Nbs Technical Note: DEPARTMENT OF COMMERCE I National Bureau of Standards
Nbs Technical Note: DEPARTMENT OF COMMERCE I National Bureau of Standards
L
NBS TECHNICAL PUBLICATIONS
PERIODICALS Building Science Series-Disseminates technlcdl InformatIon
developed dt the BureJ.u on bUIlding materials, components,
JOURNAL OF RESEARCH-The Journal of Research of the systems, and whole structures The seTies presents research results,
NatIOnal Bureau of Standards reports NBS research and develop- test methods, and performdnce cntena related to the structural and
ment 10 those disciplines of the physICal and engmeenng sCiences In environmental functions and the dUT<lbJlIty and s.:lfety charac
which the Bureau IS actIve These Include physIcs, chemIstry, teTlSI1CS of bUIlding elements and systems.
engmeeflog, mathematics, and computer sCiences Papers cover a
broad range of subjects, With major emphaSIS on measurement Technical Nates-StudIes or reports which are complete In them-
methodology and the baSIC technology underlying standardlzatlOo, selves but restrictIve in theIr treatment of a subject Andlogous to
Also mcluded from time to lime are survey articles on tOPiCS monographs but not so comprehenSIve m scope or definItIve In
closely related to the Bureau's technical dnd sCientific programs treatment of the subject drea Often serve as a vehIcle for final
As d speclal serVlce to sub~cnbers edch Issue contdms complete reports of work performed dt NBS under the sponsorshIp of other
CItatIOns to .':Ill fe,cenl Bureau pubbcatlOns in both NBS and non- government agencies
NBS media. Issued SIX tImes a year Annual subSCription domestic
$18; foreign $22 50. Single copy, $4 25 domestr<:; $535 foreign Voluntary Product Standards-Developed under procedures
pubhshed by the Department of Commerce In Part 10, TItle J 5, of
the Code of Federdl ReguldtlOns. The stdndards estabhsh
NONPERIODICALS natlonally recogmzed requirements for products, and prOVIde all
concerned Interests with a ba<;ls for common understandmg of the
Monographs-Major contributIons to the technr<:a.l literature on chanwtemtlcs of the products. NBS adminIsters thIS program as a
vanous subjects related to the Bureau's sClentilic and techmcal ac- supplement to the dctlVltH:S of the pnvdte sector stdndardlZlng
tIVIties. organllCitlOns.
Handbooks-Recommended codes of engmeermg and mdustrlal
practIce (lncludmg safety codes) developed in cOvperiltlon WIth In- Consumer Information Series-PractIcal mformatlOn, based on
terested Industries, profeSSIonal organizatIOns, dnd regulatory N as research and expeTlence, covermg aredS of JOterest to the con~
bodies sumer. EaSIly understandable language dnd Illustrations prOVIde
useful background knowledge for shoppmg In today's tech.
Special Publications-Include proceedIngs of conferences spon-
nologlcal marketplace
sored by NBS, NBS dnnual reports, and other spec1d.1 publications
dpprOpriate to thIS grouping such J,S wall charts, pocket cdrds, and Order the alJo..e NBS publica/10m from SuperINtendent oj Docu-
bibhographies me/HI, Government PrrntINg Office, Washing/on, DC 20402
Applied Mathematics Series-Mathemdtrc,d tdbles, manudls, and Order the follOWing NBS pubfIcatlon~-FIPS and NBS[R'~-from
studle~ of speCIal mterest to physiCIsts, englOeers, chemIsts, the NatIOnal Techmcal In!ormatrofl Serwcer. SpringfIeld. VA 22161
bIologIsts, mathematiCians, computer programmers, and others Federal Information Processing Standards Publications (FIPS
engaged in SCIentIfic and technlcdl work PVB)~PubJlcations m thJS senes collectIvely constitute the
National Standard Reference Data Series-Provides quantltallve Federdl Information Processmg Stdnddfds RegIster The RegIster
ddtd on the physlc<il and chemIcal properties of matenals, com- serves as the offIcial source of InformatIon in the Federal Govern·
ptled from the world's ltterdture and cntlcally evaluated. ment regardmg stdndards Issued by NBS pursudnt to the Federal
Developed under d worldWIde program coordmdted by NBS under Property and Aclmmlstratlve Service'> Act of 1949 as amended,
the duthority of the NatlOndl StdnddTd Ddto( Act (Pubhc Law Public Law 89·j06 (79 Stat 1127), and as implemented by Ex-
90-396) ecutIve Order J 1717 (38 FR 12315, dated May 11, 1973) dnd Part 6
of Title 15 CFR (Code of Federdl RegulatJons).
