Design of Experiments
Design of Experiments
Shiv G. Kapoor
Department of Mechanical Science and Engineering
University of Illinois at Urbana-Champaign
OUTLINE
1. Introduction
Role of Experimental Design, Important Concepts in the DOE
2. Review of Basic Statistical Methods and Probability Concepts
Discrete and Continuous Probability Distribution Functions,
Normal and Sampling Distributions, Tests of Hypotheses
3. Comparative Experiments
Comparing Two Treatments
4. Design and Analysis of 2k Factorial Experiments
General Factorial Designs and Design at Two levels
Calculation and Interpretation of Main and Interaction effe
5. Two-Level Fractional Factorial Designs
Rationale for, and Consequences of, Fractions of Two-Level
Factorials
Concept of Design Resolution
What is Variability?
Let us understand the proper interpretation of
variability in data via a dialog between the
professor and a young, naive student.
Professor: “I am interested in the tool life of
this tool.”
Conditions
Speed: 170 FPM
Feed: .017 IPR
Depth of Cut: 0.07 IN
Workpiece 1018 Steel 6”dia, 24” long
Speed
Tool Life
Feed
Depth of Cut
Material
Power
Regulator
Speed
Tool Life
Feed
Depth of Cut
Material
Experimental error
1. Composed of many minute disturbances
which individually have little effect on the
outcome of the experiment.
2. Collectively these small chance occurrences
may increase the dispersion or spread of the
results to the point where real variable effects
are masked.
@ 2006 Dr. Shiv G. Kapoor All Rights Reserved
IE 400 Lecture 1
DIFFICULTIES WITH EXPERIMENTAL
WORK WHICH REQUIRES STATISTICAL
METHODS
Experimental error
3. Composed of more than errors of
measurement – not all instrumentation
oriented. A good measurement system
accounts for no more than 10-15% of the
total error.
4. Can be a function of both unknown and
known sources.
@ 2006 Dr. Shiv G. Kapoor All Rights Reserved
IE 400 Lecture 1
Statistical analysis
1. Can the results be explained solely by
chance causes?
2. How much data is required to reveal the
existence of true effects in light of chance
error?
Example of Blocking
Material Material
A B
@ 2006 Dr. Shiv G. Kapoor All Rights Reserved
IE 400 Lecture 1
SOME IMPORTANT CONCEPTS RELATED
TO STATISTICAL DESIGN OF
EXPERIMENTS
Example of Blocking
First Experimental Design:
Twenty tools are made, ten with material A and
ten with material B.
Example of Blocking
First Experimental Design:
At the end of the experiments the mean
amount of wear is determined based on the ten
measurements for each material type.
The mean difference is calculated and
examined by a statistical test of significance.
No real difference is found.
@ 2006 Dr. Shiv G. Kapoor All Rights Reserved
IE 400 Lecture 1
SOME IMPORTANT CONCEPTS RELATED
TO STATISTICAL DESIGN OF
EXPERIMENTS
RANDOMIZATION TO GUARANTEE
VALIDITY OF TEST RESULTS
Example:
Two factors: temperature and pressure are thought to
affect chemical reaction time:
Mr. X’s
Experiment
Mr. Y’s
Experiment
Characterization of Data
Three Characteristics:
1) Central Tendency
2) Dispersion or Variability
3) Shape of Distribution of Frequencies
CHARACTERIZATION OF DATA
i =1
The variance of the population is referred to as σ2.
University of Illinois at Urbana-Champaign 2006 by Dr. Shiv G. Kapoor
CHARACTERIZATION OF DATA-AN
EXAMPLE
CHARACTERIZATION OF DATA-AN
EXAMPLE
70 + 72 + .... + 69 700
XA = = = 70
10 10
70 + 70 + ... + 70 700
XB = = = 70
10 10
CHARACTERIZATION OF DATA-AN
EXAMPLE
∑ ( X Ai − X A )2 ∑( X Bi − X B )2
SA = i =1
= 1.33 , S B = i=1
= 0.44
2 2
10 − 1 10 − 1
University of Illinois at Urbana-Champaign 2006 by Dr. Shiv G. Kapoor
CHARACTERIZATION OF DATA-AN
EXAMPLE
X A = 70 microinches, X B = 70 microinches,
S A = 1.15 microinches, S B = 0.66 microinches.
CHARACTERIZATION OF DATA-AN
EXAMPLE
Note that
d
f(x)= F(x)
dt
University of Illinois at Urbana-Champaign 2006 by Dr. Shiv G. Kapoor
d
f(x)= F(x)
Mathematical Expectation
1
f(x) = a≤x≤b
b-a
= 0 elsewhere
The mean and variance of this distribution are:
∞ 1 (b + a )
µ = E(x) = ∫ x dx =
-∞ (b − a ) 2
∞
Var(x) = E (x-µ ) 2 = ∫ (x-µ) 2f(x)dx
-∞
(b-a) 2
=
12
Example 1
Given:
1
f(x) = = 1.0 11.5 ≤ x ≤ 12.5
(12.5-11.5)
f(x) = 0 elsewhere
Also, let Profit, P be a random variable. It will take the values of
P = 0.25 11.7 ≤ x ≤ 12.2
P = 0.10 x ≥ 12.2
P = -0.02 x <11.7
∞
Since f(x) is known, we can find E(P) = ∫-∞
P(x) f(x) dx
12.2 11.7 12.5
E(P) = ∫11.7
(0.25) 1. dx + ∫
11.5
(−.02).1. dx + ∫
12.2
(0.10).1.
