Name : Ambient Air Name : Argon in Ambient Air

Instrument : Chemito GC with TCD Instrument : Chemito GC with TCD & Cryogenic Attachment

Analytical Conditions Analytical Conditions -

Col : Molecular sieve, 5A, 6ft 2 Col : Molecular sieve, 5A 6ft.
Inj : 50°C Inj : 30°C
Det : 100°C Det : 50°C
Col : 40°C 1 Col : 0°C 2 3
TCD : 220 mA TCD Current : 220 mA

1. Argon
1. Oxygen 2. Oxygen
2. Nitrogen 0 1 2 3 4 5 3. Nitrogen 0 4 8 12

Code No.: G_001 Code No.: G_002

Name : Reformer Gas Name : Reformer Gas with Ammonia

Instrument : Chemito 'GAS PARTITIONER GC' with TCD Instrument : Chemito 'GAS PARTITIONER GC'

Analytical Conditions Analytical Conditions

Col : Proapak Q & Molecular Sieve Col : 1% PEA on Porapak T + 25% KOH
Inj : 100°C on CHW(HP) & Molecular Sieve 13X, 20 ft
Det : 100°C Inj : 100°C
Col : 40°C Det : 100°C
TCD Current : 200 mA Oven : 85°C

1 5 6
1 23 4 6

1. Composite 2
2. CO2
3. NH3
1. Composite 4. H2
2. C02 5. Ar 7 8
3
3. O2 6. N2
4. N2 7. CH4
5 4 9
5. CH4 8. CO
6. CO 9. H20
0 5 10 15 0 5 10 15

Code No.: G_003 Code No.: G_004

Name : O2 & N2 in Argon Gas Name : Traces of Hydrocarbons in Ultra Pure Argon
Instrument : Chemito GC with TCD & AGSV Instrument : Chemito GC with FID & Methanator

Analytical Conditions Analytical Conditions

Col : Molecular Sieve 5A 6 ft. Col : Porapak N, 12 ft
Inj : 50°C Inj : 50°C
Det : 100°C Det : 100°C
Oven : 40°C Oven : 40°C
TCD Current : 110 mA Methanator : 390° C
Carrier : Argon Sample : 2 ml std Mix in Argon
Sample : 1 ml of 0.02% O2 & N2 each
in Argon Std.
1

2
1. CO (2ppm)
2. CH4 (1 ppm) 1 3
3. CO2 (10 ppm)
4. C2H2 (1 ppm) 2 4 5
1. Oxygen 5. C2H4 (1 ppm)
2. Nitrogen
0 1 2 3 0 5 10 15 20 25

Code No.: G_005 Code No.: G_006

Name : CO & CO2 Traces by Methanator Name : CO & CO2 Traces in Presence of Methane
Instrument : Chemito GC with Methanator & FID Instrument : Chemito GC with Methanator & FID

Analytical Conditions Analytical Conditions

Col : Unibead 'C' Col : Unibead 'C'
Inj : 100°C Inj : 100°C
Det : 100°C Det : 100°C
Oven : 80°C Oven : 80°C
Catalyst Temp: 390°C Catalyst Temp : 390°C
Sample : 2 ml of Std. Mix Sample : 2 ml of Std. Mix
1 1
2

2 3

1. CO (5 ppm)
1. CO (5 ppm ) 2. CH4 (2% )
2. CO2 (8 ppm ) 3. CO2 (8 ppm)
0 10 20 30 0 10 20 30

Code No.: G_007 Code No.: G_008

Name : N20 Traces Analysis Name : N20 Traces in Ambient Air

Instrument : Chemito GC with ECD Instrument : Chemito GC with ECD

Analytical Conditions Analytical Conditions

Col : Proapak N, 12ft Col : Proapak N, 12ft
Inj : 100°C Inj : 100°C
Det : 200°C Det : 200°C
Oven : 80°C ECD Source : 300°C
ECD Source : 300°C Sample : 1ml of Ambient Air
Sample : 1ml of N2O in Air

1
1

0 1 2 3 4 5 1. N2O 0 1 2 3 4 5
1. N2O (0.2 ppm)

