Post-Cocoon Processing Techniques
Post-Cocoon Processing Techniques
Structure
4.0 Objectives
4.1 Introduction
4.2 Raw Material - Cocoon
4.3 Cocoon Quality
4.4 Reeling Process
4.5 Raw Silk Testing and Grading
4.6 Twisting
4.7 Weaving Process
4.8 Wet Processing
4.9 Project for 100 ends Multi-end reeling basin unit to produce 10 kg raw silk/
day
4.10 Let Us Sum Up
4.11 Glossary
4.12 Suggested Further Reading
4.13 References
4.14 Answers to Check Your Progress
4.0 OBJECTIVES
After reading this unit, you will be able to:
l assess the quality of cocoon used for reeling;
l discuss about different processes involved in reeling and other processes to be
followed to process raw silk;
l identify the job opportunities in post-cocoon sector; and
l determine the profitability of a reeling unit.
4.1 INTRODUCTION
In the previous units, you have understood about the various entrepreneurial
opportunities in mulberry cultivation and silkworm rearing. In this unit, opportunities
in the post-cocoon sectors are discussed. Among all the textile fibres, silk occupies
the top place for the qualities of softness, lustre, dyeability, durability and elegance
and is regarded as the queen of textiles. The end products are saris, dress materials,
scarves, wall hangings, furnishing materials, neck-ties and also for industrial applications
such as parachutes and electric insulation etc.
(300)
Example = (320) × 100 = 94%
l) Percentage of Raw Silk Yield - Amount of raw silk obtained from the cocoons
and it is expressed in percentage and calculated as below:
Silk obtained 15 g
Raw silk % = Cocoon weight × 100 Example = 100 g × 100 = 15%
Raw silk % 15
RSR % = × 100 Example = × 100 = 83%
Shell Ratio % 18
n) Renditta : It is the quantity of cocoons required to produce 1kg of raw silk
and is calculated using the following formula:
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Entrepreneurial Opportunities Constants : Shell ratio Raw silk recovery percentage
in Sericulture
13 – 15 55%
15.1 – 18 60%
18.1 – 20 70%
20.1 – above 75%
1 1
Estimated renditta = Example = =7.9
M1×M2×M3 90/100×20/100×70/100
Note: If the good cocoon percentage is 90 and shell ratio is 20, calculate the estimated
renditta using the above standards and formula.
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Post-Cocoon Sector
4.4.4 Cooking
1) Wetting / retting: The cocoons are retted at 70 – 75 °C for 60 – 90 seconds.
2) High Temperature Treatment: The cocoons are treated at 90 - 92 °C for
90 – 120 seconds.
3) Low Temperature Treatment : The cocoons are treated at 70 – 75 °C for
60 – 90 seconds (permeation).
4) Cooking: Using steam the cocoons are treated at 97–98 °C for 90–120
seconds and then immersed in 97°C water for 60 seconds.
5) Conditioning : (Adjusting part) The treatment is carried out by sprinkling the
cold water and reducing the temperature from 97 to 70°C in about 4 to 6
minutes. Then, it is brushed and supplied to reeling.
4.4.5 Brushing
Brushing is an operation in which correct ends from the cooked cocoons are grouped
to facilitate reeling. Brushing operation has a direct relation to silk waste generation
and by using proper methodology, waste generation can be reduced and productivity
can be enhanced (Fig. 4.6).
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Post-Cocoon Sector
4.4.6 Reeling
Raw silk reeling is a process of combining number of ends of the cocoon filaments
together to form a single thread of desired denier. Since reeling operation bears a
close relationship to work efficiency and raw silk quality, it is necessary to give much
attention and take great care in the use of techniques, machinery and management to
produce good quality raw silk. Silk reeling in India is carried out on a variety of
reeling gadgets viz., charaka, Cottage basin and multi-end reeling machines (Fig.4.7).
4.4.7 Re-reeling
Re-reeling is done to transfer the raw silk reeled on small reel to large reel (1.5
meter circumference) for adjusting width, and length of the skein uniformity. The
other important objectives are to eliminate gum spots in the reeled silk, tie up any
loose ends to form continuous length of silk thread to eliminate thin places and to
ensure smooth and efficient operation during the winding process (Fig.4.8).
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Entrepreneurial Opportunities 4.4.8 Lacing of Skeins
in Sericulture
Silk skeins should be laced in order to keep the silk threads intact and avoid
entanglements. Silk skeins are laced at 6 places using the cotton thread in the form
of “8”. In order to facilitate the findings of ends of skeins during the next process, it
is essential to join and tie the top end and the tail end together by extra lacing thread
which is inserted in the middle of the breadth of the skeins. Each lacing will have 4
stitches to form 5 loops. Lot of care should be taken during lacing and removal of
silk skiens from the large reel to avoid breaking of silk threads (Fig.4.9).