= 0.125 + (-0.004) + 0.03 = $0.151 = 15 cents.
Example
The heat shield plates for the space shuttle must have a
closely measured thickness in order to withstand the
rigors of heat from re-entry. After testing 400 of them,
the engineer found the thickness was normally
distributed with a mean of 22.5 mm. It was also found
that 382 plates were within 20 +/- 2.50 mm. If the
defective plates deviate more than 1.80 mm from the
mean, find the number of plates to be rejected during
the testing.
X − µ
z =
σ x
n
University of Illinois at Urbana-Champaign 2006 by Dr. Shiv G. Kapoor
DISTRIBUTION OF SAMPLE MEANS
Method 1 : H 0 : µ x =µ 0 H1 : µ > µ 0
Method 2 ; H 0 : µ x =µ 0 H1 : µ< µ 0
Method 3 : H 0 : µ x =µ 0 H1 : µ ≠ µ0
Solution
µ ± 1.96σ x / n
embraces 95% of all the sample means.
σx
In other words, X ± 1.96 is called a 95%
n
confidence interval for the true mean µ.
Graphically, we can show it as in Fig.2 and
Fig.3
σx
A more general statement is that X ± z 1−α / 2
n
is a 100(1-α)% Confidence Interval for µ.
σx σx
1.96 1.96
n n
s
X ± t v ,1−α / 2
n
where v is the degree of freedom and it equals n-1.
Example
Given that the sample size, n is small, the sample stat, follows a t-distribution.
X
Hence a 99% confidence interval for the true mean diameter is given by
s s
X - tν ( ) ≤ µ ≤ X + tν ( )
n n
0.003 0.003
0.305-3.355 ≤ µ ≤ 0.305 + 3.355
9 9
0.30165
The width of C. I. is ≤ µ ≤ 0.30835
s
2 tν = 2.(0.00335)=0.0067 .
n
University of Illinois at Urbana-Champaign 2006 by Dr. Shiv G. Kapoor
Session 3
Comparative Experiments
Prof. Shiv G. Kapoor
Comparative Experiments
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
Objective:
To compare the noise levels produced by two,
otherwise identical, circular saws, one
designed with equal blade spacing (the
‘conventional’ design) and another with uneven
spacing (the ‘modified’ design).
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
Calculation of V(N c − N m )
It can be shown theoretically that the variance
of ( N c − N m ) is
V ( N c − N m ) = V( N c ) + V( N m ) - 2 COV( N c N m ) (3)
where COV( N c N m ) is called the covariance of N c and N m .
Calculation of V(N c − N m)
V ( N c − N m ) = V( N c ) + V( N m ) (4)
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
Calculation of V(N c − N m )
Estimating the variances V( N c ) and V( N m) by
the sample variances , Sc2 and Sm2, we have
S2 S2 (5)
V ( N c − N m ) = V( N c ) + V( N m ) = c + m
nc nm
Assumption: The two data sets come from
the same process (two normal distributions
with equal variances, i.e. Sc2=Sm2=S2)
Calculation of V(N c − N m )
The common (Pooled) variance is defined as:
( n − 1 )S c + ( n m − 1 )S m
2 2
= c
2
Sp
( nc − 1 ) + ( nm − 1 )
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
∑(N ci − N c )2
1
Sc = i =1
= ( 225.5) = 45.10
2
nc − 1 6 −1
8
∑(N mi − N m )2
1
Sm = i =1
= ( 212.88) = 30.41
2
nm − 1 8 −1
IE 400 Lecture 3 @2006 Dr. Shiv G. Kapoor All Rights Reserved
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
( 6 − 1) + (8 − 1)
225 .50 + 212 .88
= = 36 .53
5+7
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
Calculation of V(N c − N m )
It can be shown theoretically that the variance
of ( N c − N m ) is
V ( N c − N m ) = V( N c ) + V( N m ) - 2 COV( N c N m ) (3)
where COV( N c N m ) is called the covariance of N c and N m .
Calculation of V(N c − N m)
V ( N c − N m ) = V( N c ) + V( N m ) (4)
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
Calculation of V(N c − N m )
Estimating the variances V( N c ) and V( N m) by
the sample variances , Sc2 and Sm2, we have
S2 S2 (5)
V ( N c − N m ) = V( N c ) + V( N m ) = c + m
nc nm
Assumption: The two data sets come from
the same process (two normal distributions
with equal variances, i.e. Sc2=Sm2=S2)
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
∑(N ci − N c )2
1
Sc = i =1
= ( 225.5) = 45.10
2
nc − 1 6 −1
8
∑(N mi − N m )2
1
Sm = i =1
= ( 212.88) = 30.41
2
nm − 1 8 −1
IE 400 Lecture 3 @2006 Dr. Shiv G. Kapoor All Rights Reserved
Test for equal variances
Calculation of V(N c − N m )
The common (Pooled) variance is defined as:
( n − 1 )S c + ( n m − 1 )S m
2 2
= c
2
Sp
( nc − 1 ) + ( nm − 1 )
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
( 6 − 1) + (8 − 1)
225 .50 + 212 .88
= = 36 .53
5+7
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
∑ di
31
d = i=1
= = 3 .1
10 10
The 95% confidence interval for the difference
is given as
d ± t V(d )
IE 400 Lecture 3 @2006 Dr. Shiv G. Kapoor All Rights Reserved
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
d
V (d )
t value.
