ Benefits It is also possible to monitoring up to four measuring points us-
ing an optional sample switching cabinet. In this case the sam-
Standardized complete system
The standardized complete system has a modular configuration
ple flows are sucked in continuously using a powerful pump in
order to achieve fast measuring times. 4
and can thus be used at various measuring locations for different
measuring tasks.
• Simple and fast to configure
• Field-tested and matched Set in rugged industrial design
• Extremely high long-term stability
• The Set BGA is based on the proven ULTRAMAT 23
Field-proven, reliable technologies
• Autocalibration function with ambient air reduces the mainte-
nance requirements
• Detonation protection in accordance with EN 12874
• Modular system design based on long-term tested compo-
nents
• LEL sensor for cabinet monitoring (optional)
Simple operation
• Intuitive menu guidance
• Configuration on large displays with plain text
• Two freely-configurable limits per measured component
be calibrated every three months. An appropriate calibration Sample preparation 600 x 600 x 220 mm
gas is therefore required. It is supplied to the analyzer through a (W x H x D)
manually switchable ball valve. Weight
Set BGA measuring system Approx. 50 kg
Sample preparation Approx. 22 kg
System design
■ Design
The Set GGA is available in the following versions:
• Generator Gas Analyzer (GGA)
• GGA with test gas skid
• GGA with test gas skid and installation frame
Analyzers
The GGA contains two CALOMAT 6E analyzers (19" rack unit
versions). From the gas sampling system right through to the gas
The standardized Set GGA (Generator Gas Analyzer) has been outlet, these are completely separate from one another, thereby
specially designed for monitoring hydrogen-cooled turbo gener- ensuring full redundancy.
ators.
The CALOMAT 6E is a continuous gas analyzer for determining
H2 and He in binary or quasi-binary gas mixtures.
■ Benefits
To measure the hydrogen and inert gases continuously, the ex-
Standardized complete system
• Simple and fast to configure
act thermal conductivity of the sample gas mixture is measured
and the concentration calculated from this. Only binary gas mix- 4
tures can be directly measured.
• Field-proven, harmonized and reliable set
• Low purchase price and economic operation The CALOMAT 6E is used to measure 0 to 100 % CO2/Ar in air,
0 to 100 % H2 in CO2/Ar or 80 to 100 % H2 in air, in the context
• Suitable for optimizing the efficiency of H2-cooled turbo of monitoring hydrogen-cooled turbo generators, on account of
generators its high measuring range dynamics.
Field-proven, reliable technologies The units are approved for use in ATEX Zone 2. Gas mixtures
• High-precision and reliable purity monitoring of hydrogen may also be fed in according to the definition of Zone 1. In terms
of tightness and compressive strength, the measuring cell and
• Microchip-based thermal conductivity measurement
entire physical structure of the gas path, from inlet to outlet, are
• Redundant measuring system certified up to 55 000 hPa . This is much higher than the pressure
• SIL 1 certificate for the analysis hardware that arises when oxyhydrogen gas is ignited.
Simple operation A flame arrestor at the sample gas inlet provides additional
safety.
• Intuitive menu prompting
• Configuration on large displays with plaintext The integrated LCD display shows the measured values, status
bar and measuring ranges simultaneously.
• Use of CO2 and AR as inert gas possible
The T90 time is less than 5 s. This means that the delay between
the measurement and displaying the result is very short.
■ Application
Tests carried out under harsh field conditions have indicated that
This set is used in power generation applications. the 3-week drift of the measurement results is less than 0.1 %.
Turbo generators in power plants are cooled with gas in order to Combined with a repeatability value of 0.1 %, this ensures that
increase their efficiency. In spite of the strict safety requirements the measurement results gathered will be both accurate and
hydrogen is used as a cooling gas. This offers huge advantages precise.
over air. These include considerably better cooling properties,
lower friction loss on rotating parts, and a higher electrical
breakdown strength. These features enable hydrogen to satisfy
the requirements for the turbo generator to reach an optimum
level of efficiency.
However, mixtures of hydrogen and air with a hydrogen content
of anything from 4 to 77 % are explosive. For safety reasons, it is
imperative that this is prevented during operation filling and
emptying of the turbo generators. International standards
(EN 60034-3 and IEC 842) state that redundant safety monitor-
ing with two independent operating systems must be used for
this.
■ Technical specifications
Climatic conditions Measuring response (relating to sample gas pressure 1 013 hPa absolute,
0.5 l/min sample gas flow and 25 °C ambient temperature)
Ambient temperature 5 ... 50 °C
Output signal fluctuation < ± 0.75% of the smallest possible
Relative humidity 70 %, non-condensing measuring range according to rating
Corrosive atmosphere No plate, with electronic damping con-
stant of 1 s ( = 0.25%)
Gas inlet conditions
• Calomat 6E Zero point drift < 1%/week of the smallest possible
span according to rating plate
- Sample gas pressure 800 ... 1 100 hPa (absolute)
Measured-value drift < 0.5%/of the smallest possible span
- Sample gas flow 30 ... 90 l/h (0.5 … 1.5 l/min) according to rating plate
• Test gas skid
Repeatability < 1% of the current measuring range
- Sample gas pressure 55 000 hPa (absolute)
Detection limit 1 % of the current measuring range
- Sample gas flow 30 … 90 l/h (0.5 … 1.5 l/min)
Linearity error < ± 1 % of the current measuring
Power supply
range
• Supply 1 200 ... 240 V AC, 47 ... 63 Hz
• Supply 2 100 ... 120 V AC, 47 ... 63 Hz Influencing variable (relating to sample gas pressure 1 013 hPa absolute,
0.5 l/min sample gas flow and 25 °C ambient temperature)
• Supply 3 24 V DC for switch amplifiers
Ambient temperature < 1%/10 K referred to smallest possi-
Type of connections ble span according to label
Pipe material Stainless steel
Accompanying gases Deviation from zero point
Connections/components • Metric (6 mm) Sample gas flow < 0.1% of the smallest possible span
• Imperial (¼") according to rating plate with a
Cabling change in flow of 0.1 l/h within the
permissible flow range
Electrical design According to IEC
Sample gas pressure < 1 % of the current measuring range
Type of cables
Cable ID
Non-armored cables
No single core labeling Power supply
with a pressure change of 100 hPa
< 0.1 % of the current measuring
4
Installation range with rated voltage ± 10 %
Site Interior
Ex-zone analyzer ATEX II, 3G
System design
Version Cabinet
Degree of protection IP54
Automatic calibration No
Signal outputs 4 ... 20 mA/isolated contact
Max. 24 V AC/DC 1 A
With sample gas return flow On request
4
M20x1.5 power supply with test gas skid (PA on stainless steel plate), ready mounted
on frame, delivery batch 1 part
Explosion protection
Certificate: ATEX II 3G, flammable and non-flammable gases B
Documentation
German 0
English 1
French 2
Spanish 3
■ Dimensional drawings
685 615
CALOMAT
Siemens
MKG31 CQ001
612
Siemens
MKG32 CQ001
Line
pressure
-FA1 -FA2
regulator
Protective casing 110
130
2000
5-way
1900
-RB5
(screwed)
4
Stopcock
1300
ball valve
Flow meter
Test gas skid Test gas skid
-SV1 -SV2
-RB1 -RB2 -RB3
40
Low-pressure
910
overflow regulator
■ Design
Standardization of systems means good clarity and simple facil-
ities for configuration. Different versions mean that it is possible
to appropriately adapt the system to the requirements. The mod-
ules can be combined as desired. Standardization also means
that not all imaginable versions are included, and that special re-
quirements such as armored cables, customer-specific docu-
mentation, specific conductor labeling, or certificates such as
CE or 31B cannot be implemented at all, or not without an extra
charge.
The design is divided into the following standard modules: sam-
pling, pressure reduction, sample preparation system,
SITRANS CV, gas supply, calibration gases.
The Set CV (Calorific Value) is a standardized system for deter-
mining the quality of natural gas with SITRANS CV and
MicroSAM.
Gas supply
station
■ Benefits
Standardized complete system
4 • Easily and quickly configured, from sampling to the gas
supply
• Field-proven, harmonized and reliable set
• Suitable for determining the natural gas quality with high Sampling Sample SITRANS CV Flow
accuracy probe preparation computer
CV Control SW
Field-proven, reliable technologies
• Version with German Federal Testing Authority certification
(without mass memory, without DSfG) available for fiscal
metering
• GC MEMS technology with low consumption levels, high
linearity/accuracy over the entire measuring range, and short
cycle times
General information
Easy installation
The set can be dimensioned for a 230 V AC or 115 V AC power
• Installation in EEx Zone 1 possible supply. It is not possible to switch between supplies.
• Compact and rugged design for erecting indoors and
The gas connections can be supplied with either metric or impe-
outdoors
rial dimensions.
• Minimum space requirements
On the metric line, the gas connections are in the form of metric
clamping ring glands with a diameter of 3 mm. The imperial line
■ Application contains gas connections in the form of imperial clamping ring
For the chromatography industry, the natural gas market is one glands with a diameter of 1/8 inch. The pipes between the sam-
of the fastest growing in the world. There are a variety of reasons pling probe, pressure reduction, sample preparation device,
for this. While global energy requirements are increasing, there and SITRANS CV are optionally available. The system is gener-
is a parallel trend of fossil fuel reserves being depleted. Natural ally designed for temperatures between -20 and +55 °C in areas
gas is one type of fossil fuel that can still be found in vast, un- with a risk of explosions. When provided with heating, the sys-
tapped reserves. In addition to this, the market is becoming in- tem can also be used down to -30 °C. The natural gas to be mea-
creasingly liberalized, and the number of participants has risen sured should be in a stable gaseous form, dry and clean.
considerably as a result - from the production stage, across the Sampling probe
entire distribution network, right through to the end customer. In
turn, this has generated more transfer points at which the quality The basic components of a sampling probe are a lance, process
and quantity of natural gas need to be determined for account- connection, process isolation and, if necessary, pressure reduc-
ing purposes. tion. The high-pressure version is not supplied pre-assembled.
The market requires a reliable complete system which is spe- Lance
cially designed for natural gas. With the Set CV, Siemens offers A representative sample should be taken from the central third
a system that covers all the requirements of such applications, of the pipeline. With a lance length of 1 m it is therefore possible
from sampling to pressure reduction, sample preparation and to extract a sample from a pipeline with a diameter of up to
determination of quality, supplying carrier and calibration gases, 1 600 mm. In addition, two versions with different types of lance
right through to expansion of the communication interfaces. diameter are available. On the one hand, a pipe whose outer di-
The set offers various modules to cover market requirements. ameter is 6 mm and inner diameter is 2 mm. And on the other, a
Using the different versions, the set can be adapted, and the pipe whose outer diameter is 12 mm and inner diameter is 8 mm.
modules can be freely-combined. The lance can be supplied in a permanently installed or remov-
able state (not for 12 mm).
The system components selected are mounted and supplied SITRANS CV/MicroSAM system components
with all pipes and wires installed in the protective casing. Protective casing/plate for SITRANS CV/MicroSAM
It is also possible to provide a heater in the protective transmitter The SITRANS CV/MicroSAM is available mounted either on a
box which can be controlled between 10 and 40 °C in steps of plate, in the protective casing, or in the heated protective casing.
5 degrees. The system components selected are mounted and
supplied with all pipes and wires installed in the protective cas- The stainless steel mounting plate, measuring 682 x 482 x 3 mm
ing. The heating has a power of 400 W. (H x W x D), is suitable for wall mounting.
Aerosol filter/glycol filter The unheated protective transmitter box, made from fiber glass-
reinforced plastic and suitable for wall mounting measures
These filters have the task of removing any impurities that may 800 x 600 x 480 mm (H x W x D) and is fitted with stainless steel
have been introduced into the natural gases by aerosols or gly- hinges, quick-release locks, safety glass windows and a stain-
cols, thus providing an additional level of safety for the less steel mounting plate.
SITRANS CV and, therefore, the system functionality. The aero-
sol filter is supplied with 5 replacement diaphragms and the gly- The protective casing can also be supplied with heating as an
col filter with 10 replacement cartridges. option. The heating can be adjusted between 10 and 40 °C, in
increments of 5. The system components selected are mounted
Manual laboratory sampling and supplied with all pipes and wires installed in the protective
An additional control valve permits manual laboratory sampling casing. The heating has a power of 400 W.
as an option. When not in use, it is fitted with a blanking plug on
the output end.
Pipe base for enclosure attachment
A hot-dip galvanized 2" pipe base, 1 700 mm high, with mount-
ing brackets and joining sheet enables free-standing mounting
of the protective casing or the mounting plate as an alternative
to wall mounting.
■ Technical specifications
General information System components
Ambient temperature -30 ... 55 °C (with heating) On mounting plate 682 x 482 x 3 mm
Explosion protection ATEX Category II 2G, T3 In protective casing 800 x 600 x 480 mm
Supply voltage 230 V AC, 115 V AC or 24 V DC Protective casing heating Power consumption 400 W
Max. permissible pressure at 16 000 kPa Adjustable between 10 and 40 °C, in incre-
input of high-pressure reduc- ments of 5.
tion Terminal box 340 x 170 x 91 mm
Max. permissible pressure at 16 000 kPa Pipe base 2-inch pipe base, 1700 mm high
input of sample preparation
system with pressure regula- Heated line Heating power is 38 W per meter
tor
Self-regulating heating up to approximately
Max. permissible pressure at 10 ... 60 kPa above atmospheric pressure 80 °C
output of sample preparation Notice: Sample must not contain ethine!
Outer material is PE
system
corrugated hose with 43 mm outer diameter
Sampling
Gas supply
Lance Outer diameter 6 mm and inner diameter
2 mm Transfer station Max. cylinder pressure 20 000 kPa
or outer diameter 12 mm and inner diameter Output pressure 50 ... 1 000 kPa
8 mm Pipe base 2-inch pipe base, mounted
Length 1 000 mm8 Height 2 200 mm
Special probe with BTU dia- Immersion depth approx. 380 mm Gas cylinder cabinet Gas cylinder cabinet for two 50 l carrier gas
phragm and pressure reduc- Protection pipe outer diameter 25.4 mm cylinders and one 10 l calibration gas cylin-
tion, non-retractable der. Dimensions are 1 250 x 400 x 2 050 mm
Process connection At flange DN65 PN16 Form C, Cylinder heating The cylinder heating system is dimensioned
4
max. 1 600 kPa gas pressure for 10 l calibration gas cylinders and ensures
At flange DN65 PN160 Form E, that no condensation occurs within the gas
max. 16 000 kPa gas pressure cylinder.