NOTE' The pnnclpdl pubJlcdtion outlet for the foregomg data lS NBS Interagency Reports (NBSIR)-A speCIal senes of InteTlm or
the Journal of PhYSICdl and ChemIcal Reference Data (JPCRD) fmal reports on work performed by NBS for outSIde sponsors
published quarterly for NBS by the Ameflcdn Chemlcdl Society (both government and non-government). In generdl. Inltlal diS-
(ACS) and the Amencan Institute of PhysJCS (AlP) Subscriptions, tnbutlOn IS hdndled by the sponsor~ publiC dlstnbutlon IS by the
repnnts, and supplements dval1able from ACS, 1155 SIxteenth St, NutlOn<l\ Techmcdl lnformahon SerVIces, SpnngfleJd, VA 22161,
NW, Wdshmgton, DC 20056 In paper copy or mIcrofiche form.
An Accuracy Statement for a Facility Used to
Calibrate Static Pressure Transducers and
Differential Pressure Transducers at High
Base Pressure
C. F. Sindt
J. F. laBrecque
Sponsored by:
The American Gas Association
1515 Wilson Blvd.
Ariington, VA 22209
and
1. Introduction
This accuracy statement describes the equipment used for differential and
static pressure transducer calibrations and the tracibility of the accuracy of
this equipment to the National Bureau of Standards. The purpose of the pressure
calibration facility is to calibrate both the static pressure transducers and
the differential pressure transducers used in the Gas Mass Flow Reference Facil-
ity. The calibration facility is designed to calibrate the transducers in place
using the transducer signal conditioning equipment as used for data gathering in
the flow facility. The equipment included in the calibration of the transducer
and its signal conditioning system is a transducer, an electrical power supply
for the transducer, an analog-to-digital voltage converter, a channel
multiplexer and a mini-computer.
The pressure range of the calibration facility to calibrate the static
pressure transducers is 3.8 (550 psi) to 4.27 MPa (620 psi}, and an air dead
weight tester provides the calibration standard. The differential pressure
transducers are calibrated with a mercury manometer which can be used at base
pressures as high as 34 MPa. For our'use, the base pressure at 4.1 MPa (600
I
L
psi) is applied to both sides of the mercury manometer and the differential
pressure transducer, then the desired differential is added to the base
pressure. These differential pressure transducers are calibrated in the range
of Z.5 kPa (10 in. HZO) to 50 kPa (ZOO in. HZO). We have examined
experimentally the accuracy to which this manometer can calibrate these
transducers.
Z. SURllla ry
By using an air dead weight gage as the transfer standard between
NBS-Washington and NBS-Boulder, we have been able to establish a calibration
facility that contributes no ~re than ~ 690 ppm of systematic error to the
total uncertainty of the calibration of differential pressure transducers at 50
kPa and no more than ~ 65 ppm to that of the static pressure transducers. The
total uncertainty of measurements made with a pressure transducer also contains
the uncertain~ in the correction relationship between readings made on the
transducer and the corresponding readings of the standard, plus the random
imprecision of the pressure transducer. In examples given in the text of actual
calibrations of pressure transducers, a static pressure transducer is calibrated
with a total uncertainty of ~ 570 ppm at 4.1 MPa, and a differential pres'sure
transducer is calibrated with a total uncertainty of ~ lZ54 ppm at 50 kPa. The
differential pressure transducer calibration uses a cistern-type mercury
manometer, which is calibrated with the air dead weight gage. The direct
calibration of the cistern manometer is made at ambient pressure; the correction
at the base pressure of 4.1 MPa has been verified by using two air dead weight
gages, one as a reference and the calibrated gage as the measuring device.
--'
gage from a clean gas source until the piston rises in the cylinder. As a min-
ute amount of gas flows past the piston it drops slowly with time, but the
pressur~ is maintained as the piston falls. The piston is rotated either
manually or via a built-in motor drive. Rotation of the piston eliminates
static friction between the piston and cylinder, so the piston is floating on a
gas column and is lubricated at the cylinder walls with a gas film. The level
of pressure measured is set by the weight of the piston and the weights added
to it. The dead weight gage thereby uses the basic measurement units of mass
and pi stan area to measure pressure. The ai r dead wei ght gage used for our
calibrations has two piston-cylinder sizes. The smaller piston has a pressure
range to 4.27 MPa (620 psi). The larger piston measures pressure to 107 kPa
(15.5 psi). The smaller piston is used to calibrate the static pressure
transducers before each day of tests. The larger piston is used at ambient base
pressure to calibrate the cist~rn manometer. This in turn is used to calibrate
the differential pressure transducers before each day's tests.