IE 400 Lecture 3 @2006 Dr. Shiv G. Kapoor All Rights Reserved
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
d:
Table 2 gives the ten differences d1, d2, ...., d10.
The average difference is: d = 3.10
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
V (d ) 4.458
V (d ) = = = 0.4458
n 10
t value:
Here, one degree of freedom has already been used
up in calculating the mean, and the value of t
associated with nine degrees of freedom and
corresponding to a 95% confidence level is t9,.025 = 2.
262.
The 95% confidence interval is, from equation (6),
COMPARISON OF TWO
TECHNIQUES/DESIGNS/PROCESSES
Factorial Designs
Factorial Designs
Factorial Designs
Variables vs Levels
A design with 3 variables at 2 levels would require 8
tests for a 2 x 2 x 2 = 23 factorial design
A design with 3 variables at 3 levels would need 27
tests for a 3 x 3 x 3 = 33 factorial design.
A design with 5 variables at 2 levels would need 32
tests for a 25 factorial design.
Transforming Equations
In order to adopt a notation which will be the same for
all two-level factorial designs, we use transforming
equations to code the variables such that
the high level will be denoted by +1,
the low level will be denoted by -1.
By so doing, regardless of the physical conditions
represented by the two levels, the basic design of any
two-level factorial design becomes a simple
arrangement of +1 and -1.
Transforming Equations
For example:
The transforming equation for ambient
temperature (T) is
(T − 35)
X1 =
35
Transforming Equations
In order to code the high and low levels of the
ambient temperature into +1 and -1, we simply
substitute the two levels, 00F and 700F, of the
ambient temperature into the above transforming
equation.
(0 − 35)
For the low level, X1 = = −1
35
(70 − 35)
For the high level, X1 = = +1
35
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
Table 2 : The 23 Factorial Design for the High Strength Steel Bar Problem
Coded Test Conditions Actual Test Conditions
Test # X1 X2 X3 °F (mph) (1/8 in)
1 -1 -1 -1 0 0 4
2 1 -1 -1 70 0 4
3 -1 1 -1 0 20 4
4 1 1 -1 70 20 4
5 -1 -1 1 0 0 11
6 1 -1 1 70 0 11
7 -1 1 1 0 20 11
8 1 1 1 70 20 11
Two-Variable Interactions
The average effects E1, E2, and E3 represent the
individual effects of ambient temperature, wind
velocity, and bar size on the ultimate tensile
stress.
What about the joint effect of two variables, say,
ambient temperature and wind velocity on the
ultimate tensile stress?
or wind velocity and bar size on the ultimate
tensile stress?
These joint effects are indicated by the
two-variable interactions.
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
Two-Variable Interactions
Physically, what is a two-variable interaction?
Let us consider the hypothetical set of
data given in Figure 4.
The numbers located at each of the four
corners represent the hypothetical test
results which may be observed at the four
sets of test conditions given by the four
corners.
Wind
Velocity
90 100
(low) Ambient (high)
Temperature
Two-Variable Interactions
The difference in the test results due to a
change of ambient temperature performed
at the low level of wind velocity is
100 - 90 =10.
At the high level of wind velocity, the
difference is
120 - 110 = 10.
Two-Variable Interactions
These two differences, which are due to the
change in ambient temperature at different
levels of wind velocity, are identical.
We say, in this case, that there is no
interaction between ambient temperature and
wind velocity.
Two-Variable Interactions
In other words if the effect of changing
ambient temperature is the same at both
levels of wind velocity (or, if the effect of
changing the wind velocity is the same at both
ambient temperature levels), there is no
interaction between ambient temperature and
wind velocity.
In a sense, ambient temperature and wind
velocity act independently of one another.
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
AN EXPERIMENTAL STUDY USING A 23
FACTORIAL DESIGN
Two-Variable Interactions
On the other hand, consider the results given in the
following Figure 5.
(high
) 10
1 140
Wind
Velocit
y
90 100
(low) Ambient (high
Temperature )
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
Two-Variable Interactions
Here, for the low level of wind velocity the difference in
the results due to change in level of ambient
temperature is
100-90=10.
But at the high level of wind velocity, the difference in
the results due to change in level of ambient
temperature is
140-110=30.
Thus, the effect of changing ambient temperature is not
the same at the high and low levels of wind velocity.
Two-Variable Interactions
Likewise, the difference in the results at the
low level of ambient temperature due to the
change in wind velocity level is 110 - 90 - 20,
and the difference in the results at the high
level of ambient temperature is 140-100=40.
That is, the effect of changing the level of wind
velocity is not the same at both levels of
ambient temperature.
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
Two-Variable Interactions
In other words, the effect of ambient
temperature depends on the level of wind
velocity, they do not act independently of one
another.
1 1
E13 = (Y1 + Y3 + Y6 + Y8 ) − (Y2 + Y4 + Y5 + Y7 )
4 4
= −4650 psi
Three-Variable-Interaction, E123
Just as a two-variable interaction is a measure of the
joint effect of two–variables on a response, a three-
variable interaction is indicative of the joint effect of
three-variables on a response.
The procedure of estimating these effects is similar to
estimating the second order effects.