At flange ANSI, 2-inch, 300 lbs RF Cylinder pressure reducer Cylinder pressure reducer for reducing pri-
At flange ANSI, 2-inch, 2 500 lbs RF mary pressure of max. 30 000 kPa to back
pressure 0 … 400 kPa
High-pressure reduction in Casing with dimensions 385 x 485 x 380 mm
casing with pressure regula- Primary pressure 16 000 kPa, output pres- Heated line Heating power is 38 W per meter
tors, optional heating Self-regulating heating up to approximately
sure 100/170 kPa (power consumption 150 W) 80 °C
Pipe base 2-inch pipe base for free-standing transmitter Outer material is PE
box, 1 700 mm high corrugated hose with 43 mm outer diameter
Heated line Heating power is 38 W per meter Calibration gas
Self-regulating heating up to approx. 80 °C
Outer material is PE corrugated hose with Gas mixture 1 ... 6 The gas mixture is stable for 36 months.
43 mm outer diameter
Sample preparation for 1 to 3 sample gas flow, plus calibration gas flow
Basic configuration 0.5 µm filter, 3/2-way solenoid valve, flowme-
ter, overflow valve and stopcock
Pressure regulator, optional Primary pressure 16 000 kPa, output pres-
heating sure 100/170 kPa (power consumption 150 W)
Simple sample injection One 3/2-way solenoid valve per sample gas
stream
DB&B sample injection Two 3/2-way solenoid valves per sample gas
flow
On mounting plate 652 x 422 x 3 mm
In protective casing 750 x 520 x 430 mm
Protective casing heating Power consumption 300 W
Adjustable between 10 and 40 °C, in incre-
ments of 5
Pipe base 2-inch pipe base, 1 700 mm high
Additional filters Aerosol, glycol
4 Ex terminal box with electrical sample gas monitoring and standard sample injection;
115/230 V AC connection
3 3
Ex terminal box with electrical sample gas monitoring and DB&B sample injection; 4 4
115/230 V AC connection
Additional versions Order code
Add "-Z" to Article No. and specify Order code
Pipe bases for securing the enclosure without mounting plate/box B01
Protective top cover GRP B02
Preparation of heated line B03
Heated line for sample preparation device/SITRANS CV (C01 + C01 = 2 m) C01
Installation kit (pipe/glands/cable) for connecting to the sample preparation device C02
Separate stainless steel pipe 3.0 x 0.5 mm or 3.18 x 0.56 mm (continuous) C03
at 5 m intervals (example: C03 + C03 + C03 = 15 m)
■ Overview ■ Application
The ASM is a PC-based HMI system for monitoring, testing and The ASM is ideal for all systems and plants where high reliability
administration of analyzers in subsystems or in the complete of the measured values and documentation of the analyzer per-
plant. The relevant information of the analyzers is collected over formances are required. Using the communications network, re-
a uniform communications network and saved in a central data- mote analyzers can also be monitored from a central worksta-
base. By means of the PC's user-friendly operator interface it is tion.
possible to access measured-value trends, device statuses and
statistical evaluations, among others, or to start test routines for The ASM is particularly suitable for use in the oil & gas, petro-
validation of the results. A comprehensive reporting module is chemical, and chemical industries, and can be applied in new
available to document the evaluations. plants or also in existing plants to optimize the analyzer land-
scape.
■ Benefits ■ Design
• Monitoring, testing and administration of many different types
of analyzers using one system System design
• Visualization and operation using a single-user system up to • PC-based HMI system
distributed multiuser systems with redundant servers • Visualization and operation possible using a single-user
• Assessment of the measured-value reliability through system up to distributed multi-user systems with redundant
checking of the analyzers using various validation routines, servers
e.g. based on the industry standard ASTM D 3764 • Logging and archiving of process and system data in a central
• Increase in analyzer online time through use of the line sample database
method • Integration of different analyzers in a uniform communications
• Statistical evaluation of operating statuses and determination network
of key performance indicators (KPI) such as availability, error
rate and maintenance frequency System software
• Siemens SIMATIC WinCC for the HMI functions
4 • Reduction in maintenance costs through device-specific
planning, implementation and checking of maintenance work • Microsoft SQL Server for archiving and data collection
• Documentation of the performance of individual analyzers up • Microsoft Windows/ Windows Server as operating system
to the complete plant using the reporting module. The reports
can be saved in the ASM or exported for further use. Communication
• An Ethernet network is the basis for communication
• Integration of analyzers using PROFINET, ModbusTCP or OPC
data exchange
• Analyzes without a communication interface can be
integrated by connecting the signals to Siemens SIMATIC
components
• Data exchange with other systems possible using OPC
Networking
• Siemens Scalance Ethernet switches for design of electrical
and optical Industrial Ethernet in line and star structures;
design in ring structures is possible to increase the fail-safety
of the network
• Integration of the ASM in an existing Ethernet network may be
possible
■ Function
General information
The information of the analyzers is collected over the communi-
cations network and saved in the central ASM database for fur-
ther analysis. The ASM is accessed using a Windows worksta-
tion, and it is possible to navigate between overview displays,
device-specific displays, and general functions.
Report: AnalyserPerformance
From: 02/02/2010 01:19:00 PM Until: 04/02/2010 11:19:00 AM
4
Shelter: AH-101
Analyser: 10-AT-105001
Checking 5.48 %
Checking (TCHK) 2.42 h 5.48 %
Breakdown 0.81 %
Breakdown (TBRK) 0.36 h 0.81 %
Shelter: AH-101
Analyser: 10-AT-105001
The ASM has the following function modules for each analyzer Calibrations:
Stream
Validation_20
Validation_20
Date / Time
04/02/2010 10:00:31 AM
04/02/2010 08:54:31 AM
Validation Procedure
Bottle4Anlz001
Bottle4Anlz001
Result
Valid
Valid
Validation_20
Validation_20
04/02/2010 12:16:02 AM
03/02/2010 11:10:11 PM
03/02/2010 10:07:11 PM
Reference Sample Validation
Bottle4Anlz001
Bottle4Anlz001
Valid
Valid
Valid
Process Provides a detailed overview of the selected analyzer. The cur- Validation_20
Validation_20
Validation_20
03/02/2010 06:49:41 PM
03/02/2010 05:46:51 PM
03/02/2010 04:41:02 PM
Reference Sample Validation
Bottle4Anlz001
Bottle4Anlz001
Valid
Valid
Warning
Validation_20
Validation_20
03/02/2010 03:35:11 PM
03/02/2010 03:29:22 PM
03/02/2010 09:31:01 AM
Reference Sample Validation
Bottle4Anlz001
Bottle4Anlz001
Warning
Warning
Failed
tion data are displayed. The current measured values are Validation_20
Validation_20
Validation_20
03/02/2010 08:25:41 AM
03/02/2010 07:20:22 AM
03/02/2010 06:15:11 AM
Reference Sample Validation
Bottle4Anlz001
Bottle4Anlz001
Warning
Warning
Warning
Validation_20
Validation_20
03/02/2010 05:09:52 AM
03/02/2010 04:07:31 AM
03/02/2010 02:59:11 AM
Reference Sample Validation
Bottle4Anlz001
Bottle4Anlz001
Warning
Valid
Valid
Validation_20
Validation_20
02/02/2010 08:30:01 PM
02/02/2010 07:24:41 PM
02/02/2010 06:25:02 PM
Reference Sample Validation
Bottle4Anlz001
Bottle4Anlz001
Valid
Valid
Valid
4 One of the core functions of the ASM is checking the analyzers for client
for reliability of the measured values. Two different methods of • Windows 2003 Server SP2
measurement are available for recording the values, namely the PC hardware requirements
reference sample method and the line sample method. The re- • Processor type (recommended) • Server: dual core, 3 GHz
sulting values can be checked using different evaluation meth- • Client: Client: dual core, 2 GHz
ods (based on ASTM D3764 or deviation). The objective of the • RAM (recommended) • Server: 4 GB
validation is to recognize fluctuations and deviations with re- • Client: 2 GB1)
spect to a comparison value, and to thus permit a statement to • Graphics card (recommended) 32 MB, 1280 x 10241)
be made on the reliability and drift of the measurement. • Hard disk (recommended) • Server: 2 x 160 GB (Raid 1)
• Client: 80 GB
Method of measurement: reference sample method • Hard disk (free space for installation, • Server: > 40 GB
recommended) • Client: > 1.5 GB
The analyzer is disconnected from the process gas, and a refer-
• DVD-ROM/ USB port For software installation
ence gas connected for measurement. The composition of this
reference gas has previously been specified in the "Reference 1)
Hardware requirement when using Microsoft XP Professional
bottle management" of the ASM. Using these values, the ASM
determines the deviation between the measurement and the ref-
erence data.
■ More information
Method of measurement: line sample method Please contact your Siemens sales partner for further informa-
tion and for ordering.
With this method, a gas sample is extracted from the stream of
sample gas to the analyzer, and analyzed in the laboratory. The
resulting values are passed on to the ASM and compared with
the analyzer's measured values. With this method, the analyzer
need not be disconnected from the process gas, and perma-
nently remains available for the process measurement.
Evaluation based on ASTM D3764
Based on the international standard ASTM D3764, the results
are checked using various statistical methods, including stan-
dard deviation, Dixon freak value test, and systematic error.
Evaluation using deviation method
Limit values are defined for this evaluation: the warning limit and
the control limit. Simple rules are used to define how the reliabil-
ity of the measurement is to be assessed when these limits are
violated. For example, it can be defined that a single violation of
the limit can be tolerated, but that repeated violation is an imper-
missible condition.
General information
5/2 Communication
5/2 Continuous gas analysis
5/7 Gas analysis library for SIMATIC PCS 7
5/8 Process gas chromatography
5/13 Ex versions
5/13 Continuous gas analysis, extractive
5/21 Continuous gas analysis, extractive
ATEX II 2G control unit
5/22 Continuous gas analysis, extractive
ATEX II 2G control unit,
leakage compensation
5/24 Continuous gas analysis, extractive
ATEX II 2G/3G control unit,
continuous purging
5/26 Continuous gas analysis, extractive
Purging unit FM (Class I Div 2)
5/27 Continuous gas analysis, extractive
Additional units
5/29 Continuous gas analysis, in-situ
LDS 6
5/31 Continuous gas analysis, in-situ
LDS 6, EEx barrier
5/32 Continuous gas analysis, in-situ
SITRANS SL
5/33 Process gas chromatography
5/34 Tables
5/34 Conversion tables
5/35 Dew point/saturation table
5/37 International standards
5/39 Definitions
Siemens PA 01 · 2015
© Siemens AG 2014
General information
Communication
Continuous gas analysis
■ Overview
Reliable functioning of analyzers is of decisive importance for Networking over ELAN
process control. It is necessary to record, correct and transmit
measured values, to set and modify parameters, to check func- ELAN communication is used e.g. for the correction of cross-in-
tions, to update calibrations, and to scan status signals e.g. for terference. Direct connection is only possible between Siemens
preventive maintenance. Communication between the operator gas analyzers.
and device is therefore an important part of process analysis, Specification for the interface cable
and the offered facilities have become a decisive performance Surge impedance 100 ... 300 , with a measuring
feature of analyzers. frequency of > 100 kHz
Extractive Cable capacitance Typ. < 60 pF/m
The gas analyzers of Series 6 (ULTRAMAT 6, Core cross-section > 0.22 mm2, corresponds to
ULTRAMAT/OXYMAT 6, OXYMAT 6, OXYMAT 61, FIDAMAT 6 AWG 23
and CALOMAT 6) as well as the ULTRAMAT 23 offer the following Cable type Twisted pair, 1 x 2 conductors of
communications facilities in addition to data transmission over cable section
analog and binary outputs:
Signal attenuation Max. 9 dB over the whole length
• RS 485 interface
Shielding Copper braided shield or braided
• SIPROM GA shield and foil shield
• PROFIBUS DP/PA Connection Pin 3 and pin 8
• Generic communications interface (only OXYMAT 6,
ULTRAMAT 6 and ULTRAMAT/OXYMAT 6).
RS 485 interface
The serial interface integrated as standard permits communica-
tion between several analyzers over the internal bus (ELAN). Pa-
rameterization is carried out using the analyzer’s menu.
0
*1'
9-pin connector
(RS 485)
5
9 (device 1)
0
0
*1'
9-pin connector
(RS 485)
9 (device 2)
0
0
*1'
9-pin connector
(RS 485)
9 (device 3)
0
General information
Communication
Continuous gas analysis
Bus terminating resistors Hardware requirements
Pins 3-7 and 8-9 of the first connector of a bus cable must be The following hardware and system requirements must be
bridged (ELAN networking). provided for the PC/laptop configuration in order to use
SIPROM GA:
Note
• Windows computer with Pentium 133 MHz and 32 MB RAM:
It is advisable to install a repeater on the device side in the case Recommendation: Pentium II 266 MHz and 64 MB RAM
of a cable length of more than 500 m or with high interferences.
• CD-ROM drive (for installation)
Networking with SIPROM GA • Vacant hard disk capacity of at least 10 MB
When used externally, the RS 485 interface requires software • VGA graphics card (Windows-supported);
matched to the analyzers, e.g. SIPROM GA. resolution: 1024 x 768
SIPROM GA is a software program for communication between • Printer (Windows-supported)
PC/laptop and analyzers. A maximum of 12 devices (electronics • MS-Windows 95, ME; NT 4, Windows 98, Windows 2000 or
modules) with up to four channels/measured components of the Windows XP operating system
following type can be connected, displayed and remote-con-
trolled per COM interface: • Vacant COM port (COM 1, 2 ...)
- The RS 485 / RS 232 interface converter is required for
• OXYMAT 6/61 coupling to the RS 485 ELAN network
• OXYMAT 64 - A standard 10-Mbit or 100-Mbit network (RJ45 connection)
• ULTRAMAT 6 with TCP/ IP is required for connecting the Ethernet / RS 485
interface converter
• CALOMAT 6
Accessories for the network
• CALOMAT 62
• FIDAMAT 6 For cables, connectors, repeaters etc., see Catalog IK PI or
CA 01 on the Mall under SIMATIC NET communications sys-
• ULTRAMAT 23 tems/PROFIBUS/network components.