Both of the piston-cylinder assemblies were calibrated by the National
Bureau of Standards' National Measurement Laboratory at Gaithersburg, MD. The
calibrations determine the effective area of each piston at the specified test
conditions. The specified conditions and the calibrations are included as
AppendiK A. As described in AppendiK A, a number of models were fit to the
calibration data. The model
Force = Area K Pressure
has been selected as adequate for both piston assemblies to determine the
effective piston area. Also note that the ranges reported in AppendiK A are
slightly less than we have available on our gage. This discrepancy resulted
because NBS-Gaithersburg did not calibrate the weight set and, therefore, was
not aware of the weights available in our set. Our weight set was calibrated at
the State of Colorado Metrology Laboratory, Denver, CO. The report of this
calibration is included as Appendix B. Note that the masses are reported as
apparent mass versus brass. This calibration technique of using apparent mass
versus brass corrects for the air buoyancy of weights of unknown density,
provided we use this mass and the air buoyancy correction for brass to calculate
the force on the piston of the air dead weight gage. The air buoyancy
correction is then
3
1 - a
b
where a is the local air density and b is the density of the standard brass
weight which is 8.4 g/cm3 •
Besides the air bouyancy correction for the weights, several other
corrections must be considered for each data. point for accurate pressure
measurement using the dead weight gage. They include corrections for the
thermal expansion of the piston and cylinder, corrections for local gravity,
and corrections for the elasticity of the piston and cylinder. As noted in
Appendix A, these corrections have been applied to the calibrations at
NBS-Gaithersburg. The'thermal expansion correction is made for each gage
reading by measuring the gage temperature using a built in thermometer and
applying the correction using the coefficient of thermal expansion of the piston
and cylinder material. The gravity correction is constant and is applied to
each reading using the local acceleration of gravity. The piston and cylinder
were calibrated at ~BS at pressure so a~ elastic deformation is, in effect,
I
included in the caliibration. Table I gives the error uncertainties for these
corrections.
Having calibrated a pressure transducer at, say, a fixed set of conditions
against the air dead weight gage, the total uncertainty of the ave~age of n
measurements made with the calibrated transducer at this same set of conditions
is defined here as:
where SE s is the systematic error limit for the standard, "/3 is the standard
deviation of the correction of the readings of the calibrated meter to those of
the standard, "c is the standard deviation for readings made with the
calibrated gage, n is the number of readings made at the fixed, set of conditions
and 2.576 1s the 99.5 percentile of the standard normal distribution. The "8
and "c are not ~dded in quadrature because the correction is now fixed and its
uncertainty be~omes a systematic error for future measurements using the
calibrated gage.
Most often "/3 and "c are unknown and must be estimated from the data,
that is, "13 is estimated from the data used to calibrate the transducer and
4
lOt
ac is estimated from pressure measurements made with the transducer. Then the
total uncertainty limit (T.U.L.) for an average of n measurements made with the
calibrated tranducer is defined as:
where ~ and ~ are the estimated standard deviations, and A and B are factors
greater than 1 which increase the limit in proportion to our uncertainty of the
estimates. These values of A and B decrease toward 1 as the number of
observations used in making each of the estimates increases. The value of
2.576A is taken from the table of the 99.5 percentiles of the student-t
statistics and B is derived using the table of the 0.01 percentiles of the
chi -square di stribution. Both A and B are functions of the number of
observations used. See NBS Handbook 91 [1).
For the high pressure piston, SE s equals 57 ppm for the piston area, plus
3 ppm uncertainty for the weights, plus 5 ppm uncertainty for the gage
corrections (65 ppml. The two flow system static pressure transducers are
calibrated using a first degree least squares fit to six replicated pressure
values (12 points). The same values, to a close approximation, are used for
each calibration, and the values are in the range of 3.8 MPa to 4.27 MPa. From
our experience with the two static pressure transducers in over a dozen
calibrations, we can ascribe for our example the nominal values of 100 ppm and
200 ppm to the estimates of afj and ac, respectively. We use the value A = 1.2
because of using 12 points in each calibration, and the value B = 1.2 because we
have over a dozen such calibrations (i.e. over 100 pointsl. In our example of
how these numbers are used, we consider an average of n=10 values, then
A /',
The estimates of afj and ac were obtained from linear least squares fits of the
transducer data to the corresponding air dead weight data. The uncertainty in
the calibration of the air dead weight gage, SE s =65 ppm, adds little to the
T.U.L.
5
4. Differential Pressure Transducer Calibration Facility
We are using a high-base-pressure cistern-type mercury manometer to
calibrate the transducers used to measure pressure drop across orifice plates.
