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A. Constant Weighing of Empty Crucible Crucible 1 Crucible 2

This document describes the process and results of a gravimetric analysis to determine the percentage of SO3 in an unknown soluble sulfate sample. The analysis involved weighing crucibles empty and after addition of the sulfate sample, BaCl2 solution, and barium sulfate precipitate. Constant weights were obtained after multiple heatings. Calculations using the weights determined the percentage of SO3 was 43.68% on average for the two trials, with a relative standard deviation of 3.367%.

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97 views1 page

A. Constant Weighing of Empty Crucible Crucible 1 Crucible 2

This document describes the process and results of a gravimetric analysis to determine the percentage of SO3 in an unknown soluble sulfate sample. The analysis involved weighing crucibles empty and after addition of the sulfate sample, BaCl2 solution, and barium sulfate precipitate. Constant weights were obtained after multiple heatings. Calculations using the weights determined the percentage of SO3 was 43.68% on average for the two trials, with a relative standard deviation of 3.367%.

Uploaded by

danica
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© © All Rights Reserved
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GRAVIMETRIC ANALYSIS

A. Constant Weighing of empty Crucible 1 Crucible 2


crucible
Weight after 1st heating 20.5974 22.9602
2nd heating 20.5970 22.9598
3rd heating 20.5978 22.9608
4th heating 20.5981 22.9605
Constant weight(g) (wt±0.0003g) 0.0003 0.0003
Trial 1 Trial 2
B. Weight of Unknown Soluble 0.6310 0.5063
Sulfate (g)

C. Weight of BaCl2, 2H2O (g) 1.3193 1.2870

D. Constant Weighing of unknown Crucible 1 Crucible 2


BaSO4 ppt in crucible
Weight after 1st heating 21.3824 23.6396
2nd heating 21.3822 23.6206
3rd heating 21.3826 23.6206
4th heating 21.3824
Constant weight(g) (wt±0.0003g) 0.0002 0.000
Trial 1 Trial 2
E. Weight if BaSO4 ppt (g) 0.7843 0.6601

F. %SO3 42.64% 44.72%

Mean % SO3 43.68%


Standard deviation (s) %SO3 1.471%
Relative Standard Deviation rsd 3.367%

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