SIPROM GA allows access to device parameters, right up to the Networking with SIPROM GA via converter
configuration of devices. All analyzer functions (except factory
default functions) can be remote-controlled and monitored in this Up to 12 analyzers with max. four components each can be net-
manner. SIPROM GA is therefore an ideal servicing and mainte- worked.
nance tool for Siemens gas analyzers. The functional principle is shown in the following illustration.
In addition to remote control of all operator functions,
SIPROM GA offers complete access to all diagnostics data.
SIPROM GA therefore permits preventive maintenance as well
as fast responses when maintenance becomes necessary or
when the production sequence is changed. up to 12 analyzers
SIPROM GA ensures: 5
• High operational reliability
• High availability
• Central, comprehensive information
• Fast response time
• Flexibility
• Economical system integration
In addition to output of TAG No., components, current measured
values, comprehensive diagnostics information (status) and pa-
rameter settings on the analyzer display, SIPROM GA also offers
the following features: RS 485/RS 232
• Bargraph display converter
• Recorder display of one or more measured values with printer
output Typical design of an RS 485 network with SIPROM GA
• Calibration functions (adjustment of all setpoints for calibra- The gas analyzers can be installed at distances up to 500 m.
tion, remote calibration) One network can be connected to each COM port.
• Saving of all device data
• Remote control of all device functions
• Remote calibration
• Online help
• Downloading of new device firmware
• Cyclic saving of measured values on hard disk
• Writing user data to the device’s EEPROM, or downloading
data from it.
Access to the analyzers using SIPROM GA is carried out either:
• Directly from the PC over an RS 485 interface or
• Over an Ethernet gateway
General information
Communication
Continuous gas analysis
Networking with SIPROM GA via Ethernet COM port, and thus the possibility for monitoring and operating
several widely distributed or separately installed analyzers/sys-
When networking with Ethernet, there are no limitations for the tems from one station.
distance between PC and gateway. In addition, communication
over Ethernet permits connection of several gateways to one
up to 12 analyzers
Ethernet Gateway
Ethernet Gateway
General information
Communication
Continuous gas analysis
PROFIBUS are PROFIBUS-compatible when using an optional plug-in card
(retrofitting also possible) and therefore comply with the "Device
The usual transmission of measured values and fault messages profile for analyzers" defined as binding by PI (PROFIBUS Inter-
via analog and binary outputs requires complex cabling. On the national).
other hand, when using PROFIBUS DP and PROFIBUS PA, one
single two-wire conductor is sufficient for digital transmission Customer benefits include an enormous savings potential in all
e.g. of all measured values (also from several channels), status plant areas, covering configuration and commissioning, opera-
information or diagnostics functions for preventive maintenance. tion and maintenance, up to subsequent plant expansions.
The PROFIBUS DP version with its high transmission rate for rel- Operation of the gas analyzers from a control system or a sepa-
atively small data quantities per device is widely used in produc- rate PC is possible using the SIMATIC PDM (Process Device
tion automation, whereas PROFIBUS PA takes into account the Manager); this is software which executes under Windows and
features important for process engineering, e.g. large data which can also be integrated into the SIMATIC PCS 7 process
quantities and use in hazardous areas. control system. This permits a clear presentation for integration
of the analyzers in the system as well as for the complex param-
The limited dynamic performance of 4 to 20 mA mA signals can eter structure of the analyzers.
be replaced, the laborious configuring of measuring ranges can
be omitted. By using simulated measured values without media, Direct connection of the analyzers to a control system is also
increased safety can be provided for the plant configuration, possible without PDM, e.g. using STEP7, but this necessitates
and configuration errors can be avoided. Parameter sets can be additional programming and offers less user friendliness. In
generated offline (from your desk) and subsequently down- most cases, this direct connection is therefore only applicable if
loaded and saved in the device. Local operations can thus be acyclic (device operation) data are not used.
reduced to a minimum.
A differentiation is made between cyclic and acyclic services.
The Siemens gas analyzers Cyclic services are used to transmit time-critical data such as
• OXYMAT 6/61 measured values and statuses. Acyclic services permit scan-
ning or modification of device parameters during operation.
• OXYMAT 64
• ULTRAMAT 23 Both graphic displays and values can be output on a PC. Signal-
ing of maintenance, fault and diagnostics information is also cy-
• ULTRAMAT 6 clic. These data are displayed in plain text when using
• CALOMAT 6 SIMATIC PDM.
• CALOMAT 62 The binary outputs can also be switched using cyclic services,
• FIDAMAT 6 thus also permitting triggering of relays over PROFIBUS (e.g. for
measuring point switchover, calibration etc.).
5
3URFHVVFRQWUROV\VWHP
6
'33$FRXSOHU '33$OLQN
*DVDQDO\]HUV
*DVDQDO\]HU
*DVDQDO\]HU
General information
Communication
Continuous gas analysis
The following acyclic device parameters and configurations Generic communications interface
can be used in PROFIBUS DP and PROFIBUS PA by means of (only OXYMAT 6, ULTRAMAT 6 and ULTRAMAT/OXYMAT 6)
SIMATIC PDM:
User benefits are offered thanks to numerous functions which
• Factory data are mainly required in the automotive industry, for example to
• Diagnostics values carry out repeated linearization. In contrast to PROFIBUS and
• Logbook ELAN, communication is only possible between one device and
one PC, and takes place according to the master/slave princi-
• Display measuring ranges ple. The device only transmits data when requested by a com-
• Zero calibration mand telegram, where only one command can be processed
• Sensitivity calibration and replied to at a time.
• Setpoints for zero/sensitivity The generic communications menu can be called using
Function88, and the parameters adjusted.
• Total/single calibration and AUTOCAL
• Select measuring ranges Continuous gas analysis/in-situ
• Define measuring ranges LDS 6 can send and receive data over an Ethernet connection
• Electric time constants together with the LDScom software. This installation and service
tool is able to check and adapt device status and calibration pa-
• On/off functions rameters from a remote location. If necessary, even a complete
• Chopper frequency system check can be carried out over the remote connection. If
• Magnetic field frequency servicing is necessary, the required information can be sent to
the Siemens service engineer by modem, and he can then carry
• Date/time out the appropriate measures from the remote location.
• Measuring point switchover
This facility for remote maintenance and diagnostics is imple-
• Logbook settings mented using a standard LAN modem.
• Relay assignment
• Binary inputs
• Reset
• Save/load data
• Suppression of short noise signals Public telephone network
• Calibration tolerances Modem
Ethernet
• Switch valves
• PROFIBUS configuration LDS 6
General information
Communication
Gas analysis library for SIMATIC PCS 7
■ Overview ■ Function
Driver blocks
PCS 7 Add-on fit for SIMATIC PCS 7 V7 The gas analyzers are integrated into the hardware configuration
of the SIMATIC PCS 7 process control system using their GSD
files. Parameterization of the driver blocks is subsequently car-
ried out corresponding to the device configuration. The driver
blocks provide the following functions:
• Reading of analyzer values
• Starting of autocalibration
• Evaluation of device-specific diagnostics
• Standard diagnostics
• Alarms for analyzer values (alarm limits adjustable on the
block)
• Simulation
Symbols and faceplates
The symbols are automatically created and connected using the
wizard "Create block symbols". The faceplates can be displayed
in various views:
• Standard
• Maintenance
• Configuration
• Limits
• Trend
• Alarm
■ More information
The driver blocks from the gas analysis library permit integration Please contact your Siemens sales partner for further informa-
of the following gas analyzers into the SIMATIC PCS 7 process tion and for ordering.
control system over PROFIBUS DP:
• ULTRAMAT 6 and ULTRAMAT 23
• CALOMAT 5
• OXYMAT
The driver blocks permit access to the measured values and to
the calibration functions of these devices. They can also be used
to evaluate and display diagnostics information, and to trigger
alarms if necessary.
Note:
The gas analysis library can be used together with
SIMATIC PCS 7 V6 and V7.
General information
Communication
Process gas chromatography
■ Overview
The MAXUM edition II and MicroSAM gas chromatographs can Memory division
transfer measured results and status information to process con-
trol systems, operator panels or printers during operation. To ensure that the meaning of the registers is known to each net-
work station, this must be defined in the configuration. The re-
Interfaces sults of each component in each sample must be written into de-
fined positions in the PCS memory. These address declarations
Chromatograph, operator panel, printer and control system use depend on the number of chromatographs, samples and com-
special electronic interfaces: ponents. The same applies to status, sample sequence and
• Electrical connection sample release. Standard addresses are also defined in these
The device interfaces are connected by electric cables. cases.
The electrical properties of the interfaces are standardized.
OPC server (OLE for Process Control)
• Control of communication and language
Rules must be observed to control the communication. It must OPC is a vendor-independent software interface. It allows stan-
be clearly defined in networks who is the "sender" and who is dardized access from Windows applications to chromatograph
the "receiver" of the data. Both communication partners must data. OPC corresponds to a typical client/server architecture.
use the same protocol. OPC allows a universal connection between any Windows appli-
MODBUS cation which supports an OPC client interface and the MAXUM
edition II / MicroSam.
MODBUS is a rule for controlling data transfer between two com-
puter systems - a transmission protocol. MODBUS is the "de The OPC server is usually installed on a separate PC.
facto" industry standard for connecting measuring and control OPC is a modern alternative to MODBUS. MAXUM edition II and
devices to process control systems (PCS). Most process control MicroSAM do not require an additional interface, they use the
systems can be equipped with serial interfaces and MODBUS. existing Ethernet connection (TCP/IP).
Using the MODBUS coupling, information can be sent interfer- OPC standardizes the access to measured values, status func-
ence-proof via just one data line. Information can be read from tions, control functions and analytical data in a manner similar to
process gas chromatographs (PGC), and certain functions of MODBUS.
the PGC can also be parameterized.
Advantages with OPC applications:
Advantages:
• Reduced maintenance costs
• Information on the PGC status during operation
• Simple GUI for configuration
• Supply of protected data in numerical form without falsification
by interfering pulses • Reduced system integration costs
• Reduced cabling overhead • Reduced test costs
• Reduced maintenance costs
The MODBUS coupling can:
5 • Transmit measured values
• Transmit status information
• Output information on the current analysis
• Trigger control functions
The MODBUS uses a master/slave transmission procedure.
The control system is always the master, the process gas chro-
matograph is the slave.
The representation of data in the message frames is based on
the compact RTU format.
23&FOLHQW 23&VHUYHU
23&FOLHQW
3&66LHPHQV3&6
OPC server
General information
Communication
Process gas chromatography
Hardware components Software
NAU - Network Access Unit Modern chromatographs are controlled by microprocessors.
We differentiate between software in the device and software on
An NAU expands and supplements a GC network, and has three a PC operator panel.
fundamental functions:
• Enclosure for 7 additional I/O plug-in cards Software in the chromatograph
• Connection of serial ASCII printers and external host PCs The chromatograph can carry out analyses independently, with-
(control system) out an operator panel being connected. It then requires its own
• Central operation of a GC network from one point control software and local operating software (HMI).
The Network Access Unit (NAU) is an input/output station for the Software in the operator panel (PC)
Siemens process chromatographs. It can be used to centrally Siemens gas chromatographs can be operated over Ethernet
call, process and pass on data. It is used if it is not possible to and a PC, by using the built-in control panel (HMI), or with a Net-
connect the electronics close to the analyzer, if the number of Mi- work Extension Unit (NAU).
croSam inputs/outputs is insufficient, or if installation in a central
control room is required. This significantly reduces the required Workstation software
wiring to the control room. The most important programs this contains are the MAXUM Sys-
The NAU can also be used as a central control unit for function tem Manager, the MAXUM EZChrom and the HMI-Emulation. In
testing, data output and parameterization of the MicroSam. It addition, it contains useful MAXUM utilities and loadable exten-
permits access to the MicroSam to which it is connected, as well sions such as:
as to all other Siemens gas chromatographs and further NAUs of MaxBasic
the system which are networked over the system bus.
For modification of MaxBasic programs in the gas chromato-
The NAU is connected to the Ethernet or DataNet and has a total graphs or the NAU.
of 7 slots to accommodate a wide range of electronics cards.
These comprise cards for analog and digital signal processing MAXUM OPC Server
as well as interfaces for host computers and process control For coupling of the MAXUM e.g. to control systems.
systems. An NAU can be expanded by a further 10 slots using a
CAN Extension Unit. Simulated Distillation
A total of 7 different electronics cards are available: For import/export of methods for simulated distillation.
MAXUM System Tools
• Input/output module 8 analog outputs For data logging, for firmware updating, or for operation of dis-
• Input/output module 4 digital outputs, continued OptiCHROMs (APC 8.0).
4 digital inputs Different levels of operation
• Input/output module 2 digital outputs,
5
2 digital inputs, Operation of the PC is in three levels:
2 analog outputs, • System Manager - network monitoring and configuration of the
2 analog inputs chromatograph
• Communication module 10 Base FO Ethernet • EZChrom - method development and control of analysis
(fiber-optic coupling)
• MMI emulation - operator control and monitoring
• Communication module DataNET Copper
(redundant system bus) System Manager:
Configuration of database and applications
• Communication module DataNET Fiber Optic
• Communication module Advanced Data Highway
The System Manager provides the connection to the chromato-
(OptiCHROMe Advance graph as well as an overview of the network.
coupling) It is additionally used for configuration and high-level monitoring
CEU - CAN Extension Unit (only MAXUM edition II) of the chromatograph, and additionally branches to the MMI em-
ulation, EZ Chrom and Basic editor.
• Increases the I/O capacity of the GC or NAU
• 10 additional I/O plug-in cards The System Manager almost exclusively outputs static displays,
i.e. it fetches a table from the chromatograph’s database, and
• Has its own power supply saves it again there later. Only results and alarms are displayed
• Also for zone 1 dynamically.
ANG - Advance Network Gateway The System Manager presents the hardware in tables, e.g. the
system table contains all hardware components of the chromato-
Connects OptiCHROMs to the Ethernet network. graph: detectors, valves, ovens, digital outputs, etc.