Using this manometer, the transducers can be calibrated at the base pressures
used duri ng gas flow tests. The range of the di fferenti al pressure transducers
are 25 kPa (100 in. H20) and 50 kPa (200 in. H20). They are both calibrated
using a base pressure of 4.1 MPa (600 psi).
Amercury height sensing element is incorporated on the low pressure side
(tube side) of the cistern manometer. The manometer is constructed of stainless
steel so that the sensing element must detect a magnetic fl oat on the mercury
surface by sensing the change in inductance in a wire coil. The coil sensing
unit is driven by an electrical servo system, and it tracks the float and is
attached to a perforated metal band which pulls around a cog wheel. The wheel
drives a counter that displays the column height in inches. The ratio of the
cistern volume change to the low pressure side or column volume change is 20 to
1; the cistern level change is included in column height display through the
choice of gear ratios in the gear train between the cog wheel and the readout
counter.
Early in the program the manometer became e~ratic, especially at zero
differential pressure. After experimenting with several configurations of
floats, a steel ball 3.2 mm smaller in diameter than the inside diameter of the
manometer tube was selected. All data in the report were obtained using this
float.
When measuring mercury height at high base pressures, corrections must be
applied to the manometer readings relative to low base pressure conditions. A
head correction to the mercury column is required to account for the difference
in density in the two gas columns from the ~op of the mercury column to the
pressure transducer level. For the maximum mercury displacement used, 387 mm
(207 in. H20), the correction is -0.03 mm 1-0.016 in. H20}. This correction
is linear with height and independent of base pressure if we assume perfect gas
laws apply. At high base pressure, the pressure acting on the manometer tube
expands it slightly. The ratio of wall thickness to the inside diameter of the
cistern is similar to that of the tube and presumably expands a commensurate
amount. At the high base pressures, the gas column in the high pressure side of
the manometer contributes significantly to the ~rcury column height. This
,
6
differential pressure across the manometer is desired. The corrected mercury
column height hcor is
where hobs is the column height read, and PN and PHg are the
nitrogen gas and mercury liquid densities, respectively, at the temperature and
pressure of the measurement. At the base pressure at which the transducers will
be calibrated, 4.1 MPa, the correction amounts to 0.4% or 1.6 mm (0.86 in.
H20) for a 400 mm Hg column height.
Compressibility of the mercury, which increases density, must also be
considered when using a mercury manometer at elevated pressure. From NBS
Monograph 8 [2], the density of mercury increases 0.02% at 4.1 MPa. Table 2
gives the uncertainties of the errors associated with these corrections to the
cistern manometer.
The cistern manometer has no redundancy to test for proper operation of the
readout machinery. Therefore, the air dead weight gage with the low pressure
piston is included in the calibration system to provide a means of monitoring
the performance of the cistern manometer.
Use of the air dead weight gage and the low pressure piston does not permit
us to check the high pressure corrections to the cistern manometer at the
desired base pressure. Therefore, we elected to perform a limited number of
calibrations of the cistern manometer at high base pressure by using two air
dead weight gages. When using two air dead weight testers for calibrating a
differential pressure device, one instrument is used as the reference or base
pressure measurement and the other instrument measures the base pressure plus
the differential. Since both instruments are first balanced at the base
pressure the reference instrument does not need to be calibrated. Therefore, we
used the calibrated instrument for the base plus differential pressure. Because
the instrument must operate at the base plus the desired differential pressure
the high pressure piston must be used in this calibrating scheme. This means
that the precision for this calibration is limited to the precision of the high
pressure piston and not the low pressure piston as is the case for ambient base
pressure calibration.
L
The method using two air dead weight gages required a null device for zero
differential to determine when both gages are at equal pressures, since porting
two gage~ together produces an unstable condition allowing one gage to fall and
the other to rise. The minuscule difference in pressure produced by elevation
etc. is not enough to produce a stable condition. By using a null device to
separate the two gages, one can experimentally balance both gages at the same
pressure. To control the pressures at various gage settings and at the null,
several gas displacers are required. A schematic of the system is shown in
figure 1. Each time one displacer is adjusted the other must also be adjusted
since the mercury in the manometer transfers pressure.
To determine the absolute sensitivity of the dual piston method, we first
raised the system pressure to about 4.1 MPa with the cross-over valve open. We
then determined the null reading for the null measuring transducer. We selected
a base pressure so that the calibrating gage and not the reference gage was
balanced using preselected gage weights. Next we closed the crossover valve and
added weights to the reference gage and adjusted the displacers until both gages
were floating and the null device read the same as its previous null point. We
then added an additional 20 mg weight to the reference gage. This was easily
discernable by the null device. Twenty mg weight on the piston gage is
equivalent to 23.4 Pa (0.09 in. H20) so the balance method should be able to
detect 23.4 Pa, which is 0.05% of the range of the 50 kPa transducer.
