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Introduction To Thermal Analysis

Introduction to Thermal Analysis

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71 views

Introduction To Thermal Analysis

Introduction to Thermal Analysis

Uploaded by

Sayantan Dex
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© © All Rights Reserved
Available Formats
Download as PDF, TXT or read online on Scribd
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M.E.

Brown

Introduction to Thermal Analysis


Techniques and Applications

Series: Hot Topics in Thermal Analysis and Calorimetry, Vol. 1

2nd ed. 2001, XII, 264 p.

Printed book

to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry


Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC
PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN:
0-306-48404-8 Print ISBN: 1-4020-0472-9 2004 Kluwer Academic Publishers New York,
Boston, Dordrecht, London, Moscow Print 2001 Kluwer Academic Publishers Dordrecht
All rights reserved No part of this eBook may be reproduced or transmitted in any
form or by any means, electronic, mechanical, recording, or otherwise, without written
consent from the Publisher Created in the United States of America Visit Kluwer Online at:
http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com
CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First
Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition
and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1
Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of
Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions
16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19
3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature
Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA)
29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.

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