DNH - DataNET Hub In addition, the System Manager can:
Communications router completely redundant in the network: • Save databases of a chromatograph as a file on the PC, or
has 2 own TCP/IP addresses, dual electronics and power load them from the PC into the chromatograph.
supply. • Upgrade the chromatograph software.
ANCB - Advance Network Communication Board • Call EZChrom, MMI emulation, Datalogger or the MaxBasic
Converts the communications protocols in the device editor.
Two versions:
• MAXUM directly to DataNET
• MAXUM directly to OptiCHROM data highway
General information
Communication
Process gas chromatography
EZChrom: APC 8.0
Generate methods and sample sequences
This is an interface to the OptiCHROM Advance gas chromato-
The EZChrom software is installed on the PC and is also in- graphs. It is started from the MAXUM System Manager. It permits
cluded in the operator software in the chromatograph, e.g. it operation of older types of chromatograph via a PCI card.
integrates the detector signals there, calculates the results, or
switches time-controlled events. The following can be executed with APC 8.0:
• Service panel emulation on the PC
EZChrom on the PC is responsible for the following tasks:
• Data logging
• Generate or modify methods
• Viewing of chromatograms
• Carry out re-integration
• Editing of tables in OptiCHROM.
• Calibrate a method
• Display and print saved and real-time chromatograms GC-Tools operating software
• Archive chromatograms GC-Tools is the Windows-based operating software for discon-
tinued Siemens gas chromatographs of Series 202 and 302. This
• Generate and modify sample flow sequences software expands the BEDI operating software, which is based
• View analysis clock on MS-DOS.
• Switch the chromatograph to Run or Hold. The Network Explorer shows all information at the device level,
MMI emulation: Operator control and monitoring e.g.:
This is identical to operation on the built-in control panel of a • Chromatogram display
MAXUM or an NAU. It is used for operator control and monitor- • Manual control of all parameters
ing. For example, it is possible to display results, switch valves • Drivers for the four serial interfaces of the chromatograph
or modify temperatures. However, there are only minimum pos-
sibilities for editing the configuration and tables. The MMI is al-
ways a dynamic display.
General information
Operator functions of Series 6
Configuration
62
70
Switch external pressures (FIDAMAT 6 "without pump" only)
Analog output
X
X
X
X
—
— —
X
5
(Code 2) 71 Relay assignment X X — X
72 Binary inputs X X — X
73 ELAN configuration X X — —
74 Reset X X — X
75 Save, load data X X — X
76 Suppression of short noise signals X X — X
77 Measured value memory (analog output) X X — —
78 Calibration tolerances X X — X
79 Change codes X X — —
80 Unit test X X — —
81 Language selection X X — —
82 Pressure correction (ULTRAMAT 6, OXYMAT 6, OXYMAT 64 X X — —
and CALOMAT 62 only)
83 Correction of cross-interference X X — —
84 Phase calibration (ULTRAMAT 6 and OXYMAT 6 only) X — — —
85 Switch valves X — — —
86 Linear temperature compensation X X — —
87 Fault on/off X — — —
88 AK configuration (ULTRAMAT 6 and OXYMAT 6 only) X — — —
89 Sample chamber heating (ULTRAMAT 6, OXYMAT 6 and X X — —
CALOMAT 62 only)
90 PROFIBUS configuration X X X X
91 Startup state (FIDAMAT 6 only) X X — —
92 Pressure values (FIDAMAT 6 only) X X — —
93 Units (FIDAMAT 6 only) X — — —
General information
FAT & factory certificates
1)
Can also be ordered following delivery
2)
H2O and 2 other gases
General information
Ex versions
Continuous gas analysis, extractive
■ Overview
Use of Series 6 in hazardous areas • Pressurized enclosure with continuous purging
The principle of this type of protection is based on having con-
Dependent on the application, the measuring equipment tinuous purging of the EEx p enclosure after the pre-purge. It
can include the following parts: prevents ingress of the surrounding atmosphere and ensures
• Analyzer that, for example, sample gas released through leaks is
• EEx p safety equipment (purging unit) thinned to the extent that a combustible mixture cannot be cre-
ated. The volume flow of the protective gas is fixed at 1 l/min
• Flame arrestors and exceeds the maximum release volume by a factor of more
• Ex i isolation amplifier than 100.
• Isolating relay Protective gas flows continuously through the enclosure with a
volume flow of at least 1 l/min; in addition, the flow ensures that
Gas analyzers the enclosure pressure is increased to at least 50 Pa higher
Suitability-tested field analyzers of Series 6 must be used to than the surrounding pressure.
measure gases in hazardous areas. The max. permissible purging gas pressure is 25 hPa.
The max. permissible sample gas pressure is equivalent to the
The Series 6 analyzers are approved in accordance with Ex type permissible analyzer sample gas pressure.
of protection "Pressurized enclosure EEx p" for Zone 1 and Zone Test certification TÜV 01 ATEX 1708 X
2. In addition, these analyzers must be connected to monitoring Device identification: II 2 G EEx p [ia] ia IIC T4.
equipment which must also be suitability-tested.
The fundamental safety requirements of both versions are satis-
Exception: a pressurized enclosure is not required in zone 2 for fied by compliance with the European standards
the measurement of gases whose composition always remains EN 50014:1997, EN 50016:1995, EN 50020:1994 and
below the lower explosive limit (LEL); in this case, it is sufficient EN 954:1996.
for the field housing to be gas fume-proof (type of protection
EEx n R). The purging gas is monitored using EEx p monitoring equip-
ment: This is a stand-alone unit which is connected electrically
Following pre-purging of 5 minutes, the monitoring equipment and pneumatically to the analyzer. Explosion protection is only
ensures that no gas fumes can enter the enclosure, and accu- provided when both devices are combined (analyzer and purg-
mulation of the sample gas in the enclosure is prevented. The ing unit, and possibly further measures) (see below).
volume flow during the pre-purging phase is > 50 l/min. The pro-
tective gas is usually fed into the analyzer enclosure from a sup- Category ATEX II 3G (Ex zone 2)
ply network via the monitoring equipment. The principle of the type of protection "Pressurized enclosure for
Category ATEX II 2G (Ex zone 1) devices of Category 3" is based on preventing the ingress of any
hazardous atmosphere into the gas analyzer.
Two versions of pressurized enclosure EEx p complying with the
directive 94/9/EC are available for use in zone 1: Two versions complying with Directive 94/9/EC are available for
use in Zone 2. In both cases, the standard devices of Series 6
• Pressurized enclosure with compensation of losses resulting
from leaks
(field version, not Ex) can be used. 5
The principle of this type of protection is based on prevention • Explosion protection due to gas-fumes-proof enclosure
of ingress of the surrounding atmosphere or of the sample gas The enclosure of the Series 6 gas analyzers (standard, field
into the enclosure of the electrical equipment. version) is sealed sufficiently to prevent gas fumes from pen-
Only that volume of protective gas is fed into the enclosure etrating. With this type of protection, only sample gases may
that is required to maintain an overpressure of at least 50 Pa be fed in which are below the LEL.
compared to the sample gas pressure and atmospheric pres- Test certificate: TÜV 01 ATEX 1686 X
sure. The maximum purging gas pressure is 165 hPa; this re- Device identification: II 3 G EEx n R II T6
sults in a maximum permissible sample gas pressure of It is not necessary to install a purging unit here.
164 hPa; • Pressurized enclosure with continuous purging
If the sample gas is combustible or occasionally flammable, Protective gas continuously flows through the enclosure with a
the analyzer enclosure must be additionally purged with inert volume flow of at least 1 l/min; furthermore, the flow results in
gas (e.g. nitrogen). In these cases, you must additionally en- an overpressure in the enclosure of at least 50 Pa compared
sure that the internal enclosure pressure is at least 5 mbar to atmospheric pressure.
higher than the fail-safe-regulated sample gas pressure. The max. permissible purging gas pressure is 25 hPa. The
If the pressure control of the sample gas is not fail-safe max. permissible sample gas pressure is equivalent to the
(= "double fault safety"), but only operationally safe (="single permissible analyzer sample gas pressure.
fault safety"), a differential pressure switch of the EEx p safety Test certification TÜV 01 ATEX 1697 X
equipment must be used to signal if the sample gas pressure Device identification: II 2/3 G EEx n P II T4
exceeds the purging gas pressure. This measure trips a safety The purging gas is monitored using E Ex p monitoring equip-
shutdown. ment. This is a stand-alone unit which is connected electrically
With occasionally flammable sample gas mixtures, flame ar- and pneumatically to the analyzer. Explosion protection is only
restors must be additionally mounted externally at the sample provided when these two units (analyzer and purging unit) are
gas inlet and outlet. combined. (see below, purging unit)
Both the differential pressure switch and the flame arrestors
come into contact with the sample gas and must therefore be The fundamental safety requirements of both versions are satis-
made of corrosion-proof material, if applicable. fied by compliance with the European standards
Test certification: PTB 00 ATEX 2022 X EN 50014:1997, EN 50016:1995, EN 50020:1994 and
Device identification: II 2 G Eex p [ia] ia IIC T4 EN 954:1996.
The EEx p monitoring equipment is a stand-alone unit which is
connected electrically and pneumatically to the analyzer. Explo-
sion protection is only provided when these two units are com-
bined.
General information
Ex versions
Continuous gas analysis, extractive
Category ATEX II 3D (Ex zone 22) The following additional safety mechanisms are recommended
for continuous gas analyzers for measuring explosive gases (in-
Ex zone 22 concerns the so-called dust protection. This is the ternal explosion protection). These requirements are based on
European successor to the previous German zone 11. Zone 22 the European ATEX approvals for analyzers, but can also be
concerns the area in which during normal operation it is not ex- used as directives in the USA since no other specific definition
pected that potentially explosive atmospheres occur in the form exists there.
of a cloud of flammable dust in the air. Should such a cloud oc-
cur, however, then only briefly. Purging requirements
Considering the more stringent conditions for zone assignment, The continuous analyzers from Siemens with approvals for
it can be expected that there will be increased demand for dust- Class I, Div. 2 never require purging in a hazardous area in ac-
protected analyzers. cordance with Class I, Div. 2 / Zone 2 under the aspect of area
The field versions of CALOMAT 6, OXYMAT 6 and ULTRAMAT 6 classification. All electronic and mechanical components are
can be used in this zone according to the conformity statement classified as “non-explosive” and can be used in environments
TÜV 03 ATEX 2278 X. in accordance with Class I, Div. 2 / Zone 2. However, purging
may be necessary for a specific application, depending on the
They are assigned the Ex identification II 3 D IP65 T60 °C or type of sample gas and the respective analyzer model in order
T65 °C or T85 °C or T135 °C. to comply with the NEC and NFPA standards and to guarantee
However, this only concerns the so-called external explosion maximum possible safety as well as protection of the system.
protection. With respect to the measurement of flammable NFPA 496 requirements for continuous gas analyzers and sys-
gases, the additional measures applicable to gas explosion pro- tems from Siemens
tection apply in addition, such as flame inhibitors. These sepa-
rate certificates apply here. The NFPA 496 "Standard for Purged and Pressurized Enclosures
for Electrical Equipment" describes in great detail and clarity the
FM/CSA Class I Div 2 requirements for purging and for the pressurized enclosure for
The field versions of the standard analysis units can be used. electric systems depending on 1) the external hazardous area
Explosion protection is only provided when combined with the classification, 2) the classification/grading of the system, 3) the
suitable equipment. type of gas in the gas path, and 4) the expected discharge of
gas (none/limited/unlimited).
Definitions
It is assumed for the internal gas path of a continuous gas ana-
Non-flammable Gas or gas compositions with concentrations below the lyzer that it exhibits only low losses under normal conditions and
gas lower explosion limit (LEL). Non-explosive, even in con- uncontrolled losses in the case of a mechanical failure (abnor-
tact with air. mal conditions).
Example: CH4 < 4.4 %; H2 < 4 %; C2H2 < 2.3 %
When connecting gases with flammable components (> LEL) to
Flammable gas Gas or gas composition with concentrations above the the gas path of an analyzer with a hermetically sealed enclosure,
LEL. Explosive, but additionally requires air and ignition the flammable component can become enriched in the inside of
energy. the analyzer enclosure – even under normal conditions – beyond
5 Explosive gas
Example: CH4 > 4.4 %; H2 > 4 %; C2H2 > 2.3 %
General information
Ex versions
Continuous gas analysis, extractive
In the case of analyzers designed for Class I, Div. 2 / Zone 2 it is Purging rate / applied pressure
assumed that they cannot ignite an explosive gas mixture under
normal conditions (single fault safety), and these analyzers can Purging with air: The air throughput for purging an analyzer for
therefore be used in an occasionally explosive atmosphere in field installation must be sufficient such that the concentration of
the environment or within the enclosure in accordance with the flammable gases is less than 25 % of the LEL (see NFPA 496,
definition of Class I, Div. 2 / Zone 2. However, a frequent or per- Section 8.3). An air throughput of 1 l/min is recommended.
manent explosive atmosphere must be avoided since a simulta- Purging with inert gas: The inert gas throughput for purging an
neous fault occurring on the electrical components of the ana- analyzer for field installation must be sufficient such that the ox-
lyzer could constitute an ignition source. ygen level is less than 5 % of the volume or, at a maximum, less
When purging a continuous gas analyzer or when purging/vent- than 50 % of the oxygen required to form an explosive mixture
ing a continuous gas analyzer system suitable for Class I, Div. 2 (see NFPA 496, Section 8.3). An inert gas throughput of 1 l/min
/ Zone 2 with instrument air or ambient air, and if failure of the is recommended.
safety vessel is not obvious, a leak detector (measurement in % Applied pressure with inert gas: The purging and holding pres-
of LEL) or similar equipment should be used in order to detect sure applied to an analyzer for field installation must be sufficient
the unlimited discharge under abnormal conditions and to avoid such that the oxygen level is less than 5 % of the volume or, at a
a frequent or permanent explosive atmosphere inside the ana- maximum, less than 50 % of the oxygen required to form an ex-
lyzer or in its environment. The leak detector must be fitted at a plosive mixture (see NFPA 496, Section 8.3). A pressure of 25 Pa
location where the escaping sample gas can be measured be- (0.1 inch water column) in accordance with NFPA 496 is recom-
fore becoming too greatly diluted. The alarm limit of the leak de- mended. It should be taken into consideration when applying a
tector must be set to a level which enables detection of a dan- pressure to an analyzer, that instead of continuous purging,
gerous state with consideration of the fact that the discharged flammable gas can collect within the analyzer if the sample gas
sample gas has most probably already been diluted before it pressure is higher than the purging pressure. It is recommend-
reaches the sensor. able to appropriately adapt the purging pressure within the per-
Further important information missible pressure range of the field device enclosure.