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Post-Cocoon Sector
4.6 TWISTING
The raw silk twisting operations are: Soaking, Winding, Doubling, Twisting, Twist
Setting and Re-winding.
4.6.1 Soaking
The ingredients of soaking bath are soap, coconut oil, castor oil or Turkey red oil,
etc. The main objectives of this process are:
l to soften the skein for smooth unwinding,
l to reduce breaks in further processes, and
l to soften gum and lubricate the yarn to make it more pliable and ductile.
Method : Mix the required quantity of soaking agents in clean water. Heat it to 35
to 40 °C. Then dip the raw silk for 24 hours into it. Take out and dry the silk. Drying
can be outdoor (shaded place) or indoor (in a drying room).
4.6.2 Winding
Semi-dried skeins after soaking are subjected to winding process for better results.
The objectives of this process are:
l conversion of raw silk skein into double flanged bobbins,
l to get long continuous length of yarn, and
l to eliminate slubs, weak places, defective knots, etc.
Method: Silk yarn is mounted on a swift or creel. Creel is weighted by means of a
dead weight to keep it under sufficient tension, so that winding rate is uniform. The
winding speed is dependent on the denier of the raw silk thread and the winding
operation is conducted at 25 ± 2°C temperature and 65 ± 2% relative humidity.
4.6.3 Doubling
In order to produce twisted silk, two or more threads are wound parallel on to one
twisting bobbin. Doubling may be 2 ply, 3 ply, 4 ply or even more depending upon
the nature of fabric required. This process increases yarn evenness, strength and
fabric cover.
Method: The doubling machine consists of a creel for mounting double-flanged
winding bobbins. The yarn from the creel passes through thread guides and stop
motion mechanism and is wound onto a double-flanged bobbin as a folded yarn.
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4.6.4 Twisting Post-Cocoon Sector
4.6.6 Re-Winding
The process by which twisted silk is rewound on to bobbins or converted to skeins
(for degumming, bleaching, dyeing) and transport.
Method: The machine is similar to winding machine but double sided and production
is more, from parallel tubes of twisting to double flanged bobbins or cones or cheeses
or hanks. Sometimes, the twisted perforated bobbins are soaked for a while in
water at room temperature before rewinding to remove stickiness or gum spots.
4.8.1 Degumming
The removal of gum from silk is known as degumming or boiling-off. When the gum
is completely removed, the silk looses 20 to 30 % of its weight. It is advantageous
to use undegummed or partly degummed silk in the warp for weaving.
Method: Silk yarn in the form of yank is suspended on the smooth wooden or
stainless steel rod in a rectangular vessel containing 25-30% of the weight of silk.
The pH of the bath is maintained between 9.5 & 10.5. The yarn is treated at 90 -
95°C for 1 to 2 hours. Vigorous boiling is avoided as it tends to entangle the yarn.
The hanks are turned frequently.
4.8.2 Bleaching
This operation is required in case of yellow silk, which is to be made white. Silk
bleaching can be effected by the process of reduction or oxidation. Oxidation process
is preferred as it destroys the colouring matter.
Method: The bath should contain 3% in volume, which is best obtained by adding
to each litre of water, 30 cc of peroxide at 100 volume. The silk is put in the bath at
the temperature 50 to 60 °C slowly raised to 80 °C and kept in motion. It is then
completely immersed in the solution and allowed to cool to room temperature, taken
out, rinsed and brightened.
4.8.3 Dyeing
It can be dyed with direct dye, acid dyes, metallic complex dyes and reactive dyes,
which are commonly used. Basic dyes, Vat, solubolized vat dyes, azoic dyes and
mordant dyes are also used to a smaller extent. Most of the silk is dyed in hank form
in rectangular vats or on the rotating roller type of hank dyeing machine. Heavy
stains are dyed in the jigger. The material is handled carefully during dyeing to avoid
chafe marks.
Method: The dyestuff is dissolved in water, 10 to 40% glauber’s salt is added and
the goods entered in the dye bath at 40°C using material to liquor ratio of 1 : 40. The
temperature of the bath is raised slowly to 90°C and dyeing continued at this
temperature for 45 minutes to one hour. At the end of the dyeing period, 1 to 2%
glacial acetic acid or formic acid (80%) is added and dyeing continued for 10 to 15
minutes. For heavy shades 1 to 3% acetic acid or 8% ammonium acetate is added
to obtain satisfactory exhaustion.
4.8.4 Printing
Printing is reproduction of designs on the fabrics. There are two types of printing (1)
Block printing (2) Screen printing. Requirement for printing are (i) dye stuff, (ii)
solvent, (iii) thickener, (iv) levelling agent, (v) oxidizing agent.