However, a simplified procedure that has been
developed to estimate all these effects will now be
discussed.
(2−1)
= ( 84 .0 − 87.5 )2 + ( 91 .0 − 87.5 )2
= 24 .50
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
( 2 − 1 ) + .......... . + ( 2 − 1 )
24.50 + 21.78 + ....... + 72
=
8
= 67.64 .
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
[(ya1 − y1)2 +( yb1 − y1)2]+[(ya2 − y2)2 +( yb2 − y2)2 +( yc2 − y2)2]+....+[ ya8 − y8)2 +( yb8 − y8)2]
Sp =
2
(2−1) +(2−1).........+(2−1)
M m = 2k
χν2=m −1 =
C Sample size = n
where N = n1+n2+…+nm
m
M = ( N − m) ln s 2p − ∑ (ni − 1) ln si2
i =1
1 m 1 1
C = 1+ ∑ −
3(m − 1) i =1 ni − 1 N − m
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
Bartlett test
s 2p = 67.64 N = 16, m = 8
M = (16 − 8) ln 67.64 − [(2 − 1) ln 24.5 + (2 − 1) ln 21.78
+ (2 − 1) ln134.48 + (2 − 1) ln 242 + (2 − 1) ln 3.92
+ (2 − 1) ln 8.82 + (2 − 1)33.62 + (2 − 1) ln 72.0]
= 5.713
1 8 1 1
C = 1+ ∑ −
3(8 − 1) i =1 2 − 1 16 − 8
1
= 1+ [8 − 5] = 1.357
21
IE 400 Lecture 10 2006 Dr. Shiv G. Kapoor All Rights Reserved
Bartlett Test
5.713
χcal
2
= = 4.21
1.357
χ7,2 α =0.05 = 14.1
Since χ2cal < χ2table, do not reject H0.
The variances are equal.
V(E1)=V(E2)+V(E3)=V(E12)=V(E13)=V(E23)=V(E123)=σ2/4
Table 4. 95% Confidence Intervals for the True Average Effects and Interactions
Average Effects 95% Confidence Interval
Ambient temperature ( E1) ±9480 psi
9150±
Wind Velocity (E2) -5100±±9480 psi
Bar Size (E3) ±9480 psi
850±
Two-Variable Interactions
Ambient temperature-Wind Velocity (E12) ±9480 psi
0±
Ambient temperature-Bar Size (E13) ±9480 psi
-4650±
Wind Velocity-Bar Size (E23) ±9480 psi
-100±
Three-Variable Interaction
±9480 psi
Ambient temperature-Wind Velocity-Bar Size (E123) 4700±
Redundancy in Two-Level
Factorials
Table 1
1 Mean
6 Main effects
15 Two-factor interaction
20 Three-factor interaction
15 Fourth order
6 Fifth order
1 Sixth order
64 Tests
IE 400 Lecture 15 @ 2006 Dr. Shiv G. Kapoor All Rights Reserved
A 23 Factorial Design
Table 2
-1 -1 -1 +1 +1 +1 -1
+1 -1 -1 -1 -1 +1 +1
-1 +1 -1 -1 +1 -1 +1
+1 +1 -1 +1 -1 -1 -1
-1 -1 +1 +1 -1 -1 +1
+1 -1 +1 -1 +1 -1 -1
-1 +1 +1 -1 -1 +1 -1
+1 +1 +1 +1 +1 +1 +1
Table 3
Run X1 X2 X3 X4
1 -1 -1 -1 -1 1
2 +1 -1 -1 -1
3 -1 +1 -1 -1
4 +1 +1 -1 -1 4
5 -1 -1 +1 -1
6 +1 -1 +1 -1 6
7 -1 +1 +1 -1 7
8 +1 +1 +1 -1
9 -1 -1 -1 +1
10 +1 -1 -1 +1 2
11 -1 +1 -1 +1 3
12 +1 +1 -1 +1
13 -1 -1 +1 +1 5
14 +1 -1 +1 +1
15 -1 +1 +1 +1
16 +1 +1 +1 +1 8
Calculation Matrix
1 + − − − − + + + + + + − − − − +
2 + + − − + − − + + − − + − − + +
3 + − + − + − − − − + − + − + +
4 + + + − − + − − − − + − − + + +
5 + − − + + + − − − − + + + − − +
6 + + − + − − + − − + − − + − + +
7 + − + + − − − + + − − − + + − +
8 + + + + + + + + + + + + + + + +
Consequences of Fractionating a
Full Factorial
Consequences of Fractionating a
Full Factorial
Consequences of Fractionating a
Full Factorial
Consequences of Fractionating a
Full Factorial
If we assume three- and four-factor interactions can
be neglected, the experiment produces the following
linear combinations:
l0 estimates mean
l1 estimates 1
l2 estimates 2
l3 estimates 3
l123 estimates 4
l12 estimates 12 + 34
l13 estimates 13 + 24
l23 estimates 23 + 14.