Gas paths material Exceptions: Inert gas should not be used as the purging gas for
certain applications. This particularly applies to safety-related
It is strongly recommended that you use gas paths made of measurements of oxygen (LEL proof) where the sample gas has
metal for applications with flammable gases since such gas a slight overpressure and the inert gas used for purging could
paths offer the greatest safety. This particularly applies to ana- dilute the sample under abnormal conditions. Such applications
lyzers or systems which are purged with instrument air or ambi- require individual assessment of the purging equipment re-
ent air since an explosive atmosphere can be produced under quired and the mode of operation.
abnormal conditions. This immediate danger does not exist in
the case of analyzers or systems purged with inert gas. Integrated systems and analyzer containers: Purging or the ap-
plication of pressure to continuous gas analyzer systems must
It should be mentioned that, with an integrated system, all parts be designed such that the requirements of NFPA 496 are com-
containing flammable gas (pumps, gas coolers, filters etc.) must plied with.
be assessed in the same manner.
5
Leak detector
Purging of left-hand analyzer side (electronics side) of
continuous gas analyzers for field installation When purging a continuous gas analyzer or when purging/vent-
ing a continuous gas analyzer system suitable for Class I, Div. 2
Since the left electronics side and the right measurement side of / Zone 2 with instrument air or ambient air, and if failure of the
continuous gas analyzers are separated gas-tight from each safety vessel is not obvious, a leak detector (measurement in %
other, it is unnecessary to purge the electronics side in most of LEL) or similar equipment should be used in order to detect
cases – purging of the (right-hand) measurement side is suffi- unlimited discharges under abnormal conditions and to avoid a
cient. frequent or permanent explosive atmosphere inside the analyzer
or in its environment. The leak detector must be fitted at a loca-
However, if doubt exists that flammable gas could penetrate the tion where the escaping sample gas can be measured before
left-hand electronics side and become enriched there, it is ad- becoming too greatly diluted. The alarm limit of the leak detector
visable to purge both sides. must be set to a level which enables detection of a dangerous
Further reasons for purging analyzers state with consideration of the fact that the discharged sample
• Corrosive sample gases: Purging with air or inert gas is nec- gas has most probably already been diluted before it reaches
essary to prevent the enrichment of corrosive gas inside the the sensor.
analyzer, whereby operators or servicing personnel could be
injured or the analyzer unit could be damaged. The dis-
charged purging gas should be released at a non-critical
point (collective vent etc.)
• Toxic gases: Purging with air or inert gas is necessary to pre-
vent the enrichment of toxic gas inside the analyzer, whereby
operators or servicing personnel could be injured. The dis-
charged purging gas should be released at a non-critical
point (collective vent etc.). Further information can be found in
the OSHA directives for handling toxic materials.
General information
Ex versions
Continuous gas analysis, extractive
■ Application
Differentiation of cases: Ex zones/danger through flammable sample gas
Gas type Sample gas non-flammable Sample gas is flammable Sample gas is flammable
below the lower explosive and/or is rarely, and then and/or is occasionally
limit (LEL) only briefly, above the LEL above the LEL
Zone
Category ATEX II 1G Individual acceptance test Individual acceptance test Individual acceptance test
(zone 0) (on request) (on request) (on request)
Category ATEX II 2G Analyzer Ex analyzer EEx p Ex analyzer EEx p Ex analyzer EEx p
(zone 1) (certificate ATEX 2022X) (certificate ATEX 2022X) (certificate ATEX 2022X)
Operating mode "Leakage
compensation"
Gas path Pipe gas path Pipe gas path Pipe gas path
Flame arrester — — Flame arrester in sample gas
inlet and outlet
Monitoring EEx p control device EEx p control device sample EEx p control device sample
(certificate ATEX E 082) gas pressure < 165 hPa, fail- gas pressure < 165 hPa, fail-
safe (certificate ATEX E 082) safe (certificate ATEX E 082)
Pressure switch — Differential pressure switch Differential pressure switch
(when sample gas pressure is (when sample gas pressure is
not controlled fail-safely) not controlled fail-safely)
Category ATEX II 2G Analyzer Ex analyzer EEx p Ex analyzer EEx p Ex analyzer EEx p
(zone 1) (certificate ATEX 1708X) (certificate ATEX 1708X) (certificate ATEX 1708X)
Operating mode
"Continuous purging"
Gas path Pipe gas path Pipe gas path Pipe gas path
Flame arrester — — Flame arrester in sample gas
inlet and outlet
Monitoring EEx p control device (certifi- EEx p control device (certifi- EEx p control device (certifi-
cate DMT 99 ATEX E 082) cate DMT 99 ATEX E 082) cate DMT 99 ATEX E 082)
Pressure switch — — —
5
Category ATEX II 3G Analyzer Standard analyzer in field Standard analyzer in field Standard analyzer in field
(zone 2) housing (addition E11: housing (addition E12: housing (addition E12:
certificate ATEX 1686X) certificate ATEX 1697X) certificate ATEX 1697X)
Gas path Pipe or hose gas path Pipe gas path Pipe gas path
Flame arrester — — Flame arrester in sample gas
inlet and outlet
Monitoring — EEx p control device (certifi- EEx p control device (certifi-
cate DMT 99 ATEX E 082) cate DMT 99 ATEX E 082)
Non-hazardous zone Analyzer Analyzer as rack unit or in Analyzer as rack unit or in Analyzer as rack unit or in
field housing field housing field housing
Gas path Pipe or hose gas path Pipe gas path, recommended Pipe gas path, recommended
Enclosure purging with inert Enclosure purging with inert
gas (N2) recommended gas (N2) recommended
Flame arrester — — Flame arrester in sample gas
inlet and outlet
Monitoring — — Simplified monitoring of
purging recommended
General information
Ex versions
Continuous gas analysis, extractive
Use of OXYMAT 6 in hazardous area and/or for measurement of flammable gases
Article No. Certification Additional unit
(short codes)
Gas Dust Purging Flame Pressure Ex i isolation Ex i isolat-
unit arrestor switch amplifier ing relay
Category Operating mode Ex Ex 7MB8000- 7MB8000- 7MB8000- 7MB8000- 7MB8000-
zone zone
ATEX II 2G Leakage 7MB2011-***0*-2*** X — 2BB 6BA/6BB1) 5AA1) 3AB1) 4AB1)
(zone 1) compensation
7MB2011-***0*-3*** X — 2BA 6BA/6BB1) 5AA1) 3AB1) 4AA1)
Continuous 7MB2011-***0*-6*** X — 2CB 6BA/6BB1) o 3AB1) 4AB1)
purging
7MB2011-***0*-7*** X — 2CA 6BA/6BB1) o 3AB1) 4AA1)
ATEX II 3G Flammable gases 7MB2011-***0*-0*** E12 — 2CB 6BA/6BB1) o o o
(zone 2)
7MB2011-***0*-1*** E12 — 2CA 6BA/6BB1) o o o
7MB2011-***0*-0*** E42 — 6BA/6BB1) o o o
7MB2011-***0*-1*** E42 — 6BA/6BB1) o o o
Non-flammable 7MB2011-***0*-0*** E11 — o o o o o
gases
7MB2011-***0*-1*** E11 — o o o o o
7MB2011-***0*-0*** E41 — o o o o
7MB2011-***0*-1*** E41 — o o o o
Non-haz- Non-hazardous 7MB2011-***0*-0*** E40 — o o o o
ardous gas zone
zone 7MB2011-***0*-1*** E40 — o o o o
7MB2011-***0*-0*** — — o o o o o
7MB2011-***0*-1*** — — o o o o o
7MB2021-****0-**** X — o o o o o
General information
Ex versions
Continuous gas analysis, extractive
Use of ULTRAMAT 6 in hazardous area and/or for measurement of flammable gases
Article No. Certification and Additional unit
short codes
Gas Dust Purging unit Flame Pressure switch Ex i isolation Ex i isolating
arrestor amplifier relay
Category Operating mode 7MB2111- Ex Ex zone 7MB8000- 7MB8000- 7MB8000- 7MB8000- 7MB8000-
7MB2112- zone
ATEX II 2G Leakage *****-2*A* X — 2BB 6BA/6BB1) 5AA1) 3AB1) 4AB1)
(zone 1) compensation
*****-3*A* X — 2BA 6BA/6BB1) 5AA1) 3AB1) 4AA1)
Continuous *****-6*A* X — 2CB 6BA/6BB1) o 3AB1) 4AB1)
purging
*****-7*A* X — 2CA 6BA/6BB1) o 3AB1) 4AA1)
ATEX II 3G Flammable *****-0*A* E42 — 6BA/6BB1) o o o
(zone 2) gases
*****-1*A* E42 — 6BA/6BB1) o o o
*****-0*A* E12 — 2CB o o o o
*****-1*A* E12 — 2CA o o o o
Non-flammable *****-0*A* E41 — o o o o
gases
*****-1*A* E41 — o o o o
*****-0*A* E11 — o o o o o
*****-1*A* E11 — o o o o o
Non-hazard- Non-hazardous *****-0*A* X E40 — o o o o
ous zone gas zone
*****-1*A* X E40 — o o o o
General information
Ex versions
Continuous gas analysis, extractive
Use of CALOMAT 6 in hazardous area and/or for measurement of flammable gases
Article No. Certification Additional unit
Gas Dust Purging unit Flame arrester Pressure Ex i isolation Ex i isolat-
switch amplifier ing relay
Category Operating 7MB8000- 7MB8000- 7MB8000- 7MB8000- 7MB8000-
mode
ATEX II 2G Leakage 7MB2511- X — 2BB 6BA/6BB1) 5AA1) 3AB1) 4AB1)
(zone 1) compensation ***0*-0AE*
7MB2511- X — 2BA 6BA/6BB1) 5AA1) 3AB1) 4AA1)
***0*-1AE*
Continuous 7MB2511- X — 2CB 6BA/6BB1) o 3AB1) 4AB1)
purging ***0*-0AF*
7MB2511- X — 2CA 6BA/6BB1) o 3AB1) 4AA1)
***0*-1AF*
ATEX II 3G Flammable 7MB2511- X X — 6BA/6BB1) o o o
(Zone 2) gases ***0*-*AJ*
7MB2511- X — 2CA/2CB 6BA/6BB1) o o o
***0*-*AC*
7MB2521- X — acc. to 6BA/6BB1) o o o
***0*-*AB*2) Certificate
Non-flammable 7MB2511- X X — o o o o
gases ***0*-*AH*
7MB2511- X — o o o o o
***0*-*AB*
7MB2521- X — o o o o o
***0*-*AB*
Non-haz- Non-hazardous 7MB2511- — X — o o o o
ardous gas zone ***0*-*AG*
zone
General information
Ex versions
Continuous gas analysis, extractive
Ex approval
ATEX CLASS I Div 2 ATEX
2G - LC 2G - CP 3G burn. 3G nbrn. FM CSA 3D (dust)
see basic MLFB Z + E12 Z + E11 Z + E20 Z + E20 Z + E4X
except CALOMAT except
CALOMAT
Field device
U6F ATEX 2022 X ATEX 1708 X ATEX 1697 X ATEX 1686 X 3016050 1526657 ATEX 2278 X
U6F-S ATEX 2022 X ATEX 1708 X ATEX 1697 X ATEX 1686 X 3016050 — —
O6F ATEX 2022 X ATEX 1708 X ATEX 1697 X ATEX 1686 X 3016050 1526657 ATEX 2278 X
O6F-S ATEX 2022 X ATEX 1708 X ATEX 1697 X ATEX 1686 X 3016050 — —
C6F ATEX 2022 X ATEX 1708 X ATEX 1697 X ATEX 1697 X 3018862 1526660 ATEX 2278 X
C6F-S ATEX 2022 X ATEX 1708 X ATEX 1697 X ATEX 1697 X 3018862 o —
C62F ATEX 2022 X ATEX 1708 X — — — — —
C62F-S ATEX 2022 X ATEX 1708 X — — — — —
5 C6E
C6E-S
—
—
—
—
ATEX 1873 X
ATEX 1873 X
3018862
3018862
1526660
—
—
—
C62E — — — — — —
C62E-S — — — — — —
O61 — — — — — —
O64 — — — — — —
F6 — — — (SET) — —
U23 — — ATEX 0027 x 3035269 2133209 —
U23 O2p — — ATEX 0027 x 3035269 2133209 —
U23 H2S — — ATEX 0027 x 3035269 2133209 —
CP = Continuous Purging
LC = Leakage compensation
… -S = Special application
burn. = Flammable gases
nbrn. = Non-flammable gases
o = In progress
General information
Ex versions
Continuous gas analysis, extractive - ATEX II 2G control unit
■ Overview
EEx p safety equipment (purging unit) Additional function
The EEx p safety equipment to be connected to the analyzer By connecting additional pressure sensors, the internal pressure
must have at least the following features: of the enclosure is maintained at a pressure higher than that of
• Adjustable pre-purging phase; purging gas flow must be the sample gas by means of a proportional valve. During the pre-
approximately 50 l/min purging phase the purging gas flow is max. 4 100 Nl/h with an
internal enclosure pressure of 50 hPa.
• Limitation of purging gas pressure during the pre-purging
phase: < 165 hPa 4 programmable relay inputs (8 relay contacts) are available to
• "Leakage compensation" or "Continuous purging" separate the data lines.
• Connection for purging gas lines with Ø 10 mm or Ø 3/8" from During the operating phase, the pressure inside the enclosure
and to the analyzer must be maintained at a level at least 50 Pa higher than that of
the surrounding atmosphere. If the internal pressure drops be-
• Pressure after pressure reducer low the defined minimum value, safety equipment must shut
- 0.2 to 0.4 MPa (leakage compensation) down the entire electical supply to the EEx-p enclosure autono-
- 0.2 to 0.3 MPa (continuous purging) mously (including the possible data lines) .