The problem with using the dual piston method fOr high base pressure is
that the random variation over a number of days of measurements made at a
nominal pressure is four or five times that for similar measurements made at
atmospheric pressure. This allows us to only check for relatively gross errors
in the high pressure corrections. The random uncertainty for a correction at
41.3 kPa (166 in. H20), for example, is 55 Pa (!P.22 in. H20). The number
of days at which measurements were made at high base pressure is five, and some
of the uncertainty is likely due to learning the new procedures. Within this
limitation, however, we see no need for changes in the high pressure corrections
for the cistern manometer.
The cistern manometer is calibrated at ambient base pressure against the
air dead weight tester using nine specified pressure values; these values range
from 2.8 kPa (11 in. H20) to 52 kPa (207 in. H20). This ambient base pres-
sure calibration is performed in the same manner as the static pressure calibra-
tion described in section 3, except that the low pressure piston is used. All
correction to the air dead weight gage values still apply and are considered.
8
!!OJ
where SE p is 60 ppm systematic error for the low pressure piston plus 5 ppm
for corrections, plus 4 ppm uncertainty for the weights used, plus 400 ppm
uncertainty for high pressure and temperature corrections to cistern manometer
(469 ppm) and SEc = 2.576A'~, where ~ is our estimated standard deviation
for this correction to the cistern manometer reading and A' is as A is described
in the section 3 and depends on the number of readings that have gone into the
estimate~. The values for ~, A, ~, and B are as described in section 3
and are based on the fit to the n calibrations as mentioned above.
Table 3 presents these values for the 100 in. meter and Table 4 does the
same for the 200 in. meter. A large part of the systematic error of the
facility is due to the uncertainty in the temperature correction for the mercury
in the cistern manometer. We expect to improve our accuracy of this measurement
in the future.
9 I
l
L ~_~ --~------ - --~-~
High Pressure
Gas Supply
Trim
Displacer
Equalizer
Displacer
Reference
Deadweight Deadweight High Pressure
Tester Tester Cistern Manometer
11
I ~ _
Table 3a. Cistern Manometer Corrections and Total Uncertainty Limit for 100 in. meter (inches of water)
~
1\ /I
AP Correction (added) ~ A' 17m A .-.!iL B SEp+SE c T.U.L.
11.0 .049 .0051 1.36 .0043 1.79 .023 1.37 .020 .021 .15
19.6 .054 .0091 1.36 .011 1.79 .020 1.37 .020 .04B .16
41.4 -.029 .0192 1.30 .0024 1.79 .015 1.37 .020 .028 .12
60.8 .073 .0282 1.36 .0098 1.79 .014 1.37 .020 .063 .15
82.5 .122 .0382 1.14 .0060 1.79 .019 1.37 .020 .056 .16
102.7 .049 .0477 1.36 .0071 1.79 .025 1.37 .020 .073 .21
~
Table 4a. Cistern Manometer Corrections and Total Uncertainty Limit for 200 in. meter (inches of water)
1\ 1\ 1\
Correction (added) £ 17m T.U.L.
AP
~ A ~ B ~ SEp+SE c
11.0 .049 .0051 1.36 .0043 1. 79 .015 1.31 .043 .021 .14
41.4 -.029 .0192 1.30 .0024 1.79 .010 1.31 .043 .028 .12
82.5 .122 .0382 1.14 .0060 1.79 .011 1.31 .043 .056 .15
124.7 .038 .0579 1.44 .032 1.79 .011 1.31 .043 .176 .27
166.0 .096 .0770 1.14 .0053 1.79 .010 1.31 .043 .093 .19
207.4 .142 .0962 1.21 .015 1.79 .016 1.31 .043 .143 .26
Table 3b. Cistern Manometer Corrections and Total Uncertainty Limit for 100 in. meter (kPa)
A A A
LlP Correction (added) ~ A' 17m A 3L B ~ SEp+SEc T.U.L.
2.73 .012 .0013 1.36 .0011 1. 79 .0057 1.37 .0050 .0052 .037
4.88 .013 .0023 1.36 .0027 1. 79 .0050 1.37 .0050 .0119 .040
10.30 -.007 .0048 1.30 .0006 1. 79 .0037 1.37 .0050 .0070 .030
15.13 .018 .0070 1.36 .0024 1.79 .0035 1.37 .0050 .0157 .037
20.53 .030 .0095 1.14 .0015 1.79 .0047 1.37 .0050 .0139 .040
25.56 .012 .0119 1.36 .0018 1.79 .0062 1.37 .0050 .0182 .052
w
Table 4b. Cistern Manometer Corrections and Total Uncertainty Limit for 200 in. meter (kPa)
A A A
~P Correction (added) -lli A' 17m A --i... B ~ SEp+SEc T.U.L.
