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Standardization of HCL Solution

This document provides instructions for preparing and standardizing a 1 N HCl solution. It lists the necessary glassware and equipment, which includes beakers, volumetric flasks, burettes, etc. It describes how to make a 100 mL 1 N HCl solution by diluting 9 mL of concentrated HCl with distilled water. The document then explains how to standardize the HCl solution by titrating it against a sodium carbonate primary standard using methyl red as an indicator. It provides the titration procedure and equations to calculate the normality of the HCl solution from the titration results.

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Pranav Kulkarni
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2K views12 pages

Standardization of HCL Solution

This document provides instructions for preparing and standardizing a 1 N HCl solution. It lists the necessary glassware and equipment, which includes beakers, volumetric flasks, burettes, etc. It describes how to make a 100 mL 1 N HCl solution by diluting 9 mL of concentrated HCl with distilled water. The document then explains how to standardize the HCl solution by titrating it against a sodium carbonate primary standard using methyl red as an indicator. It provides the titration procedure and equations to calculate the normality of the HCl solution from the titration results.

Uploaded by

Pranav Kulkarni
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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Preparation and Standardization

of 1 N HCl Solution
Glass ware and instruments:
preparation

beaker

washing bottle

glass stirrer

volumetric flask

graduated cylinders

fume hood

Preparation and Standardization


of 1 N HCl Solution
Glass ware and instruments:
standardization

conical flask

tripod stand

burette

wire gauze

burette stand

Bunsen burner

burette clamp

Preparation and Standardization


of 1 N HCl Solution
Glass ware and instruments:
standardization

spatula

watch glass

electrical balance

oven

Preparation and Standardization


of 1 N HCl Solution
p
preparation
p
of 100 mL of 1 N HCl solution
Dilute 9 mL of HCl with distilled water to a final
volume
l
off 100 mL
L using
i a 100 mLL volumetric
l
ti
flask.

N1 :the normality of concentrated HCl used


V1 :the volume of concentrated HCl to be used for dilution
N2 :the requested normality of HCl (1 N in our experiment)
V2 :final volume after dilution (100 mL in our experiment)

Preparation and Standardization


of 1 N HCl Solution

N :the normality of the concentrated acid


% : the
th weight
i ht by
b weight
i ht concentration
t ti off the
th acid
id
sp. gr. : the specific gravity of the acid
eq. w
eq
wt. :thee equ
equivalent
v e we
weight
g oof thee acid
cd

Preparation and Standardization


of 1 N HCl Solution
standardization
Na2CO3 + 2HCl

2NaCl + H2O + CO2

anhydrous sodium carbonate is used as the


primary standard
methyl red is used as the indicator

yyellow

faint p
pink

Preparation and Standardization


of 1 N HCl Solution
titration apparutus
pp

Preparation and Standardization


of 1 N HCl Solution
burette adjusment
j

Preparation and Standardization


of 1 N HCl Solution
burette adjusment
j

Preparation and Standardization


of 1 N HCl Solution
procedure
p
wash the burette with the D. W. and the titrant (HCl)
fill the
th burette
b tt with
ith HCl to
t a level
l l (adjust
( dj t it)
dissolve the primary standard (Na2CO3) in enough D. W.
((100 mL)) usingg the conical flask
add 2 drops of methyl red
start titration by adding HCl drop wise with continuous
stirring
ti i until
til the
th solution
l ti becomes
b
f i t pink
faint
i k
heat the solution to boiling so that the colour changes
back into yyellow,, cool,, and titrate again
g
until the faint p
pink
colour is no longer affected by boiling
record the volume of HCl used and calculate the
normality
lit

Preparation and Standardization


of 1 N HCl Solution
procedure
p

end
d point
i t
(faint pink)

Preparation and Standardization


of 1 N HCl Solution
calculations
HCl

Na2CO3

N :the
th normality
lit off HCl to
t be
b calculated
l l t d
V : the volume of HCl used (in mL)
wt. : thee we
w
weight
g oof sod
sodium
u ccarbonate
bo e ((in g)
eq. wt. : the equivalent weight of sodium carbonate

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