Consequences of Fractionating a
Full Factorial
Consequences of Fractionating a
Full Factorial
Average
Test 1 2 3 12 13 23 123 y
I
1 + − − − + + + − y1
2 + + − − − − + + y2
3 + − + − − + − + y3
4 + + + − + − − − y4
5 + − − + + − − + y5
6 + + − + − + − − y6
7 + − + + − − + − y7
8 + + + + + + + + y8
4 5
Test I 1 2 3 12 13 23 123 y
1 + − − − + + + − y1
2 + + − − − − + + y2
3 + − + − − + − + y3
4 + + + − + − − − y4
5 + − − + + − − + y5
6 + + − + − + − − y6
7 + − + + − − + − y7
8 + + + + + + + + y8
In the interest of
convenience we will 4 = 12
denote these as 4 = 12 + +
and 5 = 13, where the = − −
sign really implies an − −
identity between +
=
+
4×4=12×4, 5×5=13×5
which reduces to
I = 124, I = 135.
These two identities are referred to as our design
generators. While both the left- and right-hand
sides of the equation above represent columns
of all + signs, the right-hand side retains the
individual column headings that produced the
column of all + signs by their product.
IE 400 Lecture 15 @ 2006 Dr. Shiv G. Kapoor All Rights Reserved
Design Generators and the Defining
Relation
That is,
I column = 1 column × 2 column × 4 column
Now since both the 124 and 135 columns
equal I, their product must also equal I:
(124) × (135) = I,
or, rearranging numbers (columns),
(1)(1)2345 = I.
The identity
I = 124 = 135 = 2345
is referred to as the defining relation of this 25-2
fractional factorial design, and through it we can
reveal the complete aliasing/confounding
structure of this fractional factorial design.
Test I 1 2 3 12 13 23 123
1 + − − − + + + −
2 + + − − − − + +
3 + − + − − + − +
4 + + + − + − − −
5 + − − + + − − +
6 + + − + − + − −
7 + − + + − − + −
8 + + + + + + + +
l0 l1 l2 l3 l12 l13 l23 l123
That is,
l1 estimates 1 + 24 + 35 + 12345.
Similarly, moving to column headings 2, 3
and so on, we find that
2 = 14 = 1235 = 345
3 = 1234 = 15 = 245
12 = 4 = 235 = 1345
13 = 234 = 5 = 1245
23 = 134 = 125 = 45
123 = 34 = 25 = 145.
IE 400 Lecture 15 @ 2006 Dr. Shiv G. Kapoor All Rights Reserved
Linear Effects
Hence
l2 estimates 2 + 14 + 1235 + 345
l3 estimates 3 + 1234 + 15 + 245
….
l123 estimates 123 + 34 + 25 + 145.
We have now defined the complete confounding
pattern of this 25-2 fractional factorial design and
we know precisely what effect combinations we
can obtain from the data.
IE 400 Lecture 15 @ 2006 Dr. Shiv G. Kapoor All Rights Reserved
Summary
Summary
1 Mean
5 Main effects
10 Two-factor interaction effects
10 Three-factor interaction effects
5 Four-factor interaction effects
1 Five-factor interaction effects
32 Variable effects
Summary
Alias structure
Design Resolution
Design Resolution
Design Resolution
Shiv G. Kapoor
Department of Mechanical Science and Engineering
University of Illinois at Urbana-Champaign
y = b0 + b1 X 1 + b2 X 2 + b3 X 3 + b12 X 1 X 2 +
+ b13 X 1 X 3 + b23 X 2 X 3 + b123 X 1 X 2 X 3 + ε
(1)
Shiv G. Kapoor
Department of Mechanical Science and Engineering
University of Illinois at Urbana-Champaign
Level
1 + − − − − + + + + + + − − − − +
2 + + − − − − − − + + + + + + − −
3 + − + − − − + + − − + + + − + −
4 + + + − − + + − − − + − − + + +
5 + − − + − + − + − + − + − + + −
6 + + − + − − + − − + − − + − + +
7 + − + + − − − + + − − − + + − +
8 + + + + − + − − + − − + − − − −
9 + − − − + + + − + − − − + + + −
10 + + − − + − − + + − − + − − + +
11 + − + − + − + − − + − + − + − +
12 + + + − + + + + − + − − + − − −
13 + − − + + + − − − − + + + − − +
14 + + − + + − + + − − + − − + − −
15 + − + + + − − − + + + − − − + −
16 + + + + + + + + + + + + + + + +
Test I 1 2 3 4 5
1 + − − − − +
2 + + − − − −
3 + − + − − −
4 + + + − − +
5 + − − + − −
6 + + − + − +
7 + − + + − +
8 + + + + − −
9 + − − − + −
10 + + − − + +
11 + − + − + +
12 + + + − + −
13 + − − + + +
14 + + − + + −
15 + − + + + −
16 + + + + + +
Linear Effects
Estimation of Effects
Column Column
1 y
− 6.25
+ 6.25
− 7.75
+ 6.75
= (−6.25 + 6.25 − 7.75 + 6.75 − 6.25 + 5.25
− 6.25
+ 5.25 −6.75 + 6.75 − 7.00 + 5.25 − 8.00 + 7.00
− 6.75
+ × 6.75 −5.50 + 5.25 − 7.75 + 6.50) / 8
− 7.00
+ 5.25 = −0.78125 = l1
− 8.00
+ 7.00
− 5.50
+ 5.25
− 7.75
+ 6.50
Estimation of Effects
Summary
Summary
7.06 6.00
160º
Temperature, ºF
140º
6.75 6.25
Vertical Horizontal
Machine
Summary
5.75 7.31
160º
Temperature, ºF
140º
6.00 7.00
Blue Red
Pigment
Summary
Objective
To study effect of groove
geometry on the twist drill
performance.