Code No.: G_009 Code No.: G_010

Name : CO, CO2 & CH4 in Cracking Stream Name : H2 in Cracking Stream
Instrument : Chemito GC with FID & TCD Instrument : Chemito GC with FID & TCD
and Column Switching Valve and Column Switching Valve

Analytical Conditions Analytical Conditions

Col : Mol Sieve & Porapak Q Col : Mol Sieve & Porapak Q
Inj : 50°C Inj : 50°C
Det : 50°C 3 6 Det : 50°C
Oven : 40°C Oven : 40°C

2 5

1. CO 1 2
2. CH4
1 4
3. CO2
4. CO
5. CH4
6. CO2 1. H2
2. H2

0 2 3 4 5 0 2 4 6 8 10

Code No.: G_011A Code No.: G_011B

Name : Reformer Gas with Column Switching System Name : Coal Gas Analysis
Instrument : Chemito GC with TCD Instrument : Chemito GC with TCD (Partitioner)
and Column Switching Valve
Analytical Conditions
Analytical Conditions Col : Porapak Q & Mol. Sieve 13X
Col : 6'x1/8" S.S. Porapak Q & 8' x 1/8" S.S. Inj : 50°C
3
Mol. Sieve 5A Det : 100°C
Inj : 50°C Oven : 50°C
Det : 100°C Carrier : Helium 1
Oven : 50°C
TCD Current : 200 mA 1
Sample Qty. : 1 ml

2
5 4

2 3
1. CO2 (10%)
2. Ar (1%) 4
3. N2 (25%) 1. CO2
4. CH4 (0.5%) 2. N2
5. CO (10%) 3. CH4 0 5 10 15
0 5 10 4. CO

Code No.: G_012 Code No.: G_013

Name : Traces of H2S in Natural Gas Name : Traces of Carbonyl Sulfide in Ethylene
Instrument : Chemito GC with FPD Instrument : Chemito GC with FPD

Analytical Conditions Analytical Conditions

Col : Porapak QS 4 ft, Teflon Col : Porapak QS, 4 ft.
Inj. : 50° C Inj. : 50° C
Det. : 100° C Det. : 100° C
Oven : 50° C Oven : 50° C
Sample : 1 ml. of Natural Gas Sample : 1 ml Ethylene
Det. : Flame Photometric Detector
(Dual Flame)
1

1. COS (0.5 ppm)

1. H2S (1 ppm) 0 1 0 5 10

Code No.: G_014 Code No.: G_015

Name : Dissolved Gases in transformed Oil by CSV Name : Dissolved Gases in Transformer Oil with FID &
Instrument : Chemito GC with FID / TCD Methanator
Methanator & Column Switching Valve Instrument : Chemito GC with FID & Methanator

Analytical Conditions Analytical Conditions

Col : 12'x1/8” S.S. Porapak N+4'+1/8” Unibead 'C” Col : 20 ft. Porapak Q
Inj. : 50° C Inj. : 150° C
12
Det. : 100° C Det. : 200° C
Oven : 100° C 2 6 Oven : 50° C 150° c/min
Methanator : 390° C 3 180° C (Temp.Prog.)
Oven : 50° C Sample : 1 ml (500 ppm each in Nitrogen)
4
7 8
1. Hydrogen 3
2. CO2 4
5
3. Ethylene 5 1. CO 7
4. Ethane 2. CH4
5. Acetylene 3. CO2 6
6. CO 1 4. C2H2
7. Methane 5. C2H2
8. Propane+Propylene 6. C2H6
7. C3H6 +C3H8
0 5 10 15 20 0 5 10 15 20 25

Code No.: G_016 Code No.: G_017

Name : Bio- Gas Analysis Name : Sulphur Hexa Flouride
Instrument : Chemito GC with TCD (Ni Filament) Instrument : Chemito GC with TCD

Analytical Conditions Analytical Conditions

Col : Porapak QS Col : Porapak Q
Inj. : 100° C Inj. : 50° C 1
Det. : 200° C 12 3 Det. : 100° C
Oven : 50° C Oven : 40° C
Sample : 1 ul through AGSV PTFE Connection Sample : 0.5 ml
TCD Current : 200 mA.