• Max. permissible input pressure 0.6 MPa
Enclosures frequently contain accessories to which flammable
• Relay contacts for all-pole isolation of the analyzer supply volt- gases or sometimes also flammable gas mixtures are fed via a
age separate gas path. This is the case with gas analyzers, for exam-
• Connection option for a key-operated switch and a pressure ple. In this case, it must be ensured that the pressure of the pro-
switch (intrinsically-safe circuits) tective gas is always more than 50 Pa higher than the pressure
• Device version "Leakage compensation": Connection option of the sample gas.
for a pressure switch with intrinsically-safe scan After mounting the control device APEX 2003.SI/B on the EEx-p
The Bartec control unit APEX 2003.SI/B meets the requirements enclosure, and after connecting the mains power and the pro-
for "Pressured enclosure with leakage compensation or continu- tective gas, the control module regulates and monitors the flow
ous purging" in accordance with EN 50016 or ATEX guidelines, of purging gas automatically during the pre-purging phase, and
and can be used as explosion-proof equipment in Zones 1 the internal enclosure pressure during the operating phase.
and 2. If the minimum operating pressure of the enclosure is exceeded
The purging unit ensures that in a closed enclosure, any explo- and if flow through the pressure monitoring module is sufficient,
sive gases will be purged and then a pressure higher than the the pressure sensors forward the sensor module signals to the
surrounding atmosphere will be generated and maintained. control module.
General information
Ex versions
Continuous gas analysis, extractive - ATEX II 2G control unit, leakage compensation
■ Dimensional drawings
5
General information
Ex versions
Continuous gas analysis, extractive - ATEX II 2G control unit, leakage compensation
■ Schematics
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General information
Ex versions
Continuous gas analysis, extractive - ATEX II 2G/3G control unit, continuous purging
At the same time, a higher pressure is maintained inside the Supply voltage 230 V AC (115 V AC) 10 %,
48 … 62 Hz
EEx-p enclosure than in the surrounding atmosphere. If the flow
of purging gas or the internal pressure falls below a determined Power consumption 21 W /230 V
minimum value, the supply voltage to the equipment in the pres- NO contacts K2/3; max. 250 V, 5 A with cos = 1,
surized enclosure is shut down.
K4/K5; supply voltage or floating,
4 programmable relay inputs (8 relay contacts) are available to max. 250 V, 5 A with cos = 1
separate the data lines. Communication RS 485 interface
Temperature switching value 0 … +40 °C
■ Technical specifications (option)
Control unit ATEX II 2G, Explosion protection
continuous purging
Marking EEx e d ib [ia p] IIC T4/T6
Guidelines EC EMC directive 89/336/EEC,
EC low voltage, RL 73/23/EEC, Test certification DMT 99 ATEX E 082
Ex directive 94/9/EC Ambient temperature -20 … +40 °C
Design Explosion-protected enclosure (EEx e)
with viewing window in the cover
Degree of protection IP65
■ Dimensional drawings
5
General information
Ex versions
Continuous gas analysis, extractive - ATEX II 2G/3G control unit, continuous purging
■ Schematics
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PE
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General information
Ex versions
Continuous gas analysis, extractive - Purging unit FM (Class I Div 2)
Reaction upon failure of pressure Opening of switching contact,
and alarm via signal indicator
(red display)
System type MiniPurge complete system
Operating mode Continuous purging
Type of enclosure Reinforced polycarbonate
Enclosure surface RAL 7035 gray with transparent
cover
Pressure supply Dry, oil-free air or inert gas with
regulated pressure of approx.
2000 hPa (30 psi) at inlet of
MiniPurge
Supply connections Pressure via ¼ BSPP connection,
pressure hose at least ½" or
12 mm
MiniPurge, dimensions in mm
■ Schematics
General information
Ex versions
Continuous gas analysis, extractive - Additional units
■ Overview
Installation of Ex isolation modules / Ex i isolation amplifiers Isolating relay (signal outputs with external voltage supply)
7MB8000-4AA/-4AB
The mounting rail in the analyzer has a length of approximately
250 mm, with the number of installable components being If the device has to be opened, it must be isolated at all poles
limited. from the mains cable, the binary inputs, relay outputs, analog in-
puts/ outputs, RS 485 interface cable, and the PROFIBUS PA ca-
The maximum installation height is approximately 95 mm; how- bles (not Ex i). For this purpose, isolating relays must be in-
ever, it is less in the area of the display (88 mm). The width must serted. Intrinsically-safe circuits are excepted from this.
not exceed 80 mm.
An isolating relay must be explosion-proof if it is to be set up in
The add-on devices must be approved for an ambient tempera- an area subject to explosion hazard.
ture of up to 60 °C; this temperature can be reached under ex-
treme marginal conditions. Protective gas
The label of the analyzer shows all types of explosion protection • The fed-in gases are not flammable. Air from an area not sub-
that the device itself and the components can have. ject to explosion hazard can be used as the protective gas
(purging gas).
Installation must always be discussed with the competent ex-
perts. • Flammable gases or gas mixtures that are rarely or only briefly
ignitable are fed in. The enclosure must be flooded with inert
Slots in the analyzer and the purging unit. gas.
Ex i isolation Ex isolating Comment • Gas mixtures that are occasionally ignitable are introduced.
amplifier relay 8S As with b), the enclosure must be flooded with inert gas; in ad-
Analyzers 2 2 Max. 2 dition, the sample gas inlet and outlet must be equipped with
flame arrestors.
Bartec purging 0 1 Max. 1
unit • Explosive gas mixtures that are present in the long term or per-
manently must not be connected!
Ex i isolation amplifier, 7MB8000-3AB
Flame arrestors
The analog inputs and outputs of the analyzers are not intrinsi-
cally safe in the basic version. If the gas mixture to be measured sometimes has an explosive
composition, flame arrestors must be installed in the sample gas
The analog output can be supplemented later with an intrinsi- inlet and, in certain circumstances, also in the sample gas outlet,
cally-safe analog output (explosion protection type EEx ib II C or in addition to the application already described with flammable
EEx ia II C). For this purpose, a suitable commercially available sample gases.
isolating transformer can be mounted on a rail in the device.
The material of the flame arrestors must be resistant to the flow-
Technical data: type sample gas mixture. For this reason, they are available in
5
• Intrinsically-safe analog output two different versions:
• mA isolating transformer without power supply • The detonation protection (Ex designation Ex IIG IIC) is used
to prevent flashover in the case of unstable detonations and
• For installing in the analyzer deflagrations of explosive gas or vapor/air mixtures of explo-
Isolation amplifier, rail mounting sion group IIC.
• Intrinsically-safe output EEx ia IIC • The flame arrestor consists essentially of a detonation-proof
enclosure with gas connections and a ceramic sinter cartridge
• Galvanic isolation built into the housing (max. pore width: 80 µm) to prevent
Technical data flashover.
Input voltage 8.4 V + 0.02 x load x (V/) It may be heated up to 150 °C and subjected to a pressure up to
3 bar (abs.).
Linearity < 0.1 V
Temperature impact < 0.1 %/10 K Technical data
Power supply 8.4 ... -30 V DC from the current Length 83.5 mm
loop Diameter 32 mm
Weight 160 g External thread M 30 x 1.5; 30 mm long
Ambient temperature -20 °C … +60 °C Gas connections G 1/4"
Relative humidity < 95 %, no condensation Material Stainless steel or Hastelloy C
Explosion protection Max. gas operating pressure 3 bar (abs.)
Type of protection II (1) G D [Eex ia] IIC Max. operating temperature 150 °C (200 °C on request)
EC type-examination certificate TÜV 98 ATEX 1338 Explosion group IIC
Safety limits U0 12.6 V
I0 95 mA
General information
Ex versions
Continuous gas analysis, extractive - Additional units
Differential pressure switch: 7MB8000-5AA
There must be a fail-safe guarantee that the sample gas pres-
sure will never exceed 5 hPa under the purging gas pressure.
If this cannot be guaranteed on the plant side, a differential pres-
sure switch must be mounted between the sample gas line and
the purging gas line and connected electrically with the purging
unit.
The differential pressure switch always has contact with the sam-
ple gas.
Technical data
• Differential pressure switch with magnetic spring contact
• Type 821.1
• Materials coming into contact with the sample gas:
Stainless steel, mat. no. 1.4571
• Measuring range: -20 ... +20 hPa
• Trigger point: adjustable
General information
Ex versions
Continuous gas analysis, in-situ - LDS 6
■ Overview
Sensors and cables for applications of the LDS 6 in "Intrinsic safety" is limited to circuits with relatively small capac-
hazardous areas ity. To prevent sparks during closing or opening, the capacitance
and inductance of an intrinsically-safe circuit are also limited de-
Intrinsic safety and intrinsically-safe circuit pending on the maximum current and voltage values. No sparks
Principles or thermal effects which could lead to ignition of an explosive at-
mosphere occur either in normal operation or in the process up-
The physical principle for the degree of protection "Intrinsic set. Therefore intrinsically-safe circuits may also be connected
safety" is that a certain minimum ignition energy is required to ig- or disconnected during operation when live, since the safety is
nite an explosive atmosphere. In an intrinsically-safe circuit, this also guaranteed in the event of a short-circuit or interruption. The
minimum ignition energy is not present in the hazardous area, following figure shows the block diagram for the type of protec-
neither during normal operation nor in the event of an incident. tion "Intrinsic safety".
The intrinsic safety of a circuit is achieved by limiting the current,
voltage, power and temperature. Therefore the type of protection
Limited temperature
rise Ca Ci
U0
Limited
spark
energy
PA
General information
Ex versions
Continuous gas analysis, in-situ - LDS 6
Minimum ignition curves Typical setup of an LDS 6 system in a hazardous area
The "minimum ignition curves" are used to evaluate an intrinsi- LDS 6 is capable of measuring gases in EEx environments, pro-
cally- safe circuit and to determine the maximum capacitance vided all safety-relevant points are particularly observed. The
and inductance values. They are included in the valid intrinsi- central unit of LDS 6 must always be located outside of hazard-
cally-safe standards (EN 50020 or DIN EN 50020 and ous areas.
IEC 60079-11 or EN 60079-11). Minimum ignition curves exist for
resistive, capacitive and inductive circuits. Different minimum ig- Special EEx-type sensors (see explosion protection tag),
nition curves are applied depending on the gas group for which certified according to
an intrinsically-safe circuit is to be designed, and take into ac- • ATEX II 1G Ex ia IIC T4 and
count the minimum ignition energies of the gas groups. • ATEX II 1 D Ex iaD 20 IP65 T135 °C
Associated electrical equipment allow operation inside almost any EEx-classified area.
Associated electrical equipment is a reference to equipment For the intrinsically-safe version, an EEx barrier must be pro-
which contains one or more intrinsically-safe circuits, but in vided between the sensors and central unit. A typical version is
which not all circuits are intrinsically-safe. Associated electrical shown in the following figure for intrinsically safe EEx ia sensors.
equipment usually has an isolating function, i.e. separating in-
trinsically-safe equipment from non-intrinsically-safe equipment
within a signal circuit. Such devices include, for example: safety CD6 Ex
barriers, switch amplifiers, power supply units etc. Transmitter Receiver
Associated electrical equipment is not explosion-proof and must
therefore not be installed in hazardous areas. It only contains in-
trinsically-safe circuits which may be routed into the hazardous
area. Associated electrical equipment is identified by a square
bracket enclosing "EEx" and the symbol for the type of protec-
tion, as well as absence of the temperature class
Hybrid
(e.g. [EEx ia] IIC).
cable
Sensor connecting cable
Cables
DIN/EN 60079-14 (VDE 165, Part 1) must be observed when se-
lecting and routing the cables. Particular attention must be paid Ex zone
to the characteristic values, such as electric strength and mini-
mum cross-section. In the case of intrinsically-safe circuits, the
cable capacitance and inductance must be observed in addi- Ex barrier
tion, and must not exceed the values specified for the intrinsi-
cally-safe or associated equipment used (Co, Lo). The connec-
tion points and cables of intrinsically-safe circuits must be
Hybrid cable
5
identified, e.g. in light blue, and be separated from the other
connection points and cables of non-intrinsically-safe circuits. LDS 6
General information
Ex versions
Continuous gas analysis, in-situ - LDS 6, EEx barrier
The EEx barrier defines the interface between the analyzer cen- • Maximum output voltage 24 V at 170
tral unit and the intrinsically-safe sensor heads and ensures un- • Current limitation 45 mA
der all circumstances that the total electrical energy transferred Max. power consumption 90 mA at 24 V,
via the hybrid cable to the sensors is always less that than (45 mA output) 110 mA at 20 ... 35 V DC
needed to ignite combustible gas mixtures.
Safety description 25 V, 170 , 147 mA,
Um = 250 Vrms or DC
■ Dimensional drawings
250
146
350
General information
Ex versions
Continuous gas analysis, in-situ - SITRANS SL
■ Overview
The SITRANS SL consists of a flameproof transmitter, a flame-
proof receiver, and optionally a specially certified junction box of
increased safety. The complete analytical system is accommo-
dated in the two flameproof enclosures which are connected to-
gether by a cable. A further cable is connected to the receiver,
and serves as the power supply and customer interface. Both
cables have a fixed connection to the flameproof enclosure.
They must be connected in a suitable junction box if applicable.
The receiver also has a local display.
SITRANS SL can be operated by Ex-certified infrared remote
control.
The laser has a radiated power of 0.8 mW. The irradiance is ap-
prox. 10.9 . 10 - 3 mW/mm2. This is below the values permitted in
EN 60079-28.
The SITRANS SL is available with ATEX or FM certificates.
An Ex concept with type of explosion protection "Pressurized en-
closure d" is used for the SITRANS SL. The enclosure used re-
sists an explosion caused by an explosive gas mixture in the an-
alyzer. Ignition of an explosive atmosphere produced outside the
enclosure is therefore reliably prevented.
5 Remote control
ATEX cable
Mounting bracket for gland
junction box
General information
Ex versions
Process gas chromatography
■ Overview
Safety is extremely important during the storage, manufacture, Basic design with MAXUM edition II
processing and transportation of flammable materials, espe-
cially in the chemical and petrochemical industries, and in oil The electronic components are accommodated in a pressurized
and gas production. area. If the overpressure falls below a certain value, a control de-
vice switches off the power supply when a defined threshold is
Gas chromatographs and the sample preparation carried out in reached.
these plants must be designed such that no explosive mixtures
can be ignited when applied. National directives and guidelines The MAXUM edition II is available with certificates according to
as well as international standards regulate the equipment pre- CSA/US, or ATEX certificates according to Cenelec for the EU
requisites. market.
