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Manual Polarimeter

rotación optica

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119 views

Manual Polarimeter

rotación optica

Uploaded by

SergioFernandoMendozaMendoza
Copyright
© © All Rights Reserved
Available Formats
Download as PDF, TXT or read online on Scribd
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WXG-4 Manual Polarimeter

Instruction Manual

BANTE INSTRUMENTS LIMITED


WXG-4 Manual Polarimeter 1

Introduction
Thank you for selecting the Bante Instruments WXG-4 manual polarimeter. This manual provides a step-by-step guide to help you operate the instrument,
please carefully read the following instructions before use.

UNPACKING THE INSTRUMENT:


Before unpacking, ensure that the current work environment meet following conditions.
Ambient temperature is greater than 0oC and less than 40oC.
No potential electromagnetic and ambient light interference.

The following list describes the standard accessories of the polarimeter. After the unpacking, please check all accessories are complete. If any are damaged
or missing, please contact nearest distributor.
Test tube 100 and 200 mm
Sealing rings

Prior to Use
Before plugging the plug into the power outlet, ensure that local mains power voltage matchs the polarimeter requirements.
1. Close the lid of polarimeter, press the power switch to ON position, the sodium lamp will gradually light up.

2. Wait for the light source to stabilize, rotate the focus knob until visual field became legible.

Focus knob

3. Rotate the vernier knob makes the vernier scale aim at zero position.
WXG-4 Manual Polarimeter 2

Recording the Reference Point


1. Place an empty test tube into the sample chamber.
2. Rotate vernier knob until the visual field appears uniform brightness. Record the measured value of reference point.

Filling the Sample Solution


1. Take out the test tube from sample chamber. Unscrew the cap, remove the sealing ring and glass disc.

2. Rinse the test tube thoroughly with distilled water.


3. Pour sample solution into the test tube, then screw on the test tube cap. Wipe away the drops of water on glass disc.

4. If necessary collect all air bubbles into the bubble trap.

Bubble Trap

Measurement
1. Open the lid of polarimeter, place the test tube into the sample chamber. Note, the bubble trap is upward.
WXG-4 Manual Polarimeter 3

2. Close the lid, clockwise or anticlockwise rotate vernier knob until the visual field appears uniform brightness. Record the measured value.

3. Repeat above measurements 2 times and calculate the average of measured values.

Calculation
If the measured values are positive angle (Dextrorotatory substance), minus the value of the reference point shall be the actual measured value of the
substance. If the measured values are negative angle (Levorotatory substance), minus the 180o shall be the actual value of the substance.

Determination of the Concentration


After the measurement, if you need to determine purity, concentration or proportion of the sample, please use the following formula.

=[]LC

....... Optical Rotation


[]... Specific Rotation
L....... Tube length (dm)
C...... Concentration (g/L)

Replacing the Sodium Lamp


Before replacing the sodium lamp, be sure to disconnect the power plug from the wall outlet.
1. Wait for the sodium lamp to cool down, remove the lamp cover of polarimeter.

2. Pull the sodium lamp from the socket.


3. Insert a new lamp into the socket.
4. Replace the lamp cover again in such a way that the window point in the direction of the polarizer.
WXG-4 Manual Polarimeter 4

Specifications
Model WXG-4
Measuring Range -180 o ~180 o
Scale Value 1o
Vernier 0.05 o
Magnifier 3X
Light Source Sodium Lamp
Wavelength 589.44nm
Test Tube 50/100/200mm
Power Requirements 220V/50Hz
Dimensions 500(L) 135(W) 330(H)mm
Weight 5kg
Hazardous Substance Statement
Bante Instruments Limited is committed to the reduction and eventual elimination of all hazardous substances in both the manufacturing process and finished
products we supply. We have an active manufacturing and procurement program to minimize and eliminate the use of harmful heavy metals such as cadmium,
lead, mercury and the like. New technologies and design parameters are also promoting these efforts and we expect to have little or no such materials in our
product in the coming years. We welcome our customer suggestions on how to speed up these efforts.

Warranty
The warranty period for polarimeter is one year from the date of shipment. Above warranty does not cover sodium lamp. Out of warranty products will be
repaired on a charged basis. The warranty on your polarimeter shall not apply to defects resulting from:
Improper or inadequate maintenance by customer.
Unauthorized modification or misuse.
Operation outside of the environment specifications of the products.
For more information, please contact the nearest authorized distributor.

BANTE INSTRUMENTS LIMITED


E-mail: [email protected]
Phone: +8621-6404-1598
Website: www.bante-china.com

The information in this document is subject to change without notice. Copyright Bante Instruments Limited, 2013. All rights reserved.

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