4
1. AIR
2. CH4
3. CO2 1. SF6
4. H2S
0 1 2 3 4 5 0 1 2 3 4 5

Code No.: G_018 Code No.: G_019

Name : Impurities in Argon by DID Name : Impurities in Argon by DID

Instrument : Chemito GC with DID Instrument : Chemito GC with DID

Analytical Conditions Analytical Conditions

Col : Molecular Sieve, 5A 6 ft. Col : Porapak N, 6 ft.
Inj. : 50° C Oven : 40° C
Det. : 250 ul of Std. Gas Mix by AGSV 2 Det : Discharge Ionisation Detector
Sample : 250 ul. Std Gas by AGSV.
Std. Gas Mixture

1
3

1. Hydrogen (2 ppm) 4
2. Argon (Balance)
3. Nitrogen (3 ppm) 1
4. Methane (3 ppm) 5
5. CO (0.7 ppm)
1. CO2 (2.5 ppm)
0 5 10 15 0 1

Code No.: G_020 Code No.: G_021

Name : Ammonia in Air Name : Trace Oxygen in nitrogen

Instrument : Chemito GC with TCD & AGSV Instrument : Chemito GC with ECD & AGSV

Analytical Conditions Analytical Conditions

Col : 8.9% TEPA + KOH on Porapak Q Glass Col : Mol. Sieve 5A
Inj. : 50° C Inj. : 50° C
Det. : 100° C Det. : 200° C
Oven : 45° C ECD Source : 200° C
Sample : 1 ml of 1% Ammonia Sample : 1 ml

1. Ammonia (1%) 1. Oxygen (2 ppm)

0 1 2 3 4 5 0 0.1 0.2 0.3 0.4 0.5

Code No.: G_022 Code No.: G_023

Name : Mercaptan Traces Name : Carbon Monoxide Traces
Instrument : Chemito GC with FID & AGSV Instrument : Chemito GC with FID & Methanator

Analytical Conditions Analytical Conditions

Col : 10% Carbowax x 20M, 10 ft. PTFE Col : Mol. Sieve 13 X 6 ft.
Inj. : 100° C Inj. : 100° C
Det. : 150° C Det. : 100° C
Oven : 80° C Oven : 40° C
Sample : 1 ml. Of Std. Gas Ni Catalyst
PMT : 630 VDC Temp : 400° C
Sample : 1 ml. Of Stack Vent Gas 3

2
1

2
1 1. CO (65 ppm Std.)
1. H2S (2 ppb) 2. CO from Stack Vent 4
2. CH3SH (1ppm) 3. Methane
0 5 10 4. CO (6ppm)
0 5 0 5

Code No.: G_024 Code No.: G_025

Name : H2 S & COS in Propylene Name : Impurities in N-6 Grade Helium Gas
Instrument : Chemito GC with FPD & AGSV Instrument : Chemito GC with DID

Analytical Conditions Analytical Conditions

Col : Porapak QS, 1 mtr. PTFE Col : Mol. Sieve 13 X 6 ft.
Inj. : 100° C Inj. : 50° C
Det. : 200° C Det. : 100° C (Discharge Ionisation Detector)
Oven : 50° C Sample : 250 ul. Of N 6 Helium by AGSV
Sample : 1 ml of Propylene Gas
3

1 1. Inject 3
1. COS ( 2 ppm) 1
2. Ar+O2 ( 0.6 ppm)
2. HS (5 ppm)
3. N2 (0.3 ppm)
3. Propylene
0 1 2 3 4 5 0 1 2 3 4 5

Code No.: G_026 Code No.: G_027

Name : Gas Analysis

Instrument : Chemito GC with TCD

Analytical Conditions
Col : Molecular Sieve 5A, 3 Mtr X 1/8", S.S.
Inj. : 100° C
Det. : 80° C
Current : 200 mA
Oven : 150° C
Carrier : 25 ml/min (Helium)

1. O2 3
2. N2 1 4
3. Kr
4. Ar

0 5 10 15 20 25

Code No.: G_028