MicroSAM
General information
Tables
Conversion tables
■ Overview
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General information
Tables
Dew point/saturation table
General information
Tables
Dew point/saturation table
Guide values for dead time (sec) per meter of sample gas line
d 4 mm 6 mm 8 mm 10 mm 12 mm 14 mm 16 mm 18 mm 20 mm
Q
30 l/h 1.5 3.4 6 9.4 13.5 18.4 24 30.5 37.6
60 l/h 0.8 1.7 3 4.7 6.8 9.2 12 15.3 18.8
90 l/h 0.5 1.1 2 3.1 4.5 6.1 8 10.2 12.5
120 l/h 0.4 0.9 1.5 2.4 3.4 4.6 6 7.6 9.4
150 l/h 0.3 0.7 1.2 1.9 2.7 3.7 4.8 6.1 7.5
180 l/h 0.3 0.6 1 1.6 2.3 3.1 4 5.1 6.3
210 l/h 0.2 0.5 0.9 1.3 1.9 2.6 3.4 4.3 5.4
240 l/h 0.2 0.5 0.8 1.2 1.7 2.3 3 3.8 4.7
270 l/h 0.2 0.4 0.7 1 1.5 2 2.7 3.4 4.2
300 l/h 0.15 0.34 0.6 0.9 1.4 1.8 2.4 3.1 3.8
General information
Tables
International standards
National standards also exist in most EU member states, and However, extensive harmonization has already been carried out
may be used in these countries in addition to the valid EN stan- in the explosion protection sector, and most standards now also
dards. In the Federal Republic of Germany, these are the DIN exist as "DIN EN ...." versions, which have also been incorpo-
standards and the VDE regulations. rated into the VDE regulations. DIN EN standards are identical to
the corresponding EN standards, were special national features,
e.g. concerning areas of validity etc., are formulated in a national
foreword.
General information
Tables
International standards
EN 60079-10 DIN EN 60079-10, Electrical equipment for potentially explosive gas atmospheres,
VDE 165 Part 101 Part 10: Division of potentially explosive areas
EN 60079-14 DIN EN 60079-14, Electrical equipment for hazardous areas, Part 14: Electrical installations in potentially
VDE 165 Part 1 explosive areas (except underground excavation)
EN 60079-17 DIN EN 60079-17, Electrical equipment for potentially explosive gas atmospheres, Part 17: Testing and main-
VDE 0165 Part 10 tenance of electrical installations in hazardous areas (except underground excavation)
EN 60950 DIN EN 60950, Safety of information technology equipment, including electrical office machines
VDE 0805
Harmonized European standards for explosion protection
T 1 > 450 °C T 2 > 300 °C T 3 > 200 °C T 4 > 135 °C T 5 > 100 °C T 6 > 85 °C
I Methane
II A Acetone Ethyl alcohol Petrol Acetyl aldehyde
Ethane i-amyl acetate Diesel fuel Ethyl ether
Ethyl acetate n-butane Aviation gasoline
Ammonia n-butyl alcohol Fuel oil
Benzene (pure) n-hexane
Acetic acid
Carbon monox-
ide
Methane
Methanol
Propane
Toluene
5 II B Town gas
(Illuminating
Ethylene
gas)
II C Hydrogen Acetylene Carbon disulfide
Classification of gases and vapors into explosion groups and temperature classes
General information
Definitions
■ Overview
Definitions Units of measurement
Calibration gas Vol%
Gas used for adjusting the sensitivity (deflection) of the detected Volume proportion in % of measured component, based on the
gas. It is a gas mixture of known composition (measured compo- sample gas.
nent and suitable residual gas).
ppm (vpm)
Sensitivity
Parts per million, i.e. one proportion of the measured component
Ratio between a change in output variable observed on the mea- per 106 proportions of the sample gas (corresponds to 10-4 %).
suring instrument and the change in input variable required for
this. In gas analysis technology, ppm is usually understood as vol-
ume concentrations. The dimension unit vpm is frequently used
Linearity error of devices with linear characteristics for unequivocal identification:
Deviation of measured characteristic from a linear reference 1 vpm = 1 cm³ / m³
characteristic.
Example: 1 000 vpm = 0.1 vol.% = 1 dm³ / m³
The linearity is an important variable particularly for instruments
which use a measuring effect with nonlinear characteristic and mg/m³
where the measured characteristic is linearized electronically. Mass of measured component in mg referred to 1 m³ of sample
Cross-sensitivity gas at 1 013 hPa and 20 °C.
Measure for the selectivity of a gas analyzer with regard to inter- Example: 1 vpm = 1 cm³ / m³ corresponds to:
fering components. (molecular weight of component / molecular volume of compo-
It is the ratio between the displayed value of the interfering com- nent) (mg / m³)
ponent and the displayed value of the measured component; Weight concentration
both have the same concentration.
Specification of measured values in weight concentrations is not
In the case of analyzers where the total concentration of different common with gas analysis. Weight concentrations can only be
materials is measured (e.g. total hydrocarbon concentration) determined in exceptional cases. The dimension unit mg/m³
and where the individual components are weighted differently in does not mean weight concentration.
the measuring result, these factors are specified in equivalents
of a master component (e.g. CH4 equivalents for the total hydro-
carbon measurement) and not as cross-sensitivity.
Dynamic response
The dynamic response of an analyzer is characterized by its re-
sponse time and dead time. The response time is the time which 5
passes until the output variable remains constantly within de-
fined limits following an abrupt change in the input variable. The
response time is usually understood as the time required to
reach 90 (T90) or 95 % of the expected display.
General information
Notes
Appendix
Pa
Service Engineering
Se
ld
Programs Support
6/5 Applicable practical know-how
are
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Siemens PA 01 · 2015
© Siemens AG 2014
Appendix
Siemens Industry Training
■ Contact
Visit our site on the Internet at:
www.siemens.com/sitrain
or let us advise you personally.
Siemens Industry Training Customer Support Germany:
Phone: +49 911 895-7575
Fax: +49 911 895-7576
E-Mail: [email protected]
Appendix
PIA Life Cycle Portal
Engineering, Ordering, Installation and Operation Tool
■ Overview
The PIA Life Cycle Portal provides the appropriate functionality
in all stages of the Product Life Cycle for products of Process In-
strumentation, Process Analytics and Weighing Technology.
The application guides you through Engineering & Selection,
supports you at the Order and provides tools and information for
Installation and Operation.
■ More information
PIA Life Cycle Portal
Ostliche Rheinbrückenstraße 50
76187 Karlsruhe, Germany
Tel.: +49 (721) 595 2114
E-Mail: [email protected]
www.siemens.com/pia-portal
Appendix
Partner at Industry
Appendix
Siemens Automation Cooperates with Education
Applicable practical know-how
Appendix
Siemens Automation Cooperates with Education
Applicable practical know-how
Appendix
Online Services
Information and Ordering in the Internet and on DVD
6
■ Easy Shopping with the Industry Mall
The Industry Mall is the electronic ordering platform of
Siemens AG on the Internet. Here you have online access
to a huge range of products presented in an informative and
attractive way.
Data transfer via EDIFACT allows the whole procedure from
selection through ordering to tracking and tracing of the order to
be carried out. Availability checks, customer-specific discounts
and preparation of quotes are also possible.
Numerous additional functions are available to support you.
For example, powerful search functions make it easy to select
the required products. Configurators enable you to configure
complex product and system components quickly and easily.
CAx data types are also provided here.
Please visit the Industry Mall on the Internet under:
www.siemens.com/industrymall
Appendix
Online Services
Information and Download Center, Social Media, Mobile Media
■ Downloading Catalogs
In addition to numerous other useful documents, you can also
find the catalogs listed on the back inside cover of this catalog
in the Information and Download Center. Without having to reg-
ister, you can download these catalogs in PDF format or increas-
ingly as digital page-turning e-books.
The filter dialog box above the first catalog displayed makes it
possible to carry out targeted searches. If you enter “MD 3” for
example, you will find both the MD 30.1 and MD 31.1 catalogs.
If you enter “ST 70” both the ST 70 catalog and the associated
news or add-ons are displayed.
Visit us on the web at:
www.siemens.com/industry/infocenter
■ Social Media
Connect with Siemens through social media: visit our social net-
working sites for a wealth of useful information, demos on prod-
ucts and services, the opportunity to provide feedback, to ex-
change information and ideas with customers and other
Siemens employees, and much, much more. Stay in the know
and follow us on the ever-expanding global network of social
media.
Connect with Siemens Industry at our central access point:
www.siemens.com/industry/socialmedia
Or via our product pages at:
www.siemens.com/automation
or
www.siemens.com/drives
6 To find out more about Siemens' current social media activities
visit us at:
www.siemens.com/socialmedia
■ Mobile Media
Discover the world of Siemens.
We are also constantly expanding our offering of cross-platform
apps for smartphones and tablets. You will find the current Sie-
mens apps at the app store (iOS) or at Google Play (Android).
The Siemens app, for example, tells you all about the history, lat-
est developments and future plans of the company – with infor-
mative pictures, fascinating reports and the most recent press
releases.
Appendix
Industry Services
Your machines and plant can do more – with Industry Services.
Whether it is production or process industry - in view of rising
cost pressure, growing energy costs, and increasingly stringent
environmental regulations, services for industry are a crucial
competitive factor in manufacturing as well as in process indus-
tries.
All over the world Siemens supports its customers with product,
system, and application-related services throughout the entire
life cycle of a plant. Right from the earliest stages of planning,
engineering, and building, all the way to operation and modern-
ization. These services enable customers to benefit from the
Siemens experts’ unique technological and product knowledge
and industry expertise.
Thus downtimes are reduced and the utilization of resources is
optimized. The bottom line: increased plant productivity, flexibil-
ity, and efficiency, plus reduced overall costs.
Discover all advantages of our service portfolio:
www.siemens.com/industry-services
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Siemens supports its clients with technology based Services across a plants entire life cycle.
Appendix
Industry Services
Industry Services for the entire life cycle
Online Support
Online support is a comprehensive information system for all
questions relating to products, systems, and solutions that
Siemens has developed for industry over time. With more than
300,000 documents, examples and tools, it offers users of auto-
mation and drive technology a way to quickly find up-to-date in-
formation. The 24-hour service enables direct, central access to
detailed product information as well as numerous solution exam-
ples for programming, configuration and application.
The content, in six languages, is increasingly multimediabased
– and now also available as a mobile app. Online support’s
“Technical Forum” offers users the opportunity to share informa-
tion with each other. The “Support Request” option can be used
to contact Siemens’ technical support experts. The latest con-
tent, software updates, and news via newsletters and Twitter en-
sure that industry users are always up to date.
www.siemens.com/industry/onlinesupport
Using the Online Support app, you can access over 300,000 “mySupport”. You also receive selected news on new functions,
documents covering all Siemens industrial products - anywhere, important articles or events in the News section.
any time. Regardless of whether you need help implementing
your project, fault-finding, expanding your system or are plan-
ning a new machine.
You have access to FAQs, manuals, certificates, characteristics
curves, application examples, product notices (e.g. announce- Scan the QR code
ments of new products) and information on successor products for information on
in the event that a product is discontinued. our Online Support
Just scan the product code printed on the product directly using app.
the camera of your mobile device to immediately see all techni-
cal information available on this product at a glance. The graph- The app is available free of charge from the Apple App Store
ical CAx information (3D model, circuit diagrams or EPLAN mac- (iOS) or from Google Play (Android).
ros) is also displayed. You can forward this information to your
workplace using the e-mail function. www.siemens.com/industry/onlinesupportapp
Technical Support
The ability to quickly analyze system and error messages and
take appropriate action are key factors in ensuring that plants
run safely and efficiently. Questions can arise at any time and in
any industry, whether it’s an individual product or a complete au-
tomation solution. Siemens technical support offers individual
technical assistance in matters related to functionality, how to
operate, applications, and fault clearance in industrial products
and systems – at any time and globally, over the phone, by e-
mail, or via remote access. Experienced experts from Siemens
answer incoming questions promptly. Depending on the require-
ments, they first consult specialists in the areas of development,
on-site services, and sales. Technical support is also available
for discontinued products that are no longer available. Using the
support request number, any inquiry can be clearly identified
and systematically tracked.
http://support.automation.siemens.com/WW/view/en/16605032
Appendix
Industry Services
Industry Services for the entire life cycle
Spare Parts
Drive and automation systems must be available at all times.
Even a single missing spare part can bring the entire plant to a
standstill – and result in substantial financial losses for the oper-
ator. The spare parts services from Siemens protects against
such losses – with the aid of quickly available, original spare
parts that ensure smooth interaction with all other system com-
ponents. Spare parts are kept on hand for up to ten years; de-
fective parts can be returned. For many products and solutions,
individual spare parts packages ensure a preventive stock of
spare parts on-site. The spare parts services is available around
the world and around the clock. Optimum supply chain logistics
ensure that replacement components reach their destination as
quickly as possible. Siemens’ logistics experts take care of plan-
ning and management as well as procurement, transportation,
customs handling, warehousing, and complete order manage-
ment for spare parts.
http://support.automation.siemens.com/WW/view/en/43502238
Repair Services
Reliable electrical and electronic equipment is crucial for oper-
ating continuous processes. That is why it is essential that mo-
tors and converters always undergo highly specialized repair
and maintenance. Siemens offers complete customer and repair
services – on site and in repair centers – as well as technical
emergency services worldwide. The repair services include all
measures necessary to quickly restore the functionality of defec-
tive units. In addition, services such as spare parts logistics,
spare parts storage and rapid manufacturing are available to
plant operators in all verticals. With a global network of certified
repair shops operated by Siemens as well as third parties, Sie-
mens handles the maintenance and overhaul of motors, convert-
ers, and other devices as an authorized service partner.
http://support.automation.siemens.com/WW/view/en/43512848
6
Field Services
It’s a top priority in all industries: the availability of plants and
equipment. Siemens offers specialized maintenance services
such as inspection and upkeep as well as rapid fault clearance
in industrial plants – worldwide, continuously, and even with
emergency services as needed. The services include startup as
well as maintenance and fault clearance during operation. The
startup service includes checking the installation, function tests,
parameterization, integration tests for machines and plants, trial
operation, final acceptance, and employee training. All services,
including remote maintenance of drives, are also available as el-
ements of customized service contracts.
http://support.automation.siemens.com/WW/view/en/66012486
Appendix
Industry Services
Industry Services for the entire life cycle
Training
Increasingly, up-to-date knowledge is becoming a determining
factor in success. One of the key resources of any company is
well-trained staff that can make the right decision at the right mo-
ment and take full advantage of the potential. With SITRAIN –
Training for Industry, Siemens offers comprehensive advanced
training programs. The technical training courses convey exper-
tise and practical knowledge directly from the manufacturer.