Response Parameters:
Critical Depth
Experiments were conducted and the
response in terms of critical depth for each
experiment was collected.
Table 2 gives the design matrix and the
response for each experiment.
Effect Estimates
RESPONSE:CRITICAL DEPTH
RESPONSE:CRITICAL DEPTH
0 if y − m ≤ ∆ 0
L( y) =
A0 otherwise
• If y is the quality characteristic with
m as target value for y, the
quadratic loss function is given by –
L ( y ) = k ( y − m)
2
0 if y − m ≤ ∆ 0
L( y) =
A0 otherwise
• If y is the quality characteristic with
m as target value for y, the
quadratic loss function is given by –
L ( y ) = k ( y − m)
2
∆0
• Example: For a TV set, if the color density limit is m±7. The repair cost of
TV set is Rs 98 i.e. A0 = 98. Therefore, substituting in the above
equation, the loss function becomes –
98
L( y) = 2 (
y − m) = 2 ( y − m )
2 2
7
For y = m, loss = 0
For y = (m+7), the loss L(y) = 98
For y = (m + 2), L(y) = 8
For y = (m - 3), L(y) = 18
Classification of Parameters
• A number of parameters can influence the quality characteristics or
response or the product. These parameters are of three types [1] –
1. Signal factors
2. Noise factors
3. Control factors
• Signal factors (M): These are the parameters set by the user or operator
of the product to express the intended value for the response of the
product.
For example, speed setting on a
table fan is the signal factor that
specifies the amount of breeze.
The signal factors are selected by
the design engineering based on
the engineering knowledge of the
product being developed.
P Diagram
Classification of Parameters
• Noise factors (x): These factors can not be controlled by the
designer. Three classes of noise factors as defined little later. Only
the statistical characteristics such as mean and variance of noise
factors can be known or specified but the actual values are not
known.
• The noise factors cause the response y to deviate from the target
specified by the signal factor M and lead to quality loss.
n
−
(σ ) where µ = 1 ∑ yi and
n 1
Q = k ( µ − m ) +
2 2 n
1 n
σ2 = ∑ ( yi − µ )
2
n n i =1 n − 1 i =1
• For large n, we get
Q = k ( µ − m ) + (σ )
2 2
Noise Factors or Causes of Variation
• For large n, we get –
Q = k ( µ − m ) + (σ )
2 2
• Thus the average quality loss has the following two components –
k ( µ − m ) resulting from the deviation of the average value of y from the
2
–
target
– kσ 2 resulting from the mean squared standard deviation of y around its own
mean.
• Of the two, the first one is easier
to control.
• The second one, decreasing
variance is more difficult.
Means Plot or Analysis of Means [1] Final results, optimum levels are
indicated by * [1]
Optimum combination is
A1B1C2D2 or A1B1C2D3
η ( Ai , B j , Ck , Dl ) = µ + ai + b j + ck + dl + e
i =1
Example of a Taguchi Experiment
• It is decomposed into two parts – sum of squares due to mean and total
sum of squares given as below:
• Sum of square due to mean = (number of experiments) x m 2
= 9 (41.67)2 = 15625 (dB)2
• The total sum of the squares is given by –
9
= ∑ (ηi − m ) = ( −20 − 41.67 ) + ( −10 − 41.67 ) + ... + ( −70 − 41.76 )
2 2 2 2
i =1
= 3800 ( dB )
2
• Therefore, we get –
• Total sum of squares = (Grand total sum of squares) –
(Sum of squares due to mean)
3800 = 19425 - 15625
= 3 ( mA1 − m ) + 3 ( mA 2 − m ) + 3 ( mA3 − m )
2 2 2
= 3 ( 20 + 41.67 ) + 3 ( −45 + 41.67 ) + 3 ( −60 + 41.67 )
2 2 2
= 2450 ( dB )
2
*Indicates sum of squares added together to estimate the poled error sum.
F ratio is calculated by using pooled error mean square.
References
Orthogonal Array
• 2-level arrays are:
L4, L8, L12, L16,
L32, L64.
• 3-level arrays are:
L9, L27, L81
• 2- and 3-level arrays
are: L18, L36, L’36,
L54
• There are ways by
which the standard
orthogonal arrays
can be modified to
suit our
requirements.
L18 Orthogonal array
Orthogonal Array
L8 Orthogonal array
Interacting
column
Column
A
A
B C
D
D
B C
Here we get main effects of four factors Here we get main effects of four factors
but we get effect of interaction AxC and the three desired interactions AxB,
instead of the desired BxD BxC and BxD
B C
D
Orthogonal Array and Linear Graphs
Expt 1 2 3 4 5 6 7
No
1 B1 A1 C1 D1
2 B1 A1 C2 D2
3 B1 A2 C1 D1
4 B1 A2 C2 D2
5 B2 A1 C1 D1
6 B2 A1 C2 D2
7 B2 A2 C1 D1
8 B2 A2 C2 D2
B A AxB C BxC BxD D
4
3
5
6
L18 Orthogonal Array
Experimentation Strategy
Intermediate Strategy for selecting an orthogonal array [1]
Experimentation Strategy
• The strategy of experimentation can be based on the resolution of
experiment.
• As the resolution of an experiment increases, the number of experiments
to be performed increases.
• Resolution V: all factor effects and all 2-factor interactions can be
estimated.