Recipe: i) Dyestuff : x parts ii) Diethylene Glycol : 5 parts iii)Urea:5 parts iv)Thickener:
8 parts v) Ammonium sulphate : 5 parts : vi) acetic acid (40%) vii)Water (remaining
to 100 parts)
Method: Weigh the required amount of dyestuff in a beaker. Add a little quantity of
cold water, stir it, add di-ethylene glycol and urea, stir it properly, then add gum and 67
Entrepreneurial Opportunities remaining water to make 100 parts before printing. Add acetic acid or ammonium
in Sericulture
sulphate, stir well and print on bleached fabrics using screen. Dry the fabric for 30 to
60 minutes; keep it for steaming for 30 minutes at 102°C. Take out the fabrics,
wash with cold water and treat the fabric with 1 GPL Non-ionic detergent solutions
at room temperature for 5 minutes, then wash with cold water and dry the fabrics.
I. Equipments
Sl. Equipments Number Cost (Rs.)
No.
1. Boiler (200 kg. Capacity) 1 80,000
2. Hot air stifling chamber (for bivoltine 1 25,000
cocoons 50 kg capacity
3. Steam stifling chamber (for multivoltine 1 10,000
cocoons 25 kg capacity
4. Cocoon racks (20 trays) each tray of 5 10 20,000
kg capacity
5. Multi end reeling machine 10 basin 1 unit 3,50,000
capacity along with 8 window re-reeling
and 2 nos. of 3 pan cooking units and
pressurized cooking units
6. Epprouvette 2 1,400
7. Denier scale 1 700
8. Examination stand 2 800
9. Balance (50 kg capacity) 1 10,000
10. Physical balance 1 500
11. Skeinning machine 1 400
12. Book pressing machine 1 900
13. Steel almirah for silk storage 1 3,000
Total 5,02,700
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II. Working capital Post-Cocoon Sector
4.11 GLOSSARY
Bale : A defined quantity of raw silk carefully wrapped as
a cotton cloth and gunny cloth. An Indian Bale weighs
20 Kgs.
Book : is a bundle of skeins of raw silk. A bale of Japanese
silk contains 30 books, each 2 kg. in weight and
containing about 30 skeins.
Cocoon : The silken shell spun by a silkworm larvae that serves
as protective covering to the insect during its pupal
stage of existence.
Cooking (Silk) : The process by which the silk cocoons are treated
in boiling water with a view to softening the filament
for easy unwinding during the subsequent reeling
process.
Degumming : A process of removing the sericin or gum from silk
yarn or fabric by boiling in a soap solution.
Denier : The unit for expressing the size of the silk filament.
It is weight in gms of 9,000 mts. of yarn.
Doubling : The twisting together of two or more silk threads to
70
give a yarn suitable for weaving.
Elongation : It is the distance between the length of stretched Post-Cocoon Sector
specimen and its initial length, expressed as a
percentage of initial length.
Fibroin : The fibre material of raw silk thread which is a protein
non-soluble in boiling water.
Filament : A fibre of indefinite or extreme length, eg. Silk
filament, which runs from 300 to 1,200 m.
Grade (Silk) : Classification of raw silk on the basis tests carried
out according to standard methods in silk conditioning
and testing house.
Gum : A sticky protein material that coats the filaments of
raw silk. This is otherwise called as “Sericin”.
Raw Silk : The silk reeled by drawing together the required
number of filaments from the cocoons and contains
its original gum or sericin.
Reeling : The process of unwinding silk filament from the
cocoon.
Tenacity : The tenacity of a material is the mass stress at break,
unit being grams per denier or per tex.
4.13 REFERENCES
Anonymous. 2005. Technical Note, Central Silk Technological Research Institute,
Bangalore.
Anonymous. Reeling Techniques for Quality Silk, Central Silk Technological
Research Institute, Geethanjali printers, Bangalore.
Carboni, P. 1972. Silk Biology, Chemistry and Technology. 71
Entrepreneurial Opportunities Manual on Bivoltine Silk Reeling Technology, 2003 (JICA), Central Silk Board,
in Sericulture
Bangalore.
Marks, R. and Robinson, R.T.G, 1976, Principles of Weaving, Textile institute of
Manchester.
Report on Silk Reeling by Dr. Chiyuki Takabayashi, February, 1992.
Report on Silk Reeling by Haruo Kinoshita, November, 1992.
Report of Silk Reeling by Kozo Tsubouchi, December, 1993.
Silk Reeling Technology by T.N. Sonwalkar.
8 (g)
Example = 40 (g) × 100 = 20%
Wt. in gms.
Denier = × 9000
Length in mts.
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Post-Cocoon Sector
(0.300 g)
Example = × 9000 = 2.7d.
(1000 m)
(300)
Example = (320) × 100 = 94%
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