2.73 .012 .0013 1.36 .0011 1.79 .0037 1.31 .011 .0052 .035
10.30 -.007 .0048 1.30 .0006 1. 79 .0025 1.31 .011 .0070 .030
20.53 .030 .0095 1.14 .0015 1.79 .0027 1.31 .011 .0139 .037
31.03 .009 .0144 1.44 .0080 1.79 .0027 1.31 .011 .0438 .067
41.31 .023 .0192 1.14 .0013 1. 79 .0025 1.31 .011 .0231 .047
51.61 .035 .0239 1.21 .0037 1.79 .0040 1.31 .011 .0356 .065
5. References
[1J Natre11a, M. G.; Experimental Statistics. Nat. Bur. Stand. (U.S.) Handb.
91;· January 1963.
[2J Brombacker, W. G.; Johnson, D. P.; Cross, J. L.; Mercury Barometers and
Manometers. Nat. Bur. Stand. (U.S.) Monogr. 8; May 1960.
14
_I
APPENDIX A (Part 1)
APPENDIX A (Part 2)
APPENDIX B
15 I
I
L
APPENDIX A (Part 1)
PAGE 1
NBS-BOULDER
OE SCI' I I'll ON
16
PAGE 2
17
•
P 4G E 3
WEIGHTS NOT LISTED IN T~E WEIGHT TABLE ARE ASSIGNED NU~SERS 600 TO
699. THeSE USED IN THIS RUN ARE LISTEu ON THIS PAGE. THEY INCLUDE
PISTON, WEIGHT HANGERS ETC OF THE INSTURMENT UNDER TEST. ALSO LISTED
ARt T~E ChARACTERISTICS OF THE STANDARD USED IN THIS TEST AND AVAIL-
ABLE CATA FOR THE INSTRUMENT UNDER TEST.
_I 18
.
PAGE 4
THIS TAELE LISTS THE FORCE GENERATED AY THE LOAD ON THE STANDARD
INSTRUMENT. AN AIR BUOANCY CORRECTICN HAS BEEN APPLIED. ALSO LISTED
ARE THE CORRECTIOhS FOR SURFACE TENSION. TEMPERATURE. JACKET PRES-
SURE ANC PRESSURE COEFFICIENT OF THE STANDARD.
19
PAGE 5
THIS TABLE LISTS THE FORCE GENERATED BY THE LOAD ON THE INSTRUMENT
UNDER TEST. AN AIR BUOANCY CORRECTION HAS BEEN APPLIED. ALSO LISTEO
ARE TH~ CORRECTI0~S FOR SURFACE TENSION.TE~PERATURE AND FLUIO HEAD
IN THE CONNECTING LINES BETWEEN THE TWO INSTRUMENTS.
20
•
PAGE 6
THIS, TAELE LISTS TI-E OBSERVATION "lIMBERS. PRESSURE AND THE RESIDUALS
OF TI-E fITS CONVERTED TO THE EQUIVALENT PRESSURES.
I
21
PAGE 1
22
PAGE 8
.690+01+ *+
*-
.205 +01 + +
-.281+01+
. +
-.766+01+ +
-,125+02+ +
-.174+02+ * +
+---------+---------+---------+---------+---------+---------+
0.0000 6.9117+02 1.3823+03 2.0735+03 2.7647+03 3.4559+03 4.1470+03
23
PAGE 9
.131+02+* +
.903+01+ +
.493+01+ +
.828+00+ +
*
-.327+01+ +
-.737+01+ * * +
+---------+---------+---------+---------+---------+---------+
0.0000 6.9117+02 1.3823+03 2.0135+03 2.7647+03 3.4559+03 4.1470+03
24
PAGE 10
THE RESULTS OF THE TEST ARE COMPILED IN THIS TABLE. IT LISTS THE
COEfFICIENTS AND THEIR TRIPLED sTANOARD DEVIATIONS DUE TO RANDOM
SOURCES OF ERRORS AND. FOR THE HIGHEST PRESSURE. THE UNCERTAINTY IN
PRESS~RE DUE TO THE UNCERTAINTY IN THESE COEFFICIENTS.
SELEC T I eN RULES:
ANY FIT FOR WHICH THE TRIPLED STANDARD DEVIATION OF A COEFFICIENT
IS LARGER THAN THE COEFFICIENT IS DISCARDED.