• Resolution IV: no 2-factor interactions are confounded with the main
effects. Comparison of Resolution III and IV [1]
• In Resolution III:
No two main
effects are
confounded with
each other. The 2-
factor interactions
are confounded
with each other.
Experimentation Strategy
• Screening experiments: Usually, with resolution III experiment roughly
twice a many as parameters can be studied that the resolution IV
experiments.
• It is good to conduct a resolution III experiment to determine which
parameters out of a large number of parameters influence the response
variable.
• Modeling Experiments: The resolution IV are used to conduct
experiments with the parameters that are found important during the
screening experiment. They are used to build the mathematical model.
References
Fig. 1 Schematic of cutting process [2] Fig. 2 Rotary Tool for turning [2]
1 2 3 4 5 6 7
Ra St Resp A : Feed B: Speed AxB C : Angle Ax C BxC D: Volume
n onse 0.0840.17 22 88 15 45 10 30
8 1 0.252
1 2 0.372
5 3 0.606
4 4 0.610
7 5 0.516
6 6 0.400
2 7 0.607
3 8 0.780
Total 4.143
No of 24
Values
Average 0.173
Effect
% Effect
Case Study #1: Wear of Rotating Tools in
Machining of Composites
0.16 0.24
Feed (mm/rev) Feed (mm/rev)
Speed (m/min) Speed (m/min)
88 88
0.14 Angle (deg) Angle (deg)
Volume (%of SiCp) Volume (% of SiCp)
0.10
15 15
0.084 10 0.16
0.084 10
0.08
22 22
0.06 0.12
Fig. 4 Means plot for flank wear Fig 5 Means plot for flank wear
(After 10 seconds of machining) [2] (After 50 seconds of machining) [2]
• It shows that cutting speed is the most important parameter that governs
the wear. But it is more than volume of reinforcement in the composite.
• Therefore, it is processing parameters that govern the tool wear than the
volume of reinforcement in the composite material.
• Not much change in the processing parameters occur after 10 or 50 s of
machining.
Additive Function
• The goal of Taguchi design is to determine the best levels of each of the
control factors in the design of a product or a process.
• In many cases, it is observed that the effects of control factors on
response variables are additive by nature. This way the response
variables can be predicted for any combination of levels of the control
factors by knowing only the main effects.
• But, if the effects are not additive, then it is an indication that there are
strong interactions among the control factors.
• In such cases, experiments should be conducted under all the
combinations of control factors, that is full factorial experiments are to be
conducted, which will be highly expensive.
• When interactions are strong, then the conditions under which
experiments are conducted can also be considered as a control factor. In
such cases, laboratory experiments may not simulate the conditions at
customer site.
Additive Function
• The relative magnitude and importance of interactions can be reduced
greatly through the proper choice of quality characteristics, objective
function, and control factors.
• In general, Taguchi method recommends that as far as possible,
interactions between the control factors be avoided. This way, cross-
product term does not come into the model and the function becomes
additive.
• Some guidelines for achieving additivity are [1]:
– The quality characteristics should be directly related to the energy transfer
associated with the basic mechanism of the product or the process.
– As far as possible choose continuous variables as quality characteristics.
– The quality characteristic should be monotonic. The effect of control factor on
response variable should be in a consistent direction.
– Use a quality characteristics that is easy to measure.
– When a product consists of a number of systems with a feedback mechanism
then all the sub-systems should be optimized independently.
Quality Characteristic
• The quality characteristic selection is very important.
• Yield as a quality characteristics:
• Usually, every one wants to maximize the yield of a process or product.
• But, we do not realize that the yield of a process or product depends upon
a large number of sub-processes or sub-products.
• If we choose, final objective of increasing the yield then there will be huge
number of control parameters and their interactions.
• Therefore, it is necessary to refer to something basic of the process or a
key assembly of a product and optimize it, which will indirectly improve
the yield of the final product.
• Examples of objective functions are [1]:
1. Spray painting process: Size of droplet is the main factor which influences the
paint quality.
2. Chemical Process: If a chemical is formed out of three A,B,C. The better
objective function could be concentration of each that maximizes yield.
Quality Characteristic
3. Heat exchanger design:
In a heat exchanger, the
temperature (T2) of fluid to be Schematic of heat exchanger system [1]
cooled after comes out of the
cooling chamber should be the
criterion. One can try to control the
variation in this temperature.
Schematic of paper feeding [1]
• The second figure shows that some of the lines are not parallel to
each other. It means that the effect of factor A changes as we change
the level of factor B.
• Here the additive model we considered could be misleading. This
type of interaction is called s synergetic interaction.
• But the interaction in the last figure shows that there is a huge change
in the effects of factor A as the levels of factor B change. This is
called antisynergetic interaction. In this case, the linear additive
model which we considered will not be valid.
Column Merging
• By this method, a 4-level column can be created with all 2-level
columns, 9-level column with all 3-level columns and 6-level column
in a 2-level and 3-level orthogonal array [1].
• To create a 4-level column in a standard orthogonal array, any two
columns and their interactions can be merged.
• For example, in a L8 array, columns 1, 2, and 3 can be merged to
form a 4-level column.