SITRAIN covers Siemens’ entire product and system portfolio in
the field of automation and drives. Together with the customer,
Siemens determines the company’s individual training needs
and then develops an advanced training program tailored to the
desired requirements. Additional services guarantee that the
knowledge of all Siemens partners and their employees is al-
ways up-to-date.
http://support.automation.siemens.com/WW/view/en/43514324
http://support.automation.siemens.com/WW/view/en/16605680
6
Energy & Environmental Services
Efficient energy use and resource conservation – these top sus-
tainability concerns pay off – both for the environment and for
companies. Siemens offers integrated solutions that unlock all
technical and organizational potential for successful environ-
mental management. Customized consulting services are aimed
at sustainably lowering the cost of energy and environmental
protection and thus increasing plant efficiency and availability.
The experts provide support in the conceptual design and im-
plementation of systematic solutions in energy and environmen-
tal management, enabling maximum energy efficiency and opti-
mized water consumption throughout the entire company.
Improved data transparency makes it possible to identify sav-
ings potential, reduce emissions, optimize production pro-
cesses, and thereby noticeably cut costs.
http://support.automation.siemens.com/WW/view/en/42350774
Appendix
Industry Services
Industry Services for the entire life cycle
Modernization & Optimization Services
High machine availability, expanded functionality and selective
energy savings – in all industries, these are decisive factors for
increasing productivity and lowering costs. Whether a company
wants to modernize individual machines, optimize drive sys-
tems, or upgrade entire plants, Siemens’ experts support the
projects from planning to commissioning.
Expert consulting and project management with solution respon-
sibility lead to security and make it possible to specifically iden-
tify savings potential in production. This secures investments
over the long term and increases economic efficiency in opera-
tion.
http://support.automation.siemens.com/WW/view/en/66005532
http://support.automation.siemens.com/WW/view/en/59456862
6
Service Contracts
Making maintenance costs calculable, reducing interfaces,
speeding up response times, and unburdening the company’s
resources – the reduced downtimes that these measures
achieve increase the productivity of a plant. Service contracts
from Siemens make maintenance and repairs more cost-effec-
tive and efficient. The service packages include local and re-
mote maintenance for a system or product group in automation
and drive technology. Whether you need extended service peri-
ods, defined response times, or special maintenance intervals,
the services are compiled individually and according to need.
They can be adjusted flexibly at any time and used indepen-
dently of each other. The expertise of Siemens’ specialists and
the capabilities of remote maintenance thus ensure reliable and
fast maintenance processes throughout a plant’s entire lifecycle.
http://support.automation.siemens.com/WW/view/en/65961857
Appendix
Software Licenses
■ Overview
Software types Rental floating license
Software requiring a license is categorized into types. The rental floating license corresponds to the rental license,
The following software types have been defined: except that a license is not required for each installation of the
• Engineering software software. Rather, one license is required per object (for example,
user or device).
• Runtime software
Trial license
Engineering software
A trial license supports "short-term use" of the software in a non-
This includes all software products for creating (engineering) productive context, e.g. for testing and evaluation purposes.
user software, e.g. for configuring, programming, parameteriz- It can be transferred to another license.
ing, testing, commissioning or servicing.
Data generated with engineering software and executable Demo license
programs can be duplicated for your own use or for use by third- The demo license support the "sporadic use" of engineering soft-
parties free-of-charge. ware in a non-productive context, for example, use for testing
and evaluation purposes. It can be transferred to another
Runtime software license. After the installation of the license key, the software can
This includes all software products required for plant/machine be operated for a specific period of time, whereby usage can be
operation, e.g. operating system, basic system, system expan- interrupted as often as required.
sions, drivers, etc. One license is required per installation of the software.
The duplication of the runtime software and executable pro-
grams created with the runtime software for your own use or for Demo floating license
use by third-parties is subject to a charge. The demo floating license corresponds to the demo license,
You can find information about license fees according to use in except that a license is not required for each installation of the
the ordering data (e.g. in the catalog). Examples of categories of software. Rather, one license is required per object (for example,
use include per CPU, per installation, per channel, per instance, user or device).
per axis, per control loop, per variable, etc. Certificate of license (CoL)
Information about extended rights of use for parameteriza- The CoL is the licensee's proof that the use of the software has
tion/configuration tools supplied as integral components of the been licensed by Siemens. A CoL is required for every type of
scope of delivery can be found in the readme file supplied with use and must be kept in a safe place.
the relevant product(s).
Downgrading
License types
The licensee is permitted to use the software or an earlier ver-
Siemens Industry Automation & Drive Technologies offers vari- sion/release of the software, provided that the licensee owns
ous types of software license: such a version/release and its use is technically feasible.
• Floating license
Delivery versions
• Single license
Software is constantly being updated.
• Rental license The following delivery versions
• Rental floating license • PowerPack
• Trial license • Upgrade
• Demo license can be used to access updates.
• Demo floating license Existing bug fixes are supplied with the ServicePack version.
6 Floating license
The software may be installed for internal use on any number of
PowerPack
PowerPacks can be used to upgrade to more powerful software.
devices by the licensee. Only the concurrent user is licensed. The licensee receives a new license agreement and CoL
The concurrent user is the person using the program. Use (Certificate of License) with the PowerPack. This CoL, together
begins when the software is started. with the CoL for the original product, proves that the new soft-
A license is required for each concurrent user. ware is licensed.
Single license A separate PowerPack must be purchased for each original
license of the software to be replaced.
Unlike the floating license, a single license permits only one
installation of the software per license. Upgrade
The type of use licensed is specified in the ordering data and An upgrade permits the use of a new version of the software on
in the Certificate of License (CoL). Types of use include for the condition that a license for a previous version of the product
example per instance, per axis, per channel, etc. is already held.
One single license is required for each type of use defined. The licensee receives a new license agreement and CoL with
the upgrade. This CoL, together with the CoL for the previous
Rental license product, proves that the new version is licensed.
A rental license supports the "sporadic use" of engineering A separate upgrade must be purchased for each original license
software. Once the license key has been installed, the software of the software to be upgraded.
can be used for a specific period of time (the operating hours do
not have to be consecutive).
One license is required for each installation of the software.
Appendix
Software Licenses
■ Overview
ServicePack Software Update Service (SUS)
ServicePacks are used to debug existing products. As part of the SUS contract, all software updates for the respec-
ServicePacks may be duplicated for use as prescribed accord- tive product are made available to you free of charge for a period
ing to the number of existing original licenses. of one year from the invoice date. The contract will automatically
be extended for one year if it is not canceled three months
License key before it expires.
Siemens Industry Automation & Drive Technologies supplies The possession of the current version of the respective software
software products with and without license keys. is a basic condition for entering into an SUS contract.
The license key serves as an electronic license stamp and
is also the "switch" for activating the software (floating license, You can download explanations concerning license conditions from
rental license, etc.). www.siemens.com/automation/salesmaterial-as/catalog/en/
The complete installation of software products requiring license terms_of_trade_en.pdf
keys includes the program to be licensed (the software) and the
license key (which represents the license).
Appendix
Conditions of sale and delivery
Catalogs
Industry Automation, Drive Technologies and Low-Voltage Power Distribution
Further information can be obtained from our branch offices listed at www.siemens.com/automation/partner
System Solutions for Industry Catalog Low-Voltage Power Distribution and Catalog
Interactive Catalog on DVD Electrical Installation Technology
Products for Automation and Drives, Low-Voltage Power CA 01 SENTRON · SIVACON · ALPHA LV 10
Distribution and Electrical Installation Technology Protection, Switching, Measuring and Monitoring
Devices, Switchboards and Distribution Systems
Building Control Standards-Compliant Components for LV 11
GAMMA Building Control ET G1 Photovoltaic Plants
3WT Air Circuit Breakers up to 4000 A LV 35
Drive Systems 3VT Molded Case Circuit Breakers up to 1600 A LV 36
Digital: SIVACON System Cubicles, System Lighting LV 50
SINAMICS G130 Drive Converter Chassis Units D 11
and System Air-Conditioning
SINAMICS G150 Drive Converter Cabinet Units
SINAMICS GM150, SINAMICS SM150 D 12 Digital: ALPHA Distribution Systems LV 51
Medium-Voltage Converters ALPHA FIX Terminal Blocks LV 52
SINAMICS PERFECT HARMONY GH180 D 15.1 SIVACON S4 Power Distribution Boards LV 56
Medium-Voltage Air-Cooled Drives Digital: SIVACON 8PS Busbar Trunking Systems LV 70
Germany Edition Digital: DELTA Switches and Socket Outlets ET D1
SINAMICS G180 D 18.1
Converters – Compact Units, Cabinet Systems,
Cabinet Units Air-Cooled and Liquid-Cooled Motion Control
SINAMICS S120 Chassis Format Units and D 21.3 SINUMERIK & SIMODRIVE NC 60
Cabinet Modules Automation Systems for Machine Tools
SINAMICS S150 Converter Cabinet Units SINUMERIK & SINAMICS NC 61
SINAMICS DCM DC Converter, Control Module D 23.1 Equipment for Machine Tools
SINAMICS DCM Cabinet D 23.2 SINUMERIK 840D sl Type 1B NC 62
SINAMICS and Motors for Single-Axis Drives D 31 Equipment for Machine Tools
SINAMICS G120P and SINAMICS G120P Cabinet D 35 SINUMERIK 808 NC 81.1
pump, fan, compressor converters Equipment for Machine Tools
Three-Phase Induction Motors SIMOTICS HV, D 84.1 SINUMERIK 828 NC 82
SIMOTICS TN Equipment for Machine Tools
• Series H-compact SIMOTION, SINAMICS S120 & SIMOTICS PM 21
• Series H-compact PLUS Equipment for Production Machines
Asynchronous Motors Standardline D 86.1 Drive and Control Components for Cranes CR 1
Synchronous Motors with Permanent-Magnet D 86.2
Technology, HT-direct Power Supply
DC Motors DA 12 Power supply SITOP KT 10.1
SIMOREG DC MASTER 6RA70 Digital Chassis DA 21.1
Converters
Safety Integrated
SIMOREG K 6RA22 Analog Chassis Converters DA 21.2
Digital: SIMOREG DC MASTER 6RM70 Digital DA 22 Safety Technology for Factory Automation SI 10
Converter Cabinet Units
SIMOVERT PM Modular Converter Systems DA 45 SIMATIC HMI/PC-based Automation
SIEMOSYN Motors DA 48 Human Machine Interface Systems/ ST 80/
MICROMASTER 420/430/440 Inverters DA 51.2 PC-based Automation ST PC
MICROMASTER 411/COMBIMASTER 411 DA 51.3
SIMODRIVE 611 universal and POSMO DA 65.4 SIMATIC Ident
Note: Additional catalogs on SIMODRIVE or SINAMICS Industrial Identification Systems ID 10
drive systems and SIMOTICS motors with SINUMERIK
and SIMOTION can be found under Motion Control
SIMATIC Industrial Automation Systems
Low-Voltage Three-Phase-Motors Products for Totally Integrated Automation ST 70
SIMOTICS Low-Voltage Motors D 81.1 SIMATIC PCS 7 Process Control System ST PCS 7
SIMOTICS FD Flexible Duty Motors D 81.8 System components
LOHER Low-Voltage Motors D 83.1 SIMATIC PCS 7 Process Control System ST PCS 7 T
MOTOX Geared Motors D 87.1 Technology components
SIMOGEAR Geared Motors MD 50.1 Add-ons for the SIMATIC PCS 7 ST PCS 7 AO
SIMOGEAR Gearboxes with adapter MD 50.11 Process Control System
Mechanical Driving Machines
FLENDER Standard Couplings MD 10.1 SIMATIC NET
FLENDER High Performance Couplings MD 10.2 Industrial Communication IK PI
FLENDER SIG Standard industrial gear unit MD 30.1
FLENDER SIP Standard industrial planetary gear units MD 31.1 SIRIUS Industrial Controls
SIRIUS Industrial Controls IC 10
Process Instrumentation and Analytics
Field Instruments for Process Automation FI 01
Digital: SIPART Controllers and Software MP 31
Products for Weighing Technology WT 10 Information and Download Center
Digital: Process Analytical Instruments PA 01 Digital versions of the catalogs are available on the Internet at:
Digital: Process Analytics, PA 11 www.siemens.com/industry/infocenter
Components for the System Integration There you’ll find additional catalogs in other languages.
Please note the section “Downloading catalogs” on page
Digital: These catalogs are only available as a PDF. “Online services” in the appendix of this catalog.
© Siemens AG 2014
Security information
Siemens provides products and solutions with
industrial security functions that support the
secure operation of plants, solutions, machines,
equipment and/or networks. They are important
components in a holistic industrial security
concept. With this in mind, Siemens’ products
and solutions undergo continuous development.
Siemens recommends strongly that you regularly
check for product updates.
Siemens AG Subject to change without prior notice The information provided in this catalog contains merely general
Process Industries and Drives Division PDF (E86060-K3501-A101-B1-7600) descriptions or characteristics of performance which in case of
actual use do not always apply as described or which may change
Process Automation KG 1214 PDF 482 En
as a result of further development of the products. An obligation to
76181 KARLSRUHE Produced in Germany provide the respective characteristics shall only exist if expressly
GERMANY © Siemens AG 2014 agreed in the terms of contract. Availability and technical
specifications are subject to change without notice.
All product designations may be trademarks or product names
of Siemens AG or supplier companies whose use by third parties
for their own purposes could violate the rights of the owners.
www.siemens.com/automation