TH~ FIT wITH THE SMALLEST STANDARD DEVIATION OF THE RESIDUALS REP-
RESENTS THE DATA ~GST CLOSELY.
AMONG NEARLY EQUIVALENT FITS THE ONE WITH THE SMALLER NuMBER OF
COEFFIECIENT SHOULD BE USED.
25
PAGE 10 (CONT'D)
A 5.40-05 AlA
81 0.00 KPA-l
0.00 KPA-2
r<~~--<'F. SCHOOLEY
J~MES
;71. ~?,{,7
9HIEF. TEMPERATURE MEASUREMENTS
AND STANDARDS DIVISION
CENTER FOR ABSOLUTE PHYSICAL QUANTITI
26
.
APPENDIX A (Part 2)
PAGE 1
NBS-SOUL DEI"
DESCRIPTION
27
l
PAGE 2
VALUES CF CHA«AC TERI 5 TIC PARA'IETERS OF T .... E INSTFWMENT WITH THE ES-
TIMATED UNCERTAINTY OF THE DETEP"1INATION AR':: G IV EN IN TW, FOLLOWING
TA8LEISI. EXPLANATORY INFORMAT ION IS GIVF:N IN THE ENCLOSED • 'SUP-
PLEMENT FOP RE"OR 1 5 ON DEAD "'EIGHT PI STaN G-\GES" •
28
•
PAGE :3
WEIGHTS NDT LISTED IN THE wEIGHT TARLE ~RE ~SSIGNED NUM8ERS 600 TO
699. THeSE USED IN THIS RUN ARE LISTFD DN THIS PAGE. THEY INCLUDE
PISTON. WEIGHT HANGERS ETC OF THE INSTURMFNT UNDER TEST. ALSO LIST~)
ARE THE (H~RACTERISTICS OF TH~ STANDARD USED IN THIS TEST AND AVAIL-
.. aLE CAT~ FOR THE INSTRUMENT UNDER TEST.
29
•
PAGE 4
TH1S TABLE LISTS THE fORCE GENERATED BY THE LOAD ON THE STANDARD
I"lSTRUMENT. AN AIR OUCANCY CORRECTION HAS 8"OE'l APPL IE/). ALSO LI STED
ARE T~E CORRECTIONS FOP SURFACE TENSION, TEMPERATURE. JACKET PRES-
SUR~ AND PRESSURE COEFFICIENT OF THE STANDARD.
30
.... _ __.__._------ -----------.......
.. .- --. ------ ·m
P~GF.: 5
THI S TAl?LE LI 5TS THE "OPC'" GENERAHD BY T.... E LOAD ON THE INSTRUME"!T
UNDER TEST. AN AIR BUC~NCY COFRECTICN HAS 8EEN APPLIED. ALSO LISTED
ARE T.... E CORRECTIONS FnR SURFACE TENSIrJN.TE~PER~TURE AND FLUID HEAD
IN THE crNNECTING LINFS BETWEEN T .... E TWO INSTRUMENTS.
31
PAGE 6
THIS TAFlE LISTS THE fJRSERVATION NU\1FlF.RS. PRESSURE AND THE RESIDUALS
OF THE FITS CCNVERT~O TO THE EQUIVALENT PRESSURES.
32
PAGE 7
33
Pto,GE f\
.152+00+
*
.634-01+ +
I
'I
I
I
-.251-01+
II
Ii
-.114+00+ +
-.202+00+ 2 +
+---------+---------+---------+---------+---------+---------+
0.0000 1.7454+01 3.4907+01 5.2361+01 6.9815+01 8.7268+01 1.0472+02
34
l
PAGE 9
.171+00+ +
.10~+00+ +
.414-01+ +
-.233-01+ +
-.880-01+ 2
*-+
+---------+---------+---------+---------~---------+---------+
0.0000 1.7454+01 3.4907+01 5.23tl+01 6.9~15+01 8.7268+01 1.0472+02
35
PAGE 10
THE RES~L1S OF THE TEST ARE COMPILED IN THIS TA8LE. IT LISTS THF
COEFFICIENTS 4NO ThEIR TRIPLED STANDARD DEVI4T10NS DUE TO RANDOM
SOURCES OF ERRORS AND. FOR ThE HIGHEST PRESSUR~. THE UNCERTAINTY IN
PRESSURE CUE TO THE UNCERTAINTY IN THESE COEFFICIENTS.
SELECT leN RULES:
ANY FIT FOR ~HICH THE TRIPLED STANDARD DEVIATION OF A COEFFICIENT
IS LARGER THAN THE COEFFICIENT IS DISCARDED.