• Since, three columns of 1 degree of freedom are merged to form a 3
degree of freedom, 4-level column. In the new column
• Combination (1,1) is designated as 1
• Combination (1,2) is designated as 2
• Combination (2,1) is designated as 3
• Combination (2,2) is designated as 4
• The columns corresponding to 1,2,3 are removed from the original
array and new 4-level array is introduced in it.
Column Merging
References
Dr. R. Balasubramaniam
Bhabha Atomic Research Centre
Trombay, Mumbai
5/16/2009 Dr.R.Balasubramaniam, BARC
Outline
• Burrs
• Deburring
• Design of Experiments
– External Burrs
– External Deburring
• Deburring Process
• Deburring Time
• Extent of Edge Radius Generated
– Internal Deburring
• Deburring Process
5/16/2009 Dr.R.Balasubramaniam, BARC
Burrs
• Burr, Edge and Surface Conditioning
Technology of SME defines
– Burrs as an undesirable projection on
materials formed as the result of plastic
flow from cutting, forming, blanking or
shearing operation which is unavoidable
in all kinds of machining operations.
Effects of Burrs
• Interfere with the assembly of
components
• Source of small particles inside the
assembly
• Seriously affects the performance and
reliability of the system
• Causes injury to operating personal
• External Deburring
• Internal/Inaccessible area Deburring
Deburring Methods
• Abrasive processes More than
50
• Mechanical processes
deburring
• Thermal processes processes
• Chemical processes are
practiced
• Electro chemical process
in
industries
Design of Experiment H
- External Burr T2
contd…
• 3 Input Parameters
Factor Low High
1 Response parameter
2 Level Expt:
TNR 0 mm 1 mm
• Full Factorial Experiment (A1) (A2)
DOC 0.5mm 2 mm
• 23 = 8
(B1) (B2)
• 3 Runs each Feed 0.05mm 0.15mm
• Total 24 runs (C1) (C2)
5/16/2009 Dr.R.Balasubramaniam, BARC
ANOVA Results of Burr Root
Thickness
Factors Sum of df Mean F-Ratio P-Value
squares Square
TNR(A) 2.7135 1 2.7135 131.07 0.0000*
DOC(B) 2.8359 1 2.8359 136.99 0.0000*
Feed (C) 0.4959 1 0.4959 23.96 0.0002*
AB 0.3384 1 0.3384 16.35 0.0011*
AC 0.3384 1 0.3384 16.35 0.0011*
BC 0.1890 1 0.1890 9.13 0.0086*
Error 0.3105 17 0.0207 P-Value less than 0.05
is significant
Total 7.2216 23
R-Squared = 95.7 R-Squared (Adjusted) = 94.18
Effect of Factors
Factors % Effect
TNR(A)
37.5
DOC(B)
39.3
Feed (C)
6.8
AB
4.6
AC
4.6
BC
2.6
Error
4.6
5/16/2009 Dr.R.Balasubramaniam, BARC
Main Factor Effects Plot
Burr Root Thickness
1.49
1.29
1.09
in mm
0.89
0.69
+ - - -
1.20
+
0.90 +
in mm
-
0.60
-
-
0.30
0
1 2 1 2 1 2
AB AC BC
5/16/2009 Dr.R.Balasubramaniam, BARC
Regression Co-efficients for Burr
Root Thickness
Factors Co-efficient
Constant -0.2975
A : TNR 1.5433
B : DOC 0.3800
C : Feed 2.2917
AB -0.3167
AC -4.7500
BC 2.3667
Regression Equation
• Burr Root Thickness
SOD Diameter
Edge Generation
Mixing ratio
Type of Abrasive
Velocity
5/16/2009Parameters
Input Dr.R.Balasubramaniam, BARC 17
Response parameters
Convex Edge
00, <h/2
Concave Edge
>00, <h/2
Taper Edge
0 0 0
0 1 0
1 0 0
1 1 1
NPR 0 1 0 0
MR 0 1 0 0
ASize 0 1 0 0
All 2 factors 0 6 0 0
Error 0 37 0 0
Total 12 47
• Fixed SOD
Regression Co-efficient
Factor Co-efficient
Constant 7.05
NPR(B) -1.05
MR(C) -20.0
ASize(D) -0.28
BC 3.33
BD -0.33
CD 0
5/16/2009 Dr.R.Balasubramaniam, BARC
Experiment for Extent of Edge
Radius Generated
• Convex Edge Radius
Regression Equation
Secondary
erosion on this
target
Primary erosion
on this target
Nozzle
• Removal of Burr
• Edge Radius
BSD
PL1
PL2
Tmax
Weak Burr Region
Hmax
No Burr Region
2700
ANOVA
Source Sum of Sq df Mean Sq. F-Ratio P-Value
MR(B) 0 1 0 0 1.0
AB 0 1 0 0 1
AC 0.75 1 0.75 37 0*
AD 0.75 1 0.75 37 0*
BC 0 1 0 0 1
BD 0 1 0 0 1
CD 0.75 1 0.75 37 0*
Total 5.25 47
• ASize
• SOD
• BSD
• Interactions of AC, AD and CD
Conclusions
• Design of Experiments and Analysis of
variables helped in
– Identifying the significant factors affecting the
response factors.
– Developing Regression Models
1 2 3 4 5 6 7
Ra St Resp
n onse
Total
No of
Values
Average
Effect
% Effect
Response Table for L8 orthogonal array
1 2 3 4 5 6 7
Ra St Resp
n onse
Total
No of
Values
Average
Effect
% Effect