THE FIT WITH THE S"'ALL!:ST STANDARD DEVIATH1N OF THE RESIDUALS REP-
RESENTS THE DATA MOST CLOSELY.
A"'ONG NE4RLY EQUIVALENT FITS THE ONE WITH THE SMALLER NU"'BER OF
CO~FFIF(IENl SHOULD DE USED.
36
PAGE 10 (CONT'D)
A ~.70-05 AlA
81 0.00 KPA-I
82 0.00 KPA-2
NATI~AL ME~SUP~MJNT~A80RATORY
'c _::7f~7 /{:l
JAME"S";:< lH~~lEY
CH~EF, TrMPERATURE MEASURE~ENTS
AND STANDARDS DIVISION
CENTER FOR AOSOLUTE PHYSICAL QUANTITIES
37
APPENDIX B
STATE OF COLORADO
DEPARTMENT OF AGRICULTURE
1525 Sherman Street
Denver, Colorado 60203
(303) 839-2811
Morgan Smith,
Commissioner
OWNER: National Bureau of Standards Cert. No: 7428
Donald Svedman,
Boulder, Colorado SIN: 28337 Deputy CommiSSioner
8 0.520313 "
9 0.260165 "
10 0.130072 0.24 ulb
11\ 0.0520390 0.19 ulb
12 0.0520339 "
13 0.0260203 0.18 ulb
14 0.0130124 0.17 ulb
15 0.0065115 "
The uncertainty figure is an expression of the overall uncertainty using three standard
deviations as a limit of the effect of random errors of measurement, the magnitude of
systematic errors from known sources being negligible.
THESE CERTifiCATIONS ARE TRACEABLE TO THE
N!lTIONAL BUREAU OF STANDARDS.
ALL CERTifiCATES ISSUED BY THE COLORADO
, t< DfPf,RTMENT OF AGRICULTURE-METROLOGY LAB-
:RATORY EXPIRE ONE YEAR FROM THE DATE OF
F H Br
ISSUANCE.
Colorado Met ology
3125 Wyandot St.
Denver, Colorado 80211
38
__ J
(03)839-2845
ADDRESS Boulder, Colorado Makllldescription: Ruska dead '"eight tester wei ghts
x ) MASS: The test weights described above have been compared with the standards of the Slate 'of Colorado and found
, of S1andards.
(adjusted) to be within the tolerances for their class as prescribed by the National Bureau
( X ) See "Report of TesllCailbration" attached.
) LENGTH: The linear measures described abOve have been compared with the standards of the Iltate of Colorado and
found to be within the tolerances prescribed by the National Bureau of Standards for this type of equipment.
) VOLUME: The volumetric standards described above have been compared w~h the standards of !the State of Colorado
and found (adjusted) to deliver at OF.
This value appHes when a second drain period is useclJoliowing the cessation of the main flow.
) FREQUENCY: The luning fork described abOve has been compared with the standard frequency output of the National Bureau
of Standards. This is to certify the above described tuning fork has been tested and found to oscillate
at Hz. When used with a doppler radar traffic gun operating at _ _ MHz, tt will resutt In a reading
of mph.
e Metrologist
39
N~ 7428 l
....
NBS..1l4A {REV. 2 ..80)
U.S. DEPT. OF COMM, 1. PUBLICATION OR 2. Performing Organ. Report No. 3. publication Date
REPORT NO.
BIBLIOGRAPHIC DATA NBS TN-1052
SHEET (See instructions) February 1982
4. TITLE AND SUBTITLE
5. AUTHOR(S)
C. F. Sindt and J. F. LaBrecque
6. PERFORMING ORGANIZATION (If Joint or other thon NBS. see instructions) 1. Contract/Grant No.
il 9. SPONSORING ORGANIZATION NAME AND COMPLETE ADDRESS (S"'''. City, Stat., ZIP)
12. KEY WORDS (Six to twelve entries; alphabetical order; capitalize only proper names; and separate key words by semicolons)
o Order From National Technical Information Service (NTIS), Springfield, VA. 22161 $6.50
The National Bureau of Standards I was establtshed by an act of Congress on March 3, 190(
The Bureau's overall goal is to strengthen and advance the NatIOn's sCience and technology
and facilitate theu effective applicatIon for pubhc benefit. To thIs end, the Bureau conducts
research and provides: (1) a baSIS for the NatIOn's physical measurement system, (2) sCientIfIc
and technological services for industry and government, (3) a technIcal baSIS tor equity In
trade, and (4) technical servIces to promote public safety. The Bureau's technical work IS per-
formed by the NatIOnal Measurement Laboratory, the National Engineering Laboratory, and
the Institute for Computer Sciences and